CN203021489U - Hydrogen-containing silicone oil reaction storage tank device - Google Patents
Hydrogen-containing silicone oil reaction storage tank device Download PDFInfo
- Publication number
- CN203021489U CN203021489U CN 201220692684 CN201220692684U CN203021489U CN 203021489 U CN203021489 U CN 203021489U CN 201220692684 CN201220692684 CN 201220692684 CN 201220692684 U CN201220692684 U CN 201220692684U CN 203021489 U CN203021489 U CN 203021489U
- Authority
- CN
- China
- Prior art keywords
- storage tank
- silicone oil
- reactor
- reaction kettle
- hydrogen
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
Images
Abstract
The utility model relates to a reaction device for production of hydrogen-containing silicone oil, in particular to a hydrogen-containing silicone oil reaction storage tank device. The hydrogen-containing silicone oil reaction storage tank device comprises a water-removing reaction kettle, a stirring reaction kettle, a storage tank and an oil-removing reaction kettle, and is characterized in that the stirring reaction kettle is connected with the water-removing reaction kettle, the storage tank is connected between the stirring reaction kettle and the oil-removing reaction kettle by a pipeline, the bottom of the storage tank is tapered, and a valve is arranged at the tapered bottom of the storage tank. The reaction device has a simple structure and reasonable design, the storage tank with tapered bottom is arranged between the stirring reaction kettle and the oil-removing reaction kettle, and the valve is arranged at bottom of the tapered storage tank, so that extract liquid at the lower layer can be discharged through the valve after the liquid in the storage tank is layered in a standing manner, the content of the extract liquid in the oil-removing reaction kettle is reduced and the purpose of improving the purity of the hydrogen-containing silicone oil is achieved.
Description
Technical field
The utility model relates to the reaction unit of producing for containing hydrogen silicone oil, especially a kind of containing hydrogen silicone oil reaction tank arrangement.
Background technology
Containing hydrogen silicone oil, under the metal solvent effect, can be crosslinked under proper temperature, form waterproof membrane at various substrate surfaces, be widely used as fabric, fire-fighting medium (dry powder), paper, metal, leather, timber, glass, cement, pottery, marmorean water-resisting agent, paper separant, release agent or inhibitor etc.At present, the technique that the production Methyl Hydrogen Polysiloxane Fluid mainly adopts is: after dimethyl dichlorosilane (DMCS) and dimethylchlorosilane mixing, add in the reactor of the toluene of packing in advance (or dimethylbenzene) and water, reaction is hydrolyzed, tell the sour water layer through the reactor that dewaters after hydrolysis reaction is completed, obtain the oily matter product; The oily matter product is by stirred autoclave and add resin to carry out balanced reaction, and the rear gained mixture of stirring enters de-oiling reactor water and carries out the de-oiling processing, steams solvent, low Buddhist thing under decompression, obtains the thick product of Methyl Hydrogen Polysiloxane Fluid.
But, there is certain shortcoming in above-mentioned production technique: the oily matter product is by stirred autoclave and after adding extraction liquid to stir, the gained mixture enters de-oiling reactor water and carries out the rear low pressure evaporation of de-oiling processing, because contain a certain amount of extraction liquid in mixture, resin more or less can with the containing hydrogen silicone oil evaporation process, cause the purity drop of containing hydrogen silicone oil.
Summary of the invention
For the deficiencies in the prior art, the utility model provides a kind of containing hydrogen silicone oil reaction tank arrangement, removes by tank arrangement is set the resin that adds in stirred autoclave, reduces the impurity in the de-oiling reactor, improves the purity of containing hydrogen silicone oil.
The technical solution of the utility model is: a kind of containing hydrogen silicone oil reaction tank arrangement, comprise the reactor that dewaters, stirred autoclave, storage tank and de-oiling reactor, it is characterized in that: described stirred autoclave is connected with the reactor that dewaters, and is connected with storage tank by pipeline between stirred autoclave and de-oiling reactor.
