CN202962887U - Separating device for separating solid particles - Google Patents
Separating device for separating solid particles Download PDFInfo
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- CN202962887U CN202962887U CN 201220586535 CN201220586535U CN202962887U CN 202962887 U CN202962887 U CN 202962887U CN 201220586535 CN201220586535 CN 201220586535 CN 201220586535 U CN201220586535 U CN 201220586535U CN 202962887 U CN202962887 U CN 202962887U
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- separator
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- charging chamber
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Abstract
The utility model relates to a separating device for separating solid particles. The separating device sequentially comprises an air intake regulating valve, a feeding cavity, a separating cavity and a discharge cavity from bottom to top, wherein the feeding cavity comprises an air distributor, and the separating cavity comprises a filtering unit, a vibration gauge and a fluidizing ventilation cone. The separating device for separating solid particles not only can dynamically protect solid particles and avoid material loss in the separation process, but also can realize high-precision separation of solid particles by regulating the bore diameter of the filtering unit. Besides, the separating device removes a filter cake by vibration, and the separating device is simple in structure and easy to operate.
Description
Technical field
The utility model relates to the solid particle separation field, and particularly, the utility model relates to a kind of solid particle separator.
Background technology
Modern chemistry industry, PETROLEUM PROCESSING are industrial, the energy, pharmaceuticals industry and field of environment protection etc. are widely used solid catalyst.Although solid catalyst is after use, certain variation occurs in its form and catalytic activity, and remaining solid catalyst particle is constant in catalytic activity basically.Therefore, not only cost is low but also high efficiency to reclaim the solid catalyst particle that meets the demands from dead catalyst.
Traditional separation method is all generally to use screening.But for the solid of particle size less than 100 microns, in screening process, the phase mutual friction meeting of solid particle causes large solid particle wearing and tearing, for the user who needs large-size particle as the finished product after separating, economy is very poor, and has all the time the small size solid particle to produce in finished product.
Modern crafts adopt fluid bed to separate more, and the fluid bed separating technology can reduce the impact force between solid particle effectively, makes to drop to minimum because the wearing and tearing between particle cause the possibility that particle size diminishes.CN1188532A disclose a kind of from fluidized bed airflow the separation equipment of separate solid particles.But this separation equipment can be because the shape of the stability fluctuation that air flow rate is controlled and variable grain be different and cause the part large-size particle is taken away to this buoyancy in air-flow of particle.The separating effect of this separation equipment is not remarkable.
CN 102500175A discloses a kind of method that fluidized-bed reactor separates finely ground particles, the related fluidized-bed reactor of the method is its expanding reach of reaction, this expanding reach is comprised of filter, valve, access hole, solid powder import, object position detection device, pressometer, temperature meter and tube connector, at the built-in high-temperature resistant filter of reactor, and switch the mode of blowback in conjunction with many groups, form a kind of built-in filtration dust prevention system.Add reverse nitrogen blowing system at the in-core of filter and carry out blowback, in order to the secondary aggregate of trapped small-sized particle, fall into reactor through blowback and again participates in reacting; So circulation can increase certain economic benefit, and circulation in particle, also stoped leaking outside of dust simultaneously, also will greatly dwindle external environment influence, to reach automation mechanized operation and the purpose that reduces manpower.But the filter of this reactor adopts nitrogen blowback mode to make secondary aggregate fall into reactor and again participates in reaction, and cost is higher and secondary aggregate removing effect is not ideal enough.
CN 102101108A discloses a kind of ultrasonic vibration screen, comprise support, be located at screen cloth on support and the ultrasonic wave head that shakes, the ultrasonic wave head that shakes is located at the outside of support, this ultrasonic wave head that shakes has the biography axle that shakes, support is provided with axis hole, the described biography axle that shakes inserts axis hole and makes the end that passes the axle that shakes pass axis hole from the support outside, this biography shake end of axle is connected with vibration ring, and vibration ring is pressed close to the surface of screen cloth.But it is in screening process, and the phase mutual friction meeting of solid particle causes large solid particle wearing and tearing, and the filter cake removal device is not set, and easily causes filter cake to stop up the situation of filter screen.
US Patent No. 4670993 discloses a kind of for the kaolinic method of fluidisation, a kind of fluidized bed plant is wherein disclosed, it can have separator and vibrating device, but wherein said vibrating device is to be connected on the shell of whole device, its role is to whole material is vibrated operation inconvenience.
The utility model content
For the deficiencies in the prior art, the purpose of this utility model is to provide a kind of separator of separate solid particles.Described separator can be with the solid particle high-purity separation.
Described separator comprises air inlet adjustment valve D, charging chamber F, split cavity H and discharging chamber M from bottom to top successively, and wherein, described charging chamber F comprises gas distributor E, and described split cavity H comprises filter element, vibration gauge L and fluidisation ventilation cone G.
