CN203178224U - Multifunctional low temperature destructive distillation tester - Google Patents
Multifunctional low temperature destructive distillation tester Download PDFInfo
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- CN203178224U CN203178224U CN 201320213170 CN201320213170U CN203178224U CN 203178224 U CN203178224 U CN 203178224U CN 201320213170 CN201320213170 CN 201320213170 CN 201320213170 U CN201320213170 U CN 201320213170U CN 203178224 U CN203178224 U CN 203178224U
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- temperature
- destructive distillation
- field generator
- water tank
- pipe
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Abstract
The utility model relates to a multifunctional low temperature destructive distillation tester, and belongs to the field of oil shale detection. The device comprises a temperature control box and further comprises a temperature field generator and a destructive distillation condensation collector, wherein the output end of the temperature field generator is connected with the input end of the temperature control box; the temperature field generator comprises a temperature sensor, an insulator, a heat conducting pipe, a temperature field quartz heat source, a front separator of a heating body, a rear separator of the heating body, a rear cover, a front cover and a shell; and the destructive distillation condensation collector comprises a water tank, a destructive distillation tube bracket, a destructive distillation tube, a gas guide tube and a cone-shaped flask. By means of the Gray-King low temperature destructive distillation test technology, the tester has the advantages of accurate and reliable analytical result, perfect and stable performance, advanced and scientific technology and the like, and is an innovation and novel technology in the field of oil shale test at home at present.
Description
Technical field
The utility model belongs to the resinous shale detection range, is specifically related to a kind of multifunctional low-temperature destructive distillation tester.
Background technology
The resinous shale oil content is the important means of estimating the resinous shale development and use, is the important indicator of estimating and instruct oil shale recovery, processing and utilization.Parameters such as oil content, char yeild and total moisture productive rate provide reliable foundation for resinous shale production, evaluation and refinement.
Resinous shale is a kind of important alternative energy, and the major industry purposes is oil refining and as industrial chemicals, constantly soaring along with international oil price, and energy crisis has become very important major issue.China has put into effect the policy of various encouragement new development new forms of energy as second-biggest-in-the-world energy resource consumption state, and the resinous shale development and utilization just sharply heats up at home.And it is just particularly urgent to develop domestic convenient, quick, accurate, a reliable resinous shale detecting instrument that does not still have.
Summary of the invention
At the deficiencies in the prior art, the utility model proposes a kind of multifunctional low-temperature destructive distillation tester, improve the purpose that detects resinous shale oil content convenience, rapidity, accuracy, reliability to reach.
A kind of multifunctional low-temperature destructive distillation tester, comprise temperature-controlled cabinet, also comprise warm field generator and destructive distillation condensation gatherer, wherein, the output terminal of temperature field generator connects the input end of temperature-controlled cabinet, described temperature field generator comprises temperature sensor, thermal insulator, heat pipe, a temperature quartzy thermal source, dividing plate before the calandria, the calandria rear bulkhead, bonnet, protecgulum and shell, wherein, the body outer periphery of described heat pipe is equipped with a temperature quartzy thermal source, the outer periphery of a temperature quartzy thermal source is equipped with thermal insulator, the thermal insulator outer periphery is equipped with shell, above-mentioned heat pipe, a temperature quartzy thermal source and thermal insulator constitute the heating main body, be provided with the preceding dividing plate of calandria between described heating body front end and the protecgulum, be provided with the calandria rear bulkhead between heating body rear and the bonnet, and the heating body rear is inserted temperature sensor; Described destructive distillation condensation gatherer comprises water tank, destructive distillation pipe holder, destructive distillation pipe, wireway and conical flask, and described destructive distillation pipe is arranged in the heat pipe of warm field generator, and its destructive distillation mouth passes in the plug insertion conical flask; Described wireway passes plug and inserts in the conical flask; Described destructive distillation pipe is fixed on the water tank by the destructive distillation pipe holder.
Described temperature field generator is four, and the output terminal of temperature sensor is as the output terminal of warm field generator.
Described water tank is drawer type water box, is provided with the conical flask position-limited rack for designated water level in the water tank.
Described water tank is outside equipped with for the water tank supporting seat that supports water tank.
The utility model advantage:
A kind of multifunctional low-temperature destructive distillation of the utility model tester, this instrument utilizes lattice gold low-temperature pyrolysis measuring technology, have analysis result accurately and reliably, advantage such as stable, the advanced technology science of perfect performance, be big innovation and a new technique of present domestic resinous shale field tests, extensively promote the use of at home.