Described tank bottom is taper, and the conical lower portion of storage tank is equipped with valve.
On the described reactor that dewaters, feed-pipe is installed.
Described stirred autoclave upper end is equipped with the extraction liquid feed-pipe.
On described de-oiling reactor, discharge nozzle is installed.
The beneficial effects of the utility model are: the utility model is simple in structure, reasonable in design, by the storage tank that between stirred autoclave and de-oiling reactor, a bottom to be set be taper, and the bottom of taper storage tank is equipped with valve, liquid in storage tank is emitted by valve through the extraction liquid that is positioned at lower floor after standing demix, reduce the content of extraction liquid in the de-oiling reactor, reach the purpose of the purity that improves containing hydrogen silicone oil.
Description of drawings
Fig. 1 is the structural representation of containing hydrogen silicone oil reaction tank arrangement described in the utility model.
Fig. 2 is the structural representation of containing hydrogen silicone oil reaction tank arrangement embodiment 2 described in the utility model.
In figure, the 1-reactor that dewaters, 2-stirred autoclave, 3-storage tank, 4-de-oiling reactor, 5-feed-pipe, 6-valve, 7-discharge nozzle, 8-extraction liquid feed-pipe, 9-reservoir, 10-oil pump.
Embodiment
Below in conjunction with accompanying drawing, embodiment of the present utility model is described further:
Embodiment 1: as shown in Figure 1, a kind of containing hydrogen silicone oil reaction tank arrangement, comprise the reactor 1 that dewaters, stirred autoclave 2, storage tank 3 and de-oiling reactor 4, dewater reactor 1 upper end is equipped with feed-pipe 5, stirred autoclave 2 is connected with the reactor 1 that dewaters by pipeline, stirred autoclave 2 upper ends are equipped with extraction liquid feed-pipe 8, be connected with storage tank 3 by pipeline between stirred autoclave 2 and de-oiling reactor 4, storage tank 3 bottoms are taper, the conical lower portion of storage tank 3 is equipped with valve 6, and discharge nozzle 7 is installed on de-oiling reactor 4.
Embodiment 2: as shown in Figure 2, conical lower portion valve 6 lower ends of storage tank 3 are equipped with reservoir 9, and reservoir 9 is connected with stirred autoclave 2 by pipeline, further, on reservoir 9 and pipeline that stirred autoclave 2 is connected, oil pump 10 are installed.After the extraction liquid that flows out from storage tank 3 enters reservoir 9, open oil pump 10, make the anti-stirred autoclave 2 that flow to of extraction liquid, realize the recycle of extraction liquid, can effectively reduce production costs.
The utility model is by storage tank 3 that between stirred autoclave 2 and de-oiling reactor 4, a bottom to be set be taper, and the bottom of taper storage tank is equipped with valve, liquid mixture in described storage tank 3 can be emitted by valve 6 through the extraction liquid that is positioned at lower floor after standing demix, reduce the content of extraction liquid in the de-oiling reactor, reach the purpose of the purity that improves containing hydrogen silicone oil.
Above demonstration and described ultimate principle of the present utility model and principal character and advantage of the present utility model.The technician of the industry should understand; the utility model is not restricted to the described embodiments; that describes in above-described embodiment and specification sheets just illustrates principle of the present utility model; under the prerequisite that does not break away from the utility model spirit and scope; the utility model also has various changes and modifications, and these changes and improvements all fall in claimed the utility model scope.The claimed scope of the utility model is defined by appending claims and equivalent thereof.
Claims (5)
1. a containing hydrogen silicone oil reacts tank arrangement, comprise the reactor that dewaters, stirred autoclave, storage tank and de-oiling reactor, it is characterized in that: described stirred autoclave is connected with the reactor that dewaters, and is connected with storage tank by pipeline between stirred autoclave and de-oiling reactor.
2. containing hydrogen silicone oil according to claim 1 reacts tank arrangement, and it is characterized in that: described tank bottom is taper, and the conical lower portion of storage tank is equipped with valve.
