CN203295482U - Device capable of utilizing ozone to deeply purifying distilled liquor - Google Patents
Device capable of utilizing ozone to deeply purifying distilled liquor Download PDFInfo
- Publication number
- CN203295482U CN203295482U CN2013203193079U CN201320319307U CN203295482U CN 203295482 U CN203295482 U CN 203295482U CN 2013203193079 U CN2013203193079 U CN 2013203193079U CN 201320319307 U CN201320319307 U CN 201320319307U CN 203295482 U CN203295482 U CN 203295482U
- Authority
- CN
- China
- Prior art keywords
- ozone
- condensing tower
- tower
- steamer
- air outlet
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Images
Landscapes
- Treatment Of Water By Oxidation Or Reduction (AREA)
Abstract
The utility model discloses a device capable of utilizing ozone to deeply purifying distilled liquor. The device comprises a distillation still and a condensing tower mutually connected, wherein an ozone feeding pipe I is connected onto the still head of the distillation still, and the air outlet of the ozone feeding pipe I is formed in the middle of the still head of the distillation still. According to the device, gaseous ozone is fully mixed with liquor steam, so that the contact area of the ozone and the steam is larger, and the use ratio of ozone is greatly improved; as the ozone and steam mixture cannot reach the dissolution extremity of ozone, the additive amount of ozone can be adjusted according to the actual requisite amount, and the purpose of deeply purifying distilled liquor is realized.
Description
Technical field
The utility model relates to a kind of refining plant of wine, particularly relates to a kind of ozone that utilizes and liquor is carried out the device of deep purifying.
Background technology
Ozone is a kind of unstable at normal temperatures and pressures, has the light blue gas of special odor.Ozone has extremely strong oxidation susceptibility, has the oxidizing potential of 2.07mv in basic solution, and its oxidation capacity is only second to fluorine,, higher than chlorine and potassium permanganate, is desirable Green Oxidant, at nature, can decompose voluntarily in the short period of time, there is no secondary pollution.Why ozone shows strong oxidizing property, because Sauerstoffatom in ozone molecule has strong electrophilic or proton characteristic, the nascent oxygen molecule that ozone decomposed produces, form the hydroxyl radical free radical OH with strong oxidation in its solution, the high reactivity of hydroxyl radical free radical OH is used to sterilization and disinfection in the aqueous solution, destroy organic constitution, the nontoxic non-secondary pollution of its by product.
Objectionable constituent in wine and different assorted flavor material mainly contain the above higher fatty acid ethyl esters of aldehydes, potato spirit, sulfide, 12 carbochains and heavy metal etc.The mechanism of removing objectionable constituent in wine with ozone is: the nascent oxygen molecule of ozone decomposed and the free radical OH of strong oxidizing property, the alcohol, acid, water and the carbonic acid gas that make unsaturated link(age) in harmful organic substance or conjugated double bond fragment into small molecular weight.The mineral ions such as all right plumbous oxide of ozone, manganese, iron, zinc and cadmium, the oxide compound flocculation sediment of generation indissoluble, help to filter and remove.After for example ozone can be oxidized to Fe2+ Fe3+, hydrolysis generates Fe (OH) 3 precipitations.
At present, adopt the liquid wine of ozone purification, have following problem:
1) the ozone solution degree is low, can not thoroughly purify by liquid towards wine;
2) liquid wine adopts low concentration ozone to process harmful organic substance, can not be carbonic acid gas and water with the harmful organic substance complete oxidation, also can generate a series of intermediate product, as aldehyde and acid etc.;
3) ozone is extremely unstable, and when ozone concn was 3mg/l in its solution, the transformation period was about 30 minutes, and therefore, the harmful organic substance oxidation in liquid towards wine is not thorough.
Summary of the invention
The utility model provides a kind of ozone that utilizes liquor to be carried out the device of deep purifying for solving the technical problem that exists in known technology, this device utilizes the harmful organic substance reaction in ozone and wine steam, thereby reaches the purpose of liquor being carried out deep purifying.
