CN203108518U - Alcohol oxidizing reaction device - Google Patents

Alcohol oxidizing reaction device Download PDF

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Publication number
CN203108518U
CN203108518U CN 201220720438 CN201220720438U CN203108518U CN 203108518 U CN203108518 U CN 203108518U CN 201220720438 CN201220720438 CN 201220720438 CN 201220720438 U CN201220720438 U CN 201220720438U CN 203108518 U CN203108518 U CN 203108518U
Authority
CN
China
Prior art keywords
hot water
heat exchanger
oxidation
heat
epimere
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN 201220720438
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Chinese (zh)
Inventor
刘顺祖
郭江雨
薛淑卿
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
ZOUPING SHUNKANG BIOLOGICAL SCIENCE AND TECHNOLOGY Co Ltd
Original Assignee
ZOUPING SHUNKANG BIOLOGICAL SCIENCE AND TECHNOLOGY Co Ltd
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Priority to CN 201220720438 priority Critical patent/CN203108518U/en
Application granted granted Critical
Publication of CN203108518U publication Critical patent/CN203108518U/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

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Abstract

The utility model discloses an alcohol oxidizing reaction device. The device comprises an oxidizing furnace 2 used for alcohol reaction, a hot water heat exchange device, and a filtering flame arrester 1 at a material inlet end, wherein the hot water heat exchange device comprises a hot water tank 3, a hot water pump 4 and a hot pack 5 which are connected in sequence. The alcohol oxidizing reaction device has the beneficial effects that a heating zone of the oxidizing furnace is divided into two stages which are an upper section heat exchanger and a lower section heat exchanger, hot water firstly flows through the lower section heat exchanger in which high temperature is required, water subjected to heat exchange is injected into the hot pack, then the temperature of the water is adjusted in the hot pack to achieve temperature which is required by the upper section heat exchanger, and then the water is injected into the upper section heat exchanger to heat the upper section heat exchanger, so that the hot water is sufficiently utilized, and a large amount of water resource is saved. Moreover, as a filtering device with high safety is additionally arranged at the material inlet end, impurities in alcohol steam can be removed, the frequency of side reaction in the oxidizing furnace is reduced, and the subsequent product quality is guaranteed.

Description

A kind of oxidation of ethanol reaction unit
Technical field
The utility model relates to a kind of production of acetic acid equipment, relates in particular to a kind of oxidation of ethanol reaction unit.
Background technology
In the alimentary acetic acid scale production process, carry out oxidation acetaldehyde processed at the oxidation of ethanol oxidation of ethanol reacting furnace commonly used.Traditional oxidation of ethanol stove mostly is two sections thermals treatment zone, and traditional way is that the water with different water temperatures is passed in the heat exchanger of two sections thermals treatment zone and heats, and the water after the use is directly discharged, and has so just wasted a large amount of heat energy and water.And the alcohol steam of material input directly is passed in the oxidation reaction stove, often has small amount of impurities in the alcohol steam, so just may produce side reaction in oxidation furnace, has a strong impact on the quality of subsequent handling product.
Summary of the invention
The utility model provides a kind of recycling thermal water resource at background technology, using water wisely, and increase the oxidation of ethanol reaction unit of safe filter at the input of alcohol steam.
The utility model is realized by following technical measures: a kind of oxidation of ethanol reaction unit, comprise oxidation furnace, the oxidation furnace upper end is provided with material inlet, is provided with the two sections heat exchanger in the oxidation furnace, and the upper and lower heat exchanger of oxidation furnace connects the hot water heat-exchanger rig that hot water circuit is used successively.
Concrete, the epimere heat exchanger comprises epimere hot water inlet and epimere hot water outlet, the hypomere heat exchanger comprises hypomere hot water inlet and hypomere hot water outlet.
As optimized technical scheme, above-mentioned hot water heat-exchanger rig comprises hot-water cylinder, heat-exchanger pump and the Re Bao that connects successively; Heat-exchanger pump is connected with the hypomere hot water inlet by pipeline, and the hypomere delivery port is connected with Re Bao.
In order to make the heat exchange needs of epimere heat exchanger, further feature of the present utility model has, and above-mentioned epimere hot water inlet is connected the heat bag with the epimere hot water outlet, and heat is wrapped and is provided with discharge outlet; Heat-exchanger pump is connected with Re Bao.
For the purity of the material that guarantees to enter oxidation furnace and the security that improves equipment, further feature of the present utility model has, and above-mentioned material inlet is connected with the filtration spark arrester.
For the output of material and the recycling of raw material, further feature of the present utility model also has, and above-mentioned oxidation furnace bottom is provided with discharging opening, and the oxidation furnace bottom is provided with leakage fluid dram.
The beneficial effects of the utility model are: this oxidation furnace thermal treatment zone is divided for two-stage, be upper and lower section heat exchanger, hot water is earlier through needing the higher hypomere heat exchanger of temperature, water after the heat exchange is injected into Re Baonei, adjust temperature at Re Baonei then and reach the epimere heat exchanger and be passed in the epimere heat exchanger after temperature required it is heated, make hot water obtain sufficient use like this and saved great amount of water resources.And the material input increases safe filter, can remove the impurity that has in the alcohol steam, so just reduces the side reaction in the oxidation furnace, guarantees the quality of subsequent handling product.
Description of drawings
Fig. 1 is the structural representation of the utility model specific embodiment.
Among the figure, 1, filter spark arrester, 2, oxidation furnace, 3, hot-water cylinder, 4, heat-exchanger pump, 5, Re Bao, 6, material inlet, 7, the epimere heat exchanger, 8, the hypomere heat exchanger, 9, epimere hot water outlet, 10, the epimere hot water inlet, 11, the hypomere hot water inlet, 12, hypomere hot water outlet, 13, discharge outlet, 14, discharging opening, 15, leakage fluid dram.
The specific embodiment
For clearly demonstrating the technical characterstic of this programme, below by a specific embodiment, and in conjunction with its accompanying drawing, this programme is set forth.
A kind of oxidation of ethanol reaction unit as shown in Figure 1, this covering device comprises: be used for oxidation furnace 2, the hot water heat-exchanger rig of ethanol synthesis, the filtration spark arrester 1 of material input.Wherein the hot water heat-exchanger rig comprises hot-water cylinder 3, heat-exchanger pump 4 and the Re Bao 5 that connects successively.Wherein the heat bag is the carbon steel drum, is a vapour device, and a certain amount of water of heat bag 5 storages uses for oxidation furnace 2.
Wherein, the structure of oxidation furnace 2 is: its upper end is provided with material inlet 6, is provided with two sections heat exchanger 7,8 in the oxidation furnace 2; Epimere heat exchanger 7 comprises epimere hot water inlet 9 and epimere hot water outlet 10, and hypomere heat exchanger 8 comprises hypomere hot water inlet 11 and hypomere hot water outlet 12.The oxidation furnace bottom is provided with discharging opening 14, and the oxidation furnace bottom is provided with leakage fluid dram 15.
The concrete annexation of each equipment is: the upper and lower heat exchanger 7,8 of oxidation furnace connects the hot water input unit that hot water circuit is used successively.Heat-exchanger pump 4 is connected with hypomere hot water inlet 11 by pipeline, and hypomere delivery port 12 is connected with Re Bao 5.The epimere hot water inlet is connected heat bag 5 with epimere hot water outlet 10,9, heat bag 5 is provided with discharge outlet 13; Heat-exchanger pump 4 is connected with Re Bao 5.Material inlet 6 is connected with and filters spark arrester 1.
The utility model can pass through existing techniques in realizing without the technical characterictic of describing, and does not repeat them here.Certainly; above-mentioned explanation is not to be to restriction of the present utility model; the utility model also is not limited in above-mentioned giving an example, and the variation that those skilled in the art make in essential scope of the present utility model, remodeling, interpolation or replacement also should belong to protection domain of the present utility model.

