CN203144221U - Recycling treatment system of villiaumite-containing waste alkali solution - Google Patents

Recycling treatment system of villiaumite-containing waste alkali solution Download PDF

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Publication number
CN203144221U
CN203144221U CN 201320153778 CN201320153778U CN203144221U CN 203144221 U CN203144221 U CN 203144221U CN 201320153778 CN201320153778 CN 201320153778 CN 201320153778 U CN201320153778 U CN 201320153778U CN 203144221 U CN203144221 U CN 203144221U
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CN
China
Prior art keywords
clear liquid
villiaumite
pressure filter
settling bowl
alkali solution
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
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CN 201320153778
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Chinese (zh)
Inventor
李小明
刘静涛
曹勇
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
SICHUAN ZHONGLI FLUORIDATION INDUSTRY Co Ltd
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SICHUAN ZHONGLI FLUORIDATION INDUSTRY Co Ltd
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Priority to CN 201320153778 priority Critical patent/CN203144221U/en
Application granted granted Critical
Publication of CN203144221U publication Critical patent/CN203144221U/en
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Abstract

The utility model discloses a recycling treatment system of a villiaumite-containing waste alkali solution. An infusion pump is used for conveying the villiaumite-containing waste alkali solution into a reaction kettle; an outlet of the reaction kettle is connected with a filter press; liquid at the bottom of the filter press enters a settling basin; filtering dreg at the upper part of the filter press enters a centrifugal machine to obtain a filtering solution which enters the settling basin; clean liquid in the settling basin is placed into a clean liquid storage groove by using a liquid level difference; and the clean liquid in the clean liquid storage groove is conveyed into an alkali solution circulating groove through a clean liquid pump to blend the concentration. Compared with the prior art, the recycling treatment system of the villiaumite-containing waste alkali solution realizes the recycling of the waste alkali solution, so that the pollution to an environment is avoided and also the 60% of the investment of raw materials and funds is saved.

Description

A kind of villiaumite waste lye recycling treatment system that contains
Technical field
The utility model relates to and contains villiaumite waste lye recycling process field, exactly refers to a kind of villiaumite waste lye recycling treatment system that contains.
Background technology
In sulfur hexafluoride, the tetrafluoro-methane industrialized producing technology, in order to remove HF and other the fluorine-containing harmful component in the thick gas, must carry out circulation cleaning by multistage washing tower to thick gas with the alkali lye (KOH solution) of echelon concentration, in tower, alkali lye and fluorine-containing harmful component reaction generate KF and are dissolved in the washing soda solution.F in alkaline solution +It is discarded to lose efficacy when content reaches finite concentration, environment is polluted, and this pollution damage is permanence.
The utility model content
At above-mentioned defective, the technical problem that the utility model solves is to provide a kind of villiaumite waste lye recycling treatment system that contains, and has realized the cycling and reutilization of waste lye, has both avoided environment is polluted, and has saved the starting material fund input again.
In order to solve above technical problem, the utility model provides contains villiaumite waste lye recycling treatment system, comprise infusion pump, reactor, pressure filter, whizzer, settling bowl, clear liquid storage tank and clear liquid transferpump, described infusion pump is connected with described reactor, described reactor is connected with described pressure filter, described pressure filter top is connected with described whizzer, described pressure filter bottom is connected with described settling bowl, described settling bowl is connected with described clear liquid storage tank, described clear liquid storage tank is connected with described clear liquid transferpump, and described whizzer also is connected with described settling bowl; Described infusion pump will contain the villiaumite waste lye and be delivered to described reactor, the outlet of described reactor is connected with described pressure filter, the liquid of described pressure filter bottom enters settling bowl, the filter residue on described pressure filter top enters the filtrate that whizzer obtains and enters settling bowl, clear liquid in the described settling bowl utilizes liquid level difference to put into described clear liquid storage tank, and the clear liquid in the described clear liquid storage tank is transported in the alkali lye circulation groove by described clear liquid transferpump allocates concentration.
Compared with prior art, the utility model provides contains villiaumite waste lye recycling treatment system, has realized the cycling and reutilization of waste lye, has both avoided environment is polluted, and has saved 60% starting material and fund input again.
Description of drawings
Fig. 1 is for containing the structural representation of villiaumite waste lye recycling treatment system among the utility model embodiment, the direction of arrow is the flow direction of material among the figure.
Embodiment
For those skilled in the art can understand technical scheme provided by the utility model better, set forth below in conjunction with specific embodiment.
See also Fig. 1, this figure is the structural representation that contains villiaumite waste lye recycling treatment system among the utility model embodiment, and the direction of arrow is the flow direction of material among the figure.
The utility model provides contains villiaumite waste lye recycling treatment system, comprise infusion pump 1, reactor 2, pressure filter 3, whizzer 4, settling bowl 5, clear liquid storage tank 6 and clear liquid transferpump 7, infusion pump 1 is connected with reactor 2, reactor 2 is connected with pressure filter 3, pressure filter 3 tops are connected with whizzer 4, and pressure filter 3 bottoms are connected with settling bowl 5, and settling bowl 5 is connected with clear liquid storage tank 6, clear liquid storage tank 6 is connected with clear liquid transferpump 7, and whizzer 4 also is connected with settling bowl 5; Infusion pump 1 will contain the villiaumite waste lye and be delivered to reactor 2, the outlet of reactor 2 is connected with pressure filter 3, the liquid of pressure filter 3 bottoms enters settling bowl 5, the filter residue on pressure filter 3 tops enters the filtrate that whizzer 4 obtains and enters settling bowl 5, clear liquid in the settling bowl 5 utilizes liquid level difference to put into clear liquid storage tank 6, and the clear liquid in the clear liquid storage tank 6 is transported in the alkali lye circulation groove by clear liquid transferpump 7 allocates concentration.
The workflow that contains villiaumite waste lye recycling treatment system that the utility model provides is as follows:
1, waste lye is sent in the reactor 2 sampling analysis F with pump 1 +Concentration adds clear Ca (OH) under stirring action 2Emulsion and waste lye reaction,
2KF+Ca(OH) 2=CaF 2+2KOH
Require clear Ca (OH) 2Emulsion is excessive approximately;
2, reaction product is put into pressure filter 3 in batches, under the effect of 0.3Mpa pressure, by filter cloth slag, liquid are effectively separated;
3, the pressure filter bottom liquid is put into settling bowl 5 standing sedimentations by potential difference;
4, pressure filter top filter residue takes out together with filter cloth and puts into whizzer 4, and slag, liquid are further separated, and liquid is put into settling bowl 5 by potential difference, adds flocculation agent, and standing sedimentation dries Gu slag takes out.Gu slag major ingredient: moisture<5%, CaF 2>93%;
5, to put into clear liquid storage tank 6 by potential difference standby for the clear KOH aqueous solution behind settling bowl 5 standing sedimentations;
6, the clear liquids in the clear liquid storage tank 6 are sent into the alkali lye circulation groove with pump 7, use again after regulating concentration on request;
7, the solid slag in whizzer 4, settling bowl 5, the clear liquid storage tank 6 takes out and dries, and can be used as the additive of manufacture of cement.
Compared with prior art, the utility model provides contains villiaumite waste lye recycling treatment system, has realized the cycling and reutilization of waste lye, has both avoided environment is polluted, and has saved 60% starting material and fund input again.
To the above-mentioned explanation of the disclosed embodiments, make this area professional and technical personnel can realize or use the utility model.Multiple modification to these embodiment will be apparent concerning those skilled in the art, and defined General Principle can realize under the situation that does not break away from spirit or scope of the present utility model in other embodiments herein.Therefore, the utility model will can not be restricted to these embodiment shown in this article, but will meet the wideest scope consistent with principle disclosed herein and features of novelty.