The technical scheme that the utility model is taked for the technical problem that exists in the solution known technology is: a kind of ozone that utilizes carries out the device of deep purifying to liquor, comprise interconnective still kettle and condensing tower, be connected with ozone on the still head of described still kettle and add the pipe I, described ozone adds the air outlet of managing I to be positioned at the still centriciput of described still kettle.
This device also comprises rectifying tower, the inlet mouth of described rectifying tower is connected with the steam outlet of described still kettle, the air outlet of described rectifying tower is connected with described condensing tower, be connected with ozone in the bottom of described rectifying tower and add the pipe IV, described ozone adds the air outlet of managing IV to be positioned at the lower middle position of described rectifying tower.
This device also comprises back and heats up in a steamer condensing tower, heating up in a steamer condensing tower for described time is connected between described rectifying tower and described still kettle, be connected with ozone in the bottom of heating up in a steamer condensing tower for described time and add the pipe II, the lower middle position that described ozone adds the air outlet of managing II to be positioned to heat up in a steamer condensing tower described time.
Be connected with ozone on the top of heating up in a steamer condensing tower for described time and add the pipe III, the upper middle position that described ozone adds the air outlet of managing III to be positioned to heat up in a steamer condensing tower described time.
Advantage and the positively effect that the utlity model has are:
The ozone amount of 1) sneaking in wine steam can increase according to needs, the objectionable constituent in can exhaustive oxidation wine.
2) intermediate product that in ozone and wine steam, the objectionable constituent reaction generates can be generated carbonic acid gas and water by further oxidation in enough O3.
3) ozone and wine vapor mixing do not need to stir, and with oxidized harmful organic substance, directly contact, and contact area increases greatly, are conducive to the complete, thorough of oxidizing reaction.
In sum, the utility model adopts gaseous ozone fully to mix with wine steam, and gas, vapour mixing contact area are very big, has improved widely the utilization ratio of ozone; There do not is again the solubility limit of ozone due to the mixing of gas, vapour, so the addition of ozone can be measured adjusting according to the actual needs, thereby reach the purpose of deep purifying liquor.
Description of drawings
Fig. 1 is structural representation of the present utility model.
In figure: 1, still head, 2, return and to heat up in a steamer condensing tower, 3, rectifying tower, 4, condensing tower, 5, ozone adds the pipe I, 6, ozone adds the pipe II, 7, ozone adds the pipe III, 8, ozone adds the pipe IV, 9, ozone adds the pipe V.
Embodiment
, for further understanding summary of the invention of the present utility model, Characteristic, hereby exemplify following examples, and coordinate accompanying drawing to be described in detail as follows:
See also Fig. 1, a kind of ozone that utilizes carries out the device of deep purifying to liquor, this device adopts traditional structure, there is no rectifying tower 3 as shown in Figure 1 and return and heat up in a steamer condensing tower 2, only comprise interconnective still kettle and condensing tower 4, be connected with ozone and add pipe I 5 on the still head 1 of described still kettle, described ozone adds the air outlet of managing I 5 to be positioned at still head 1 middle part of described still kettle.
Further, the device of above-mentioned deep purifying also comprises rectifying tower 3, the inlet mouth of described rectifying tower 3 is connected with the steam outlet of described still kettle, the air outlet of described rectifying tower 3 is connected with described condensing tower 4, be connected with ozone in the bottom of described rectifying tower 3 and add pipe IV 8, described ozone adds the air outlet of managing IV 8 to be positioned at the lower middle position of described rectifying tower 3.
Further, the device of above-mentioned deep purifying, also comprise back and heat up in a steamer condensing tower 2, heating up in a steamer condensing tower 2 for described time is connected between described rectifying tower 3 and described still kettle, be connected with ozone in the bottom of heating up in a steamer condensing tower 2 for described time and add pipe II 6, the lower middle position that described ozone adds the air outlet of managing II 6 to be positioned to heat up in a steamer condensing tower 2 described time., in order to improve decontamination effect improving, can be connected with ozone on the top of heating up in a steamer condensing tower 2 for described time and add pipe III 7, the upper middle position that described ozone adds the air outlet of managing III 7 to be positioned to heat up in a steamer condensing tower 2 described time.Connect ozone in condensing tower 4 bottoms and add pipe V 9.