Claims (6)

1. oxidation of ethanol reaction unit, comprise oxidation furnace (2), it is characterized in that: described oxidation furnace (2) upper end is provided with material inlet (6), be provided with two sections heat exchanger (7,8) in the oxidation furnace (2), the upper and lower heat exchanger of described oxidation furnace (7,8) connects the hot water heat-exchanger rig that hot water circuit is used successively.
2. oxidation of ethanol reaction unit according to claim 1, it is characterized in that: described epimere heat exchanger (7) comprises epimere hot water inlet (9) and epimere hot water outlet (10), and described hypomere heat exchanger (8) comprises hypomere hot water inlet (11) and hypomere hot water outlet (12).
3. oxidation of ethanol reaction unit according to claim 2 is characterized in that: described hot water input unit comprises hot-water cylinder (3), heat-exchanger pump (4) He Rebao (5) that connects successively; Described heat-exchanger pump (4) is connected with hypomere hot water inlet (11) by pipeline, and described hypomere delivery port (12) He Rebao (5) connects.
4. oxidation of ethanol reaction unit according to claim 3 is characterized in that: described epimere hot water inlet is connected heat bag (5) with epimere hot water outlet (10,9), and described heat bag (5) is provided with discharge outlet (13); Described heat-exchanger pump (4) He Rebao (5) connects.
5. oxidation of ethanol reaction unit according to claim 1 is characterized in that: described material inlet (6) is connected with and filters spark arrester (1).
6. oxidation of ethanol reaction unit according to claim 3, it is characterized in that: described oxidation furnace bottom is provided with discharging opening (14), and the oxidation furnace bottom is provided with leakage fluid dram (15).
CN 201220720438 2012-12-25 2012-12-25 Alcohol oxidizing reaction device Expired - Fee Related CN203108518U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN 201220720438 CN203108518U (en) 2012-12-25 2012-12-25 Alcohol oxidizing reaction device

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN 201220720438 CN203108518U (en) 2012-12-25 2012-12-25 Alcohol oxidizing reaction device

Publications (1)

Publication Number Publication Date
CN203108518U true CN203108518U (en) 2013-08-07

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN 201220720438 Expired - Fee Related CN203108518U (en) 2012-12-25 2012-12-25 Alcohol oxidizing reaction device

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CN (1) CN203108518U (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107261530A (en) * 2017-07-05 2017-10-20 临沂市金沂蒙生物科技有限公司 Alcohol circulating and evaporating system in acetaldehyde production

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107261530A (en) * 2017-07-05 2017-10-20 临沂市金沂蒙生物科技有限公司 Alcohol circulating and evaporating system in acetaldehyde production

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Granted publication date: 20130807

Termination date: 20141225

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