3. containing hydrogen silicone oil reaction tank arrangement according to claim 1, is characterized in that: on the described reactor that dewaters, feed-pipe is installed.
4. containing hydrogen silicone oil according to claim 1 reaction tank arrangement is characterized in that: described stirred autoclave upper end is equipped with the extraction liquid feed-pipe.
5. containing hydrogen silicone oil reaction tank arrangement according to claim 1, is characterized in that: on described de-oiling reactor, discharge nozzle is installed.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201220692684 CN203021489U (en) | 2012-12-15 | 2012-12-15 | Hydrogen-containing silicone oil reaction storage tank device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201220692684 CN203021489U (en) | 2012-12-15 | 2012-12-15 | Hydrogen-containing silicone oil reaction storage tank device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN203021489U true CN203021489U (en) | 2013-06-26 |
Family
ID=48645485
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 201220692684 Expired - Lifetime CN203021489U (en) | 2012-12-15 | 2012-12-15 | Hydrogen-containing silicone oil reaction storage tank device |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN203021489U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105237768A (en) * | 2015-11-06 | 2016-01-13 | 东莞市天桉硅胶科技有限公司 | Continuous silicon oil production line |
-
2012
- 2012-12-15 CN CN 201220692684 patent/CN203021489U/en not_active Expired - Lifetime
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105237768A (en) * | 2015-11-06 | 2016-01-13 | 东莞市天桉硅胶科技有限公司 | Continuous silicon oil production line |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN106430789A (en) | Technology for preparing boiler water from process condensate | |
| CN203021489U (en) | Hydrogen-containing silicone oil reaction storage tank device | |
| CN205367788U (en) | Full -automatic efficient jet flow pressure dissolved air vessel | |
| CN202478767U (en) | Vinyl chloride dehydration device | |
| CN209352803U (en) | Dimethyl carbonate recyclable device | |
| CN201454161U (en) | Oil-water separation system | |
| CN203807374U (en) | Production equipment of circulating terpene-phenolic resin | |
| CN107497424A (en) | A kind of graphene-based catalyst of supported palladium and preparation method thereof | |
| CN203393076U (en) | Terminal hydrogen-based polysiloxane production system | |
| CN201543276U (en) | Defoamer of reaction kettle | |
| CN203112793U (en) | Special device for treating acid-base property of methanol in production process of biodiesel fuel | |
| CN203484158U (en) | Speed increasing device for hydrogenation reaction kettle | |
| CN203903970U (en) | Multifunctional material conversion device | |
| CN202055090U (en) | Sewage-free drainage system for paper making | |
| CN201279455Y (en) | Device for replacing hydrogen using steam | |
| CN202832469U (en) | Three-phase separator taking nitrogen as dynamic gas source | |
| CN203803132U (en) | Combined solvent deacidification, dechlorination and deamination equipment | |
| CN202961978U (en) | De-foaming device | |
| CN203212439U (en) | High-pressure sludge reactor | |
| CN211688677U (en) | Oil field produced water treatment facilities | |
| CN201458995U (en) | Device for removing sodium formate from neopentyl glycol in sodium-method production | |
| CN203866226U (en) | Hydrogenization reduction device | |
| CN201404715Y (en) | Gas-liquid separator convenient for guiding liquid | |
| CN202849361U (en) | Hydrogen sulfide treatment device | |
| CN211896863U (en) | Novel water removal of biodiesel preliminary treatment deacidification device |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of utility model: Hydrogen-containing silicone oil reaction storage tank device Effective date of registration: 20160622 Granted publication date: 20130626 Pledgee: China Co. truction Bank Corp Huizhou branch Pledgor: HUIZHOU YOZHO SCIENCE & TECHNOLOGY Co.,Ltd. Registration number: 2016990000522 |
|
| PLDC | Enforcement, change and cancellation of contracts on pledge of patent right or utility model | ||
| CX01 | Expiry of patent term |
Granted publication date: 20130626 |
|
| CX01 | Expiry of patent term |