Add at ozone on the air outlet of pipe even distribution device preferably be set, be beneficial to ozone more equably with the wine vapor mixing.Can add negative pressure device in the condensation link if necessary, whole steaming wine system is distilled under negative pressure, be conducive to adding of ozone.
In the present embodiment, one have five ozone and add a little:
1) at the still centriciput of still kettle;
2) returning the lower middle position of heating up in a steamer condensing tower;
3) returning the upper middle position of heating up in a steamer condensing tower;
4) in the lower middle position of rectifying tower;
5) in the mid-way, bottom of condensing tower.
The principle of work of the device of above-mentioned deep purifying:
One) steam, by the wine unstrained spirits of fermenting-ripening, forms the wine steam with certain alcoholic strength;
Two) wine steam is up, harmful organic substance wherein and the O that introduces in the still head
3Oxidizing reaction occurs, and makes wine steam obtain deep purifying for the first time;
Three) continue through the wine steam after deep purifying for the first time up, harmful organic substance wherein with enter back the O that heats up in a steamer the condensing tower bottom
3Oxidizing reaction occurs, and makes wine steam obtain deep purifying for the second time;
Four) continue through the wine steam after deep purifying for the second time up, harmful organic substance wherein with enter back the O that heats up in a steamer condensing tower top
3Oxidizing reaction occurs, and makes wine steam obtain deep purifying for the third time;
Five) enter the rectifying tower bottom through the wine steam after deep purifying for the third time, harmful organic substance wherein and the O that enters the rectifying tower bottom
3Oxidizing reaction occurs, and makes wine steam obtain deep purifying the 4th time;
Six) enter condensing tower through the wine steam after the 4th deep purifying, form liquid wine body, the harmful organic substance in liquid wine body and the O that enters the condensing tower bottom
3Oxidizing reaction occurs, and makes liquid wine body obtain deep purifying.
With above-mentioned principle in like manner,, for the traditional Distallation systm that there is no back to heat up in a steamer condensation flow process and distillation process,, because there is no back the condensing tower of heating up in a steamer and rectifying tower, only need in still kettle still head and the bottom of condensing tower adds ozone and adds a little.Equally, distillation process is arranged, can add ozone in the bottom of rectifying tower and add a little.Have back and heat up in a steamer the condensation flow process, can add ozone and add a little going back to the bottom of heating up in a steamer condensing tower, preferably add ozone and add a little going back to the top of heating up in a steamer condensing tower simultaneously, further strengthening the deep purifying effect.
Although the above is described preferred embodiment of the present utility model by reference to the accompanying drawings; but the utility model is not limited to above-mentioned embodiment; above-mentioned embodiment is only schematic; be not restrictive; those of ordinary skill in the art is under enlightenment of the present utility model;, not breaking away from the scope situation that the utility model aim and claim protect, can also make a lot of forms, within these all belong to protection domain of the present utility model.
Claims (4)
1. one kind is utilized ozone liquor to be carried out the device of deep purifying, it is characterized in that, comprise interconnective still kettle and condensing tower, be connected with ozone on the still head of described still kettle and add the pipe I, described ozone adds the air outlet of managing I to be positioned at the still centriciput of described still kettle.
2. the ozone that utilizes according to claim 1 carries out the device of deep purifying to liquor, it is characterized in that, also comprise rectifying tower, the inlet mouth of described rectifying tower is connected with the steam outlet of described still kettle, the air outlet of described rectifying tower is connected with described condensing tower, be connected with ozone in the bottom of described rectifying tower and add the pipe IV, described ozone adds the air outlet of managing IV to be positioned at the lower middle position of described rectifying tower.
3. the ozone that utilizes according to claim 2 carries out the device of deep purifying to liquor, it is characterized in that, also comprise back and heat up in a steamer condensing tower, heating up in a steamer condensing tower for described time is connected between described rectifying tower and described still kettle, be connected with ozone in the bottom of heating up in a steamer condensing tower for described time and add the pipe II, the lower middle position that described ozone adds the air outlet of managing II to be positioned to heat up in a steamer condensing tower described time.
