CN203177686U - Mother liquor heater - Google Patents

Mother liquor heater Download PDF

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Publication number
CN203177686U
CN203177686U CN2013202130104U CN201320213010U CN203177686U CN 203177686 U CN203177686 U CN 203177686U CN 2013202130104 U CN2013202130104 U CN 2013202130104U CN 201320213010 U CN201320213010 U CN 201320213010U CN 203177686 U CN203177686 U CN 203177686U
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CN
China
Prior art keywords
mother liquor
tube
bobbin carriage
cylindrical shell
pipe
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
CN2013202130104U
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Chinese (zh)
Inventor
梁有仪
段有龙
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Acre Coking and Refractory Engineering Consulting Corp MCC
Original Assignee
Acre Coking and Refractory Engineering Consulting Corp MCC
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Acre Coking and Refractory Engineering Consulting Corp MCC filed Critical Acre Coking and Refractory Engineering Consulting Corp MCC
Priority to CN2013202130104U priority Critical patent/CN203177686U/en
Application granted granted Critical
Publication of CN203177686U publication Critical patent/CN203177686U/en
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

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Abstract

The utility model relates to the process field of spray-type saturator methods in the coking industry, in particular to a mother liquor heater, which comprises a tube body, an upper end socket tube box, a lower end socket tube box, a tube plate, a heat exchange pipe, a baffle plate, a pull rod and a pipe spacer, and is characterized in that the tube body is of a vertical structure, the upper end socket tube box is provided with a mother liquor inlet, the lower end socket tube box is provided with a mother liquor outlet, the tube body is respectively provided with a steam inlet, a condensate water outlet, a temperature measurement interface and a pressure measurement interface, a diffusion mouth is arranged on one side of the top portion of the tube body, and the heat exchange pipe is a spiral fluted tube or a transverse fluted tube structure. Compared with the prior art, the mother liquor heater has the beneficial effects that 1 the mother liquor heater enhances heat transfer, and can increases heat transfer performance 2-4 times compared with a light pipe, thereby keeping steady enhanced heat transfer effect; and 2 the pipe plate is made from a stainless steel clad plate, and can effectively prevent mother liquor from being corroded, the mother liquor can select to enter from the upper end or the lower end according to process requirement, and the process change is flexible.