Claims (1)

1. one kind contains villiaumite waste lye recycling treatment system, it is characterized in that, comprise infusion pump, reactor, pressure filter, whizzer, settling bowl, clear liquid storage tank and clear liquid transferpump, described infusion pump is connected with described reactor, described reactor is connected with described pressure filter, described pressure filter top is connected with described whizzer, described pressure filter bottom is connected with described settling bowl, described settling bowl is connected with described clear liquid storage tank, described clear liquid storage tank is connected with described clear liquid transferpump, and described whizzer also is connected with described settling bowl; Described infusion pump will contain the villiaumite waste lye and be delivered to described reactor, the outlet of described reactor is connected with described pressure filter, the liquid of described pressure filter bottom enters settling bowl, the filter residue on described pressure filter top enters the filtrate that whizzer obtains and enters settling bowl, clear liquid in the described settling bowl utilizes liquid level difference to put into described clear liquid storage tank, and the clear liquid in the described clear liquid storage tank is transported in the alkali lye circulation groove by described clear liquid transferpump allocates concentration.
CN 201320153778 2013-03-29 2013-03-29 Recycling treatment system of villiaumite-containing waste alkali solution Expired - Lifetime CN203144221U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN 201320153778 CN203144221U (en) 2013-03-29 2013-03-29 Recycling treatment system of villiaumite-containing waste alkali solution

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN 201320153778 CN203144221U (en) 2013-03-29 2013-03-29 Recycling treatment system of villiaumite-containing waste alkali solution

Publications (1)

Publication Number Publication Date
CN203144221U true CN203144221U (en) 2013-08-21

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Application Number Title Priority Date Filing Date
CN 201320153778 Expired - Lifetime CN203144221U (en) 2013-03-29 2013-03-29 Recycling treatment system of villiaumite-containing waste alkali solution

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109160636A (en) * 2018-10-15 2019-01-08 大连东泰产业废弃物处理有限公司 A kind of technique of high-concentration fluorine-contained base extraction and recycling

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109160636A (en) * 2018-10-15 2019-01-08 大连东泰产业废弃物处理有限公司 A kind of technique of high-concentration fluorine-contained base extraction and recycling

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Granted publication date: 20130821