CN203112494U - Device for preparing iodine pentafluoride by reaction between iodine trifluoride and solid iodine at room temperature - Google Patents
Device for preparing iodine pentafluoride by reaction between iodine trifluoride and solid iodine at room temperature Download PDFInfo
- Publication number
- CN203112494U CN203112494U CN 201220746595 CN201220746595U CN203112494U CN 203112494 U CN203112494 U CN 203112494U CN 201220746595 CN201220746595 CN 201220746595 CN 201220746595 U CN201220746595 U CN 201220746595U CN 203112494 U CN203112494 U CN 203112494U
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- Prior art keywords
- iodine
- pentafluoride
- trifluoride
- reaction
- pipe
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- Expired - Fee Related
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- Investigating Or Analyzing Non-Biological Materials By The Use Of Chemical Means (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
The utility model discloses a device for preparing iodine pentafluoride by reaction between iodine trifluoride with solid iodine at room temperature. The device mainly comprises an integrated reactor and an iodine trifluoride inlet pipe, an iodine powder feeding pipe and a tail gas testing pipe are communicated with and mounted on the integrated reactor, the assembly of the integrated ractor, the iodine trifluoride inlet pipe, the iodine powder feeding pipe and the tail gas testing pipe is mounted on a platform the bottom of which is connected with a support shaft, and an eccentric wheel is mounted beside the platform, and all the parts are assembled together. The device is rational in process and simple to operate, and also solves the environmental pollution problem in the production process of iodine pentafluoride.
Description
Technical field
The utility model relates to a kind of synthetic preparation facilities of Chemicals, and particularly a kind of device that adopts chlorine trifluoride and solid iodine at room temperature to carry out the prepared in reaction iodine pentafluoride is suitable for the synthetic preparation of chemical industry iodine pentafluoride.
Background technology
At present, conventional apparatus is that iodine and fluorine gas are reacted in negative-pressure container, the device complex production process, and temperature of reaction instability during reaction can not be produced continuously, and the byproduct discharging is many, the high shortcoming of single product energy consumption.
Summary of the invention
Problem to be solved in the utility model is, overcomes the deficiency of existing apparatus, and a kind of device that adopts chlorine trifluoride and solid iodine at room temperature to carry out the prepared in reaction iodine pentafluoride is provided.This installs, and not only technology is reasonable, and preparation is simple, and has solved problem of environmental pollution in the process of producing iodine pentafluoride.
The device scheme that the utility model adopts is: the reactor that is made into one, be communicated with on it chlorine trifluoride inlet pipe, iodine powder adding pipe and tail gas testing tube are installed, its assembly is installed in it is connected with on the platform of fulcrum down, eccentric wheel is installed in by the platform side, is assembled into one and constitutes.
Reactor is a nickel or stainless steel tube, adds pipe from the iodine powder and puts into the iodine powder.The cover that the iodine powder adds on the pipe lubricates with many chlorine or fluorine chlorine lubricant.Borrow eccentric wheel when fulcrum vibrates when installed platform, water constantly flows through the outside of reactor.Chlorine trifluoride enters reactor with reaction is closed in the iodine efflorescence through the chlorine trifluoride inlet pipe, and vibration is to prevent from constantly generating on the iodine surface iodine pentafluoride tectum, when the liquid sample that takes out from reactor when being colourless, reacts and has just finished.This installs, and not only technology is reasonable, and preparation is simple, and has solved problem of environmental pollution in the process of producing iodine pentafluoride.
The beneficial effects of the utility model are that technology is reasonable, prepares simply, has solved problem of environmental pollution in the process of production iodine pentafluoride.
Description of drawings
Below in conjunction with drawings and Examples the utility model is further specified.
Fig. 1 is structural representation of the present utility model.
Accompanying drawing number is: 1. eccentric wheel, and 2. chlorine trifluoride inlet pipe, 3. the iodine powder adds pipe, 4. tail gas testing tube, 5. platform, 6, reactor, 7, fulcrum.
Embodiment
With reference to Fig. 1, the reactor 6 that is made into one is communicated with on it chlorine trifluoride inlet pipe 2, iodine powder adding pipe 3 and tail gas testing tube 4 is installed, and its assembly is installed in it is connected with on the platform 5 of fulcrum 7 down, eccentric wheel 1 is installed in by platform 5 sides, is assembled into one and constitutes.
Claims (1)
1. device that adopts chlorine trifluoride and solid iodine at room temperature to carry out the prepared in reaction iodine pentafluoride, it is characterized in that: the reactor that is made into one, be communicated with on it chlorine trifluoride inlet pipe, iodine powder adding pipe and tail gas testing tube are installed, its assembly is installed in it to be connected with on the platform of fulcrum down, eccentric wheel is installed in by the platform side, is assembled into one and constitutes.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201220746595 CN203112494U (en) | 2012-12-31 | 2012-12-31 | Device for preparing iodine pentafluoride by reaction between iodine trifluoride and solid iodine at room temperature |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201220746595 CN203112494U (en) | 2012-12-31 | 2012-12-31 | Device for preparing iodine pentafluoride by reaction between iodine trifluoride and solid iodine at room temperature |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN203112494U true CN203112494U (en) | 2013-08-07 |
Family
ID=48892863
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 201220746595 Expired - Fee Related CN203112494U (en) | 2012-12-31 | 2012-12-31 | Device for preparing iodine pentafluoride by reaction between iodine trifluoride and solid iodine at room temperature |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN203112494U (en) |
-
2012
- 2012-12-31 CN CN 201220746595 patent/CN203112494U/en not_active Expired - Fee Related
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20130807 Termination date: 20141231 |
|
| EXPY | Termination of patent right or utility model |