Separator described in the utility model can vertically be arranged by air inlet adjustment valve D, charging chamber F, split cavity H, discharging chamber M (for example successively from down to up distribute) obtain; also can adopt other distribution mode (for example horizontal distribution) successively to obtain by air inlet adjustment valve D, charging chamber F, split cavity H, discharging chamber M, all in the scope of the utility model claim protection.
Preferably, described air inlet adjustment valve D is positioned on described charging chamber F bottom inflow pipeline.
Preferably, the gas that described air inlet adjustment valve passes into is inert gas, for example a kind in nitrogen, helium, neon, argon gas, Krypton or xenon or the combination of at least 2 kinds; The flow velocity of described inert gas is determined according to the particle diameter of the solid particle of required separation by one of ordinary skill in the art; When the flow velocity of gas met or exceeded the critical fludization velocity of solid particle, gas passed the bed of material that solid particle is filled from bottom to up, and in the bed of material, particle is up and down and seethes, and has the part particle to be entrained with the bed of material by air-flow.For the solid particle of different-grain diameter, corresponding critical fluidizing gas velocity is different, and the critical gas flow velocity of the less correspondence of particle is just lower.For example: need to allow particle diameter be taken out of split cavity less than the solid particle of 50 microns, we are just by air inlet adjustment valve regulation gas flow so, thereby in the adjusting split cavity, gas flow rate is controlled at 50 microns critical fluidizing gas velocities that solid particle is corresponding, make particle diameter rest on the bed of material or below the bed of material, reach the purpose of separation greater than the solid particle of 50 microns.
Preferably, described gas distributor E is positioned at charging chamber F bottom.
Preferably, described charging chamber F sidewall is provided with feed pipe A.
Preferably, described charging chamber F sidewall is provided with discharging opening B, and be used for discharging that particle diameter is excessive can't be by the particle of filter element.
Preferably, described gas distributor E is porous plate, is particularly preferably expanded metal; Described porous refers to that hole count is at least 3.
Described filter element refers to the unit with net, hole or tubular construction that can play a role in filtering, solid particle that can the high-purity separation different size.
Preferably, described filter element is positioned at split cavity H top, and described vibration gauge L is positioned at described filter element side, and described fluidisation ventilation cone G is positioned at split cavity H bottom.
Preferably, described fluidisation ventilation cone G is conical cavity, as shown in Figure 1; The bed of material that solid particle is filled in inert gas passes charging chamber F from bottom to up, and air velocity is when meeting or exceeding the critical fludization velocity of particle, and in the bed of material, particle seethes up and down, and has the part particle to be entrained with the bed of material by air-flow.When medium upwards flowed in fluidisation ventilation cone, fluidisation ventilation cone internal diameter increased gradually, and velocity of medium will reduce gradually, then by regulating air inlet adjustment valve regulation charge flow rate, controls the process of fluidisation with this.
Preferably, described filter element is comprised of tube sheet K and filter core J, and described tube sheet K is positioned at split cavity H top, and described filter core J is fixed on described tube sheet K vertically downward, and described vibration gauge L is positioned at described tube sheet K side; Described vibration gauge L is used for driving described filter element vibration, to remove filter cake.
Described tube sheet refers to get out onboard the hole with filter core joint coupling, and the mode such as filter core is penetrated to weld or be threaded is fixed, and plays fixedly a kind of accessory of tubulation effect of support.
Preferably, described vibration gauge L is the ultrasonic vibration instrument.
Preferably, described filter core adopts the wedge wire spiral winding structure, as Fig. 3, Fig. 4 and shown in Figure 5.
Preferably, described filter core inside is provided with the metal center pipe.
The filter core of wedge wire winding arrangement, to be formed by the mode spiral winding of the cross section wire that is wedge shape with spring, and fixed by some strip metal central tubes of inside, the gap width between each circle wire and adjacent wire is fixed, and is continuous infundibulate.Gap width between adjacent wire is determined as required by one of ordinary skill in the art.Filter process is exactly to allow medium pass by the filter core outside filtration gap that broadens gradually enter filter core inside, enters the discharging chamber by filter core, is discharged by discharge nozzle C; Can not pass the outer surface of wedge metal winded filtering core than the large particle in filter core outer surface gap, will be trapped within (see figure 4) outside the gap, be deposited to split cavity and discharged by discharging opening B.
Central tube is solid metal pipe, and the effect of central tube is to change filter core inner flow passage size, thereby changes flow velocity, and the small particle diameter solid particle that easier like this handle is carried secretly is brought the discharging chamber into, is difficult in the filter core inside deposition.
Preferably, described discharging chamber M is positioned at above filter element, and its sidewall is provided with discharge nozzle C.