Description of drawings
Fig. 1 is the one-piece construction right view of a kind of embodiment of the utility model;
Fig. 2 is the one-piece construction rear view of a kind of embodiment of the utility model;
Fig. 3 is the warm field generator structural representation of a kind of embodiment of the utility model;
Fig. 4 is the destructive distillation condensation collector structure synoptic diagram of a kind of embodiment of the utility model;
Fig. 5 is the plant bulk synoptic diagram of a kind of embodiment of the utility model;
Fig. 6 is the device circuit schematic diagram of a kind of embodiment of the utility model;
Fig. 7 is the program I temperature control curve map of a kind of embodiment of the utility model;
Fig. 8 is the program II temperature control curve map of a kind of embodiment of the utility model;
Fig. 9 is the operation interface synoptic diagram of a kind of embodiment of the utility model.
Embodiment
Below in conjunction with accompanying drawing a kind of embodiment of the utility model is described further.
A kind of multifunctional low-temperature destructive distillation tester, as depicted in figs. 1 and 2, comprise temperature-controlled cabinet 3, also comprise warm field generator 1 and destructive distillation condensation gatherer 2, wherein, four of warm field generator 1 output terminals 1,2,3 are connected the input end 1,2,3 and 4 of temperature-controlled cabinet 3 with 4.
As shown in Figure 3, described temperature field generator 1 comprises temperature sensor 1-1, thermal insulator 1-2, heat pipe 1-3, a temperature quartzy thermal source 1-4, dividing plate 1-5 before the calandria, calandria rear bulkhead 1-6, bonnet 1-7, protecgulum 1-8 and shell 1-9, wherein, the body outer periphery of described heat pipe 1-3 is equipped with a temperature quartzy thermal source 1-4, the outer periphery of a temperature quartzy thermal source 1-4 is equipped with thermal insulator 1-2, thermal insulator 1-2 outer periphery is equipped with shell 1-9, above-mentioned heat pipe 1-3, a temperature quartzy thermal source 1-4 and thermal insulator 1-2 constitute the heating main body, be provided with the preceding dividing plate 1-5 of calandria between described heating body front end and the protecgulum 1-8, be provided with calandria rear bulkhead 1-6 between heating body rear and the bonnet 1-7, and the heating body rear is inserted temperature sensor 1-1.Described temperature field generator 1 is four, and the output terminal of temperature sensor 1-1 is as the output terminal of warm field generator 1.
As shown in Figure 4, described destructive distillation condensation gatherer 2 comprises water tank 2-1, destructive distillation pipe holder 2-2, destructive distillation pipe 2-3, wireway 2-4 and conical flask 2-5, described destructive distillation pipe 2-3 is arranged in the heat pipe 1-3 of warm field generator 1, and its destructive distillation mouth passes among the plug insertion conical flask 2-5; Described wireway 2-4 passes plug and inserts among the conical flask 2-5; Described destructive distillation pipe 2-3 is fixed on the water tank 2-1 by destructive distillation pipe holder 2-2; Described water tank 2-1 is drawer type water box, is provided with the conical flask position-limited rack 2-6 for designated water level in the water tank 2-1.Described water tank is outside equipped with for the water tank supporting seat 2-7 that supports water tank.
Among the utility model embodiment, warm field generator 1 adopts 4 independent temperature fields, and the temperature control error is ± 5 ℃, and all the hot body endoporus is Φ 30mm, L≤250mm, and maximum temperature is 700 ℃, and soaking body temperature difference is less than 3 ℃, and rated power is 0.5KW * 4=2KW.Temperature controller adopts intelligent LCD liquid crystal display, and supply voltage is AC220V ± 10%, and program I temperature is 185 ℃～520 ℃, and program II temperature is 300 ℃～600 ℃, and weight is 65kg.As shown in Figure 5, be low-temperature pyrolysis tester dimensional drawing among the utility model embodiment, wherein the model of low-temperature pyrolysis tester is the CDW-Q type.
Adopt 3 pairs of warm field generators 1 of DMSC-1 type temperature-controlled cabinet to carry out temperature control among the utility model embodiment, its internal circuit connects as shown in Figure 6, and the K+ end connects 1 port, and the K-end connects 2 ports, and the KL1 end connects 3 ports, and the KL2 end connects 4 ports.