4. the ozone that utilizes according to claim 3 carries out the device of deep purifying to liquor, it is characterized in that, be connected with ozone on the top of heating up in a steamer condensing tower for described time and add the pipe III, the upper middle position that described ozone adds the air outlet of managing III to be positioned to heat up in a steamer condensing tower described time.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2013203193079U CN203295482U (en) | 2013-06-04 | 2013-06-04 | Device capable of utilizing ozone to deeply purifying distilled liquor |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2013203193079U CN203295482U (en) | 2013-06-04 | 2013-06-04 | Device capable of utilizing ozone to deeply purifying distilled liquor |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN203295482U true CN203295482U (en) | 2013-11-20 |
Family
ID=49571512
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2013203193079U Expired - Fee Related CN203295482U (en) | 2013-06-04 | 2013-06-04 | Device capable of utilizing ozone to deeply purifying distilled liquor |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN203295482U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103232934A (en) * | 2013-06-04 | 2013-08-07 | 李建东 | Method and device for deeply purifying distilled liquor by utilizing ozone |
-
2013
- 2013-06-04 CN CN2013203193079U patent/CN203295482U/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103232934A (en) * | 2013-06-04 | 2013-08-07 | 李建东 | Method and device for deeply purifying distilled liquor by utilizing ozone |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN102992541B (en) | Method for simultaneously extracting iodine and fucoidin from salted kelp blanching wastewater | |
| CN102491451A (en) | Device and method with ultrasonic ozone and ultraviolet synergized for water treatment | |
| CN101781068B (en) | Method for treating crude wastewater of gallic acid | |
| CN101574656A (en) | Nanometer cobalt ion-doped titanic anhydride catalyst and preparation method thereof | |
| CN103266049B (en) | Method and device for carrying out comprehensive deep purification on distilled liquor | |
| CN106554140B (en) | A kind of residual active sludge cracks decrement method | |
| CN203295482U (en) | Device capable of utilizing ozone to deeply purifying distilled liquor | |
| CN101658789A (en) | Metal-doped oxyhydroxide catalyst and preparation method and application thereof | |
| Chaohui et al. | Remove of ammoniacal nitrogen wastewater by ultrasound/Mg/Al2O3/O3 | |
| CN106823737A (en) | A kind of administering method of garbage transfer station foul gas | |
| CN103232934A (en) | Method and device for deeply purifying distilled liquor by utilizing ozone | |
| CN101838075A (en) | Process for effectively treating organophosphorus pesticide wastewater | |
| CN203295485U (en) | Device for comprehensively and deeply purifying distilled liquor | |
| CN102381943B (en) | System and technology for producing coked crude phenol | |
| CN104445575B (en) | A kind of deep oxidation treatment process of steroid hormone medicine waste water | |
| CN100999370A (en) | Treatment method of high alkalinity organic waste water | |
| CN201495121U (en) | Multifunctional chlorine dioxide disinfection device | |
| CN101607751B (en) | Method for treating organic toxic high-concentration wastewater difficult in biochemical degradation by electrolysis and high-grade oxidation combined process | |
| CN103130368A (en) | Treatment method for rapid degradation of power plant citric acid boiler cleaning waste water | |
| CN103723816B (en) | A kind of continuous degradation AES vacuum removal water Zhong diox method and treatment unit | |
| CN215855122U (en) | Device for removing free chlorine in waste sulfuric acid | |
| CN203668149U (en) | Treatment device for continuously degrading dioxane | |
| CN216236249U (en) | Aeration system for applying ozone catalytic oxidation tail gas to activated sludge | |
| CN204897643U (en) | Ozone catalytic oxidation unites biological activity charcoal filtering pond integration equipment | |
| CN102805996A (en) | Purification treatment process and system for nitrogen oxide waste gas generated during preparation of catalyst for butadiene through oxidative dehydrogenation of butene |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20131120 Termination date: 20180604 |