Description

A kind of mother liquor heater
Technical field
The utility model relates to Spray Saturator method technology field in the coking industry, particularly a kind of mother liquor heater.
Background technology
Adopting the Spray Saturator method to produce the sulphur ammonium is the common method that reclaims ammonia in the fine purification technique for coke oven gas flow process.Spray Saturator is that saturator and crystallizer are connected as a single entity, and it makes flow process more simplify.Adopt the mother liquor heater in this flow process, heat by heater from crystallization tank top part mother liquor, the saturator spray is returned in recirculation, so that saturator mother liquor temperature stabilization is in certain limit.Because it is ammonium sulfate liquor has stronger corrosivity, and is serious to equipment corrosion, therefore, very strict to the material requirement of mother liquor heater.
Present heater structure is the light pipe heat exchange structure, and heat exchange efficiency is low, therefore improve heater structure for the heat exchanger efficiency that improves heater to the chemical industry energy-saving and emission-reduction, increase the benefit extremely importantly, also meet the energy-saving and emission-reduction policy of China.
Summary of the invention
The purpose of this utility model provides a kind of mother liquor heater, improves the heater structure augmentation of heat transfer, improves heat exchange efficiency, guarantees the requirement of saturator mother liquor temperature stabilization.
For achieving the above object, the utility model adopts following technical scheme to realize:
A kind of mother liquor heater, comprise cylindrical shell, upper cover bobbin carriage, low head bobbin carriage, tube sheet, heat exchanger tube, deflection plate, pull bar and distance sink tube, described cylindrical shell is vertical structure, the upper cover bobbin carriage is provided with the mother liquor import, the low head bobbin carriage is provided with the mother liquor outlet, be respectively equipped with steam inlet, condensation-water drain, thermometric interface and pressure measurement interface on the cylindrical shell, top one side of cylindrical shell is provided with diffuses mouth, and described heat exchanger tube is spiral fluted tube or cross grooved pipe structure.
Described tube sheet is the stainless steel clad plate structure.
Corresponding mother liquor import department is provided with impingement baffle one on the described upper cover bobbin carriage.
Described steam inlet adopts the flaring joint pipe structure, and corresponding steam inlet place is provided with impingement baffle two.
Compared with prior art, the beneficial effects of the utility model are:
1) adopts spiral fluted tube or cross grooved pipe heat exchange, augmentation of heat transfer mainly is to be determined by the type of flow in the pipe in the pipe, when adopting the spiral fluted tube, it is mobile that the restriction that flows in the nearly wall of helicla flute place makes tube fluid do one-piece auger motion generation local secondary, the body resistance that helicla flute causes, produce reverse barometric gradient and make boundary layer separation, thus augmentation of heat transfer, and heat transfer property can improve 2 ~ 4 times than light pipe; When adopting cross grooved pipe, when tube fluid is flowed through transverse ring, form axial whirlpool near the tube wall, increased the disturbance in boundary layer, make boundary layer separation, be conducive to the transmission of heat, fluid passes through next transverse ring again when whirlpool will disappear, therefore constantly produce eddy current, kept stable augmentation of heat transfer effect.
2) tube sheet adopts stainless steel clad plate, can effectively prevent the corrosion of mother liquor, and mother liquor can be selected to enter from the upper end or enter from the lower end according to technological requirement, and technology changes flexibly.
Description of drawings
Fig. 1 is example structure schematic diagram of the present utility model;
Fig. 2 is the structural representation that the utility model heat exchanger tube adopts the spiral fluted tube;
Fig. 3 is that the utility model heat exchanger tube adopts the cross grooved pipe structural representation.
Among the figure: 1-mother liquor import 2-impingement baffle one 3-upper cover bobbin carriage 4-tube sheet 5-diffuses mouthful 6-steam inlet 7-thermometric interface 8-cylindrical shell 9-mother liquor outlet 10-condensation-water drain 11-pressure measurement interface 12-distance sink tube 13-heat exchanger tube 14-pull bar 15-deflection plate 16-impingement baffle two 17-low head bobbin carriages
The specific embodiment
Below in conjunction with accompanying drawing the specific embodiment of the present utility model is described further:
See Fig. 1, it is the example structure schematic diagram of a kind of mother liquor heater of the utility model, comprise cylindrical shell 8, upper cover bobbin carriage 3, low head bobbin carriage 17, tube sheet 4, heat exchanger tube 13, deflection plate 15, pull bar 14 and distance sink tube 12, cylindrical shell 8 is vertical structure, upper cover bobbin carriage 3 is provided with mother liquor import 1, low head bobbin carriage 17 is provided with mother liquor outlet 9, be respectively equipped with steam inlet 6 on the cylindrical shell 8, condensation-water drain 10, thermometric interface 7 and pressure measurement interface 11, thermometric interface and pressure measurement interface are used for placing sensor to measure shell vapor (steam) temperature and pressure, and cylindrical shell 8 tops are installed and diffused mouth 5.
The material of heat exchanger tube 13 and end socket bobbin carriage 3 adopts S39042, and the form of heat exchanger tube 13 adopts spiral fluted tube or cross grooved pipe.Because the mother liquor of its heating has severe corrosive, require equipment to have stronger antiseptic property, the material of the cylindrical shell 8 of mother liquor heater, deflection plate 15, pull bar 14 and distance sink tube 12 adopts S31603.Tube sheet is the stainless steel clad plate structure.
Corresponding mother liquor import 1 place is provided with impingement baffle 1 and prevents the direct impingement heat transfer pipe 13 of mother liquor and tube sheet 4 on the upper cover bobbin carriage 3.Steam inlet 6 adopts the flaring joint pipe structure, and corresponding steam inlet place is provided with impingement baffle 2 16.
During use, earlier the mother liquor heater mouth of pipe is connected, by diffusing air in mouthful 5 emptying shells, will diffuse mouthful 5 usefulness blind plates then and block, shell feeds steam and comes the interior mother liquor of heating tube layer, heat exchange tube structure as shown in Figures 2 and 3, when mother liquor stream is crossed spiral fluted tube and fluted tube, form local secondary at groove line place and flow and axial whirlpool, increased the disturbance in boundary layer, make boundary layer separation, thereby strengthened heat transfer.
The mother liquor of mother liquor heater can select mother liquor import 1 from the upper cover bobbin carriage 3 to enter or mother liquor outlet 9 from low head bobbin carriage 17 enters according to technological requirement, and when mother liquor was entered by mother liquor outlet 9, the function of mother liquor import 1 changed outlet into.