Among the utility model embodiment, the control of program I temperature is as shown in table 1: program I temperature control curve as shown in Figure 7;
Table 1
Among the utility model embodiment, the control of program II temperature is as shown in table 1: program II temperature control curve as shown in Figure 8;
Table 2
| Temperature range | Heat time heating time | Error | State shows |
| 600℃ | 15min | 5% | Constant temperature was reported to the police in 15 minutes |
| 300～600℃ | 60min | 5% | Temperature programmed control |
| 285～300℃ | 3min | ? | The buzzing prompting |
| 20～285℃ | 35min | ? | Heating with full power |
Multifunctional low-temperature destructive distillation tester carries out destructive distillation as shown in Figure 9, and destructive distillation pipe and the conical flask that installs the resinous shale sample connected, and the destructive distillation pipe is fixed on the destructive distillation frame, aims at equal hot hole and pushes gently, and conical flask is put into water tank; Liquid level is positioned at conical flask 2/3 place, starts air switch 1,2,3,4; Four element loop general supplies are connected; Temperature programmed control is selected I; Press start key and heat up, when making the resinous shale sample, heat up by the heating rate of table 1; Heating rate by table 2 when doing coal sample heats up; Temperature is raised to 520 ℃, and constant temperature was reported to the police in 20 minutes; Press stop key; Close air switch; The destructive distillation pipe is withdrawed from off-test, carries out next step test routine.
Sample is loaded in the destructive distillation pipe, places in the low-temperature pyrolysis stove, under the secluding air condition, with regulation heating schedule heating 520 degree, and keep certain hour, measure gained oil, water, semicoke, destructive distillation accessory substance yield after the destructive distillation.
Claims (4)
1. multifunctional low-temperature destructive distillation tester, comprise temperature-controlled cabinet, it is characterized in that: also comprise warm field generator and destructive distillation condensation gatherer, wherein, the output terminal of temperature field generator connects the input end of temperature-controlled cabinet, described temperature field generator comprises temperature sensor, thermal insulator, heat pipe, a temperature quartzy thermal source, dividing plate before the calandria, the calandria rear bulkhead, bonnet, protecgulum and shell, wherein, the body outer periphery of described heat pipe is equipped with a temperature quartzy thermal source, the outer periphery of a temperature quartzy thermal source is equipped with thermal insulator, the thermal insulator outer periphery is equipped with shell, above-mentioned heat pipe, a temperature quartzy thermal source and thermal insulator constitute the heating main body, be provided with the preceding dividing plate of calandria between described heating body front end and the protecgulum, be provided with the calandria rear bulkhead between heating body rear and the bonnet, and the heating body rear is inserted temperature sensor; Described destructive distillation condensation gatherer comprises water tank, destructive distillation pipe holder, destructive distillation pipe, wireway and conical flask, and described destructive distillation pipe is arranged in the heat pipe of warm field generator, and its destructive distillation mouth passes in the plug insertion conical flask; Described wireway passes plug and inserts in the conical flask; Described destructive distillation pipe is fixed on the water tank by the destructive distillation pipe holder.
2. multifunctional low-temperature destructive distillation tester according to claim 1, it is characterized in that: described temperature field generator is four, and the output terminal of temperature sensor is as the output terminal of warm field generator.
3. multifunctional low-temperature destructive distillation tester according to claim 1, it is characterized in that: described water tank is drawer type water box, is provided with the conical flask position-limited rack for designated water level in the water tank.
4. multifunctional low-temperature destructive distillation tester according to claim 1 is characterized in that: described water tank is outside equipped with for the water tank supporting seat that supports water tank.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201320213170 CN203178224U (en) | 2013-04-24 | 2013-04-24 | Multifunctional low temperature destructive distillation tester |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201320213170 CN203178224U (en) | 2013-04-24 | 2013-04-24 | Multifunctional low temperature destructive distillation tester |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN203178224U true CN203178224U (en) | 2013-09-04 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 201320213170 Expired - Fee Related CN203178224U (en) | 2013-04-24 | 2013-04-24 | Multifunctional low temperature destructive distillation tester |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN203178224U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104914234A (en) * | 2015-07-06 | 2015-09-16 | 中国地质大学（北京） | Shale oil containing structure measuring device and method |
-
2013
- 2013-04-24 CN CN 201320213170 patent/CN203178224U/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104914234A (en) * | 2015-07-06 | 2015-09-16 | 中国地质大学（北京） | Shale oil containing structure measuring device and method |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20130904 |