Claims (4)

1. mother liquor heater, comprise cylindrical shell, upper cover bobbin carriage, low head bobbin carriage, tube sheet, heat exchanger tube, deflection plate, pull bar and distance sink tube, it is characterized in that, described cylindrical shell is vertical structure, the upper cover bobbin carriage is provided with the mother liquor import, and the low head bobbin carriage is provided with the mother liquor outlet, is respectively equipped with steam inlet, condensation-water drain, thermometric interface and pressure measurement interface on the cylindrical shell, top one side of cylindrical shell is provided with diffuses mouth, and described heat exchanger tube is spiral fluted tube or cross grooved pipe structure.
2. a kind of mother liquor heater according to claim 1 is characterized in that, described tube sheet is the stainless steel clad plate structure.
3. a kind of mother liquor heater according to claim 1 is characterized in that, corresponding mother liquor import department is provided with impingement baffle one on the described upper cover bobbin carriage.
4. a kind of mother liquor heater according to claim 1 is characterized in that, described steam inlet adopts the flaring joint pipe structure, and corresponding steam inlet place is provided with impingement baffle two.
CN2013202130104U 2013-04-24 2013-04-24 Mother liquor heater Expired - Lifetime CN203177686U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN2013202130104U CN203177686U (en) 2013-04-24 2013-04-24 Mother liquor heater

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN2013202130104U CN203177686U (en) 2013-04-24 2013-04-24 Mother liquor heater

Publications (1)

Publication Number Publication Date
CN203177686U true CN203177686U (en) 2013-09-04

Family

ID=49074371

Family Applications (1)

Application Number Title Priority Date Filing Date
CN2013202130104U Expired - Lifetime CN203177686U (en) 2013-04-24 2013-04-24 Mother liquor heater

Country Status (1)

Country Link
CN (1) CN203177686U (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105352340A (en) * 2015-12-14 2016-02-24 黄少安 Polycarboxylic acid mother solution condenser

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105352340A (en) * 2015-12-14 2016-02-24 黄少安 Polycarboxylic acid mother solution condenser

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Legal Events

Date Code Title Description
C14 Grant of patent or utility model
GR01 Patent grant
TR01 Transfer of patent right

Effective date of registration: 20180907

Address after: 116085 128 high energy street, Qixian Ling high tech Industrial Park, Dalian, Liaoning

Patentee after: ACRE COKING & REFRACTORY ENGINEERING CONSULTING CORPORATION (DALIAN), MCC

Address before: 116085 128 high energy street, Qixian Ling high tech Industrial Park, Dalian, Liaoning

Patentee before: ACRE COKING & REFRACTORY ENGINEERING CONSULTING CORPORATION, MCC

TR01 Transfer of patent right
CX01 Expiry of patent term

Granted publication date: 20130904

CX01 Expiry of patent term