The separator of described separating particles can be used for the different solid catalyst particle of particle separation diameter, with its recycling.Described separator can not cause the phase mutual friction of solid particle, thereby has prevented the wearing and tearing of large particle diameter solid particle, and for the user who needs large-size particle as the finished product after separating, economy is excellent.
Utilize described separator separate solid particles to comprise the following steps:
(1) solid particle is added in charging chamber F;
(2) open air inlet adjustment valve D and pass into inert gas and make the solid particle fluidisation, solid particle enters split cavity (H), is then taken out of the fluidisation bed of material, carries out isolated by filtration, discharges by discharge nozzle C less than the particle of setting size;
(3) after filter core J place's formation filter cake, open vibration gauge L vibration, vibration gauge L drives tube sheet K and filter cake is removed in filter core J vibration;
(4) after isolated by filtration is completed, particle diameter is discharged recycling greater than the solid particle of setting size from discharging opening B.
Preferably, described vibration gauge L is the ultrasonic vibration instrument.
Compared with prior art; the beneficial effects of the utility model comprise: device of the present utility model not only can carry out dynamic protection to solid particle; the wearing and tearing of the large particle diameter solid particle that the phase mutual friction of solid particle causes have been avoided; thereby avoid the loss of material in separation process; and the adjusting along with the filter element aperture; can also obtain the solid particle of different accuracy, namely the High Accuracy Solid particle separation, recycle these solid particle classification and not only save cost but also can increase the benefit.In addition, what described device adopted is that filter cake is removed in vibration, and this apparatus structure is simple, processing ease.
Description of drawings
Fig. 1 is the structural representation of an embodiment of separator described in the utility model.
Fig. 2 is the flow chart of an embodiment of separation method described in the utility model.
Fig. 3 is the filter process schematic diagram of filter core described in the utility model.
Fig. 4 is the filter process schematic diagram of the wedge wire winding arrangement of filter core described in the utility model.
Fig. 5 is the structural representation of filter core described in the utility model.
Fig. 6 is the Electronic Speculum figure of absorbent particles before Application Example screening of the present invention.
Fig. 7 is the Electronic Speculum figure of absorbent particles before Application Example screening of the present invention.
Fig. 8 is the Electronic Speculum figure of absorbent particles after Application Example screening of the present invention.
Fig. 9 is the Electronic Speculum figure of absorbent particles after Application Example screening of the present invention.
Reference numeral is as follows:
A-feed pipe; B-discharging opening; C-discharge nozzle;
D-air inlet adjustment valve; E-gas distributor; F-charging chamber;
G-fluidisation ventilation cone; H-split cavity; I-separator housing;
J-filter core; K-tube sheet; L-vibration gauge;
M-discharging chamber; 1-metal center pipe; 2-wedge wire winded filtering core.
The specific embodiment
For ease of understanding the utility model, it is as follows that the utility model is enumerated embodiment.Those skilled in the art should understand, described embodiment helps to understand the utility model, should not be considered as concrete restriction of the present utility model.
Separator that the present embodiment adopts comprises air inlet adjustment valve D, charging chamber F, split cavity H and discharging chamber M from bottom to top successively; Wherein, described charging chamber F comprises gas distributor E, and described gas distributor E is expanded metal, is positioned at charging chamber F bottom, and described charging chamber F sidewall is provided with feed pipe A and discharging opening B; Described air inlet adjustment valve D is positioned on described charging chamber F bottom inflow pipeline; Described split cavity H comprises tube sheet K, filter core J, vibration gauge L and fluidisation ventilation cone G, described tube sheet K is positioned at split cavity H top, described filter core J adopts the wedge wire spiral winding structure, and be provided with metal center pipe (as Fig. 3, Fig. 4 and shown in Figure 5) in inside, be fixed in vertically downward on described tube sheet K, described vibration gauge L is the ultrasonic vibration instrument, is positioned at described tube sheet K side, and described fluidisation ventilation cone G is positioned at split cavity H bottom; Discharging chamber M is positioned at tube sheet K top, and its sidewall is provided with discharge nozzle C.
Solid catalyst goes out feed pipe A and enters in charging chamber F from described, open bottom inflow control valve D, pass into nitrogen, and adjusting air inflow quantity progressively, until inflow-rate of water turbine, fluidizing gas scatter uniformly by gas distributor E, and the solid catalyst particle in the charging chamber F that packs into is carried out the continuous circulation blowback.The relative gas speed of the fluidized gas that air inlet adjustment valve D controls is greater than the critical fludization velocity of the solid catalyst particle of 20 ~ 100 microns.
To be gap width be provided with the metal center pipe less than wedge wire spiral winding structure and the inside of 40 microns to described filter core J.Carry out the continuous circulation blowback in split cavity when described fluidizing gas, pass the filter core J with wedge wire structure less than the catalyst granules of 40 microns and enter discharging chamber M, and discharge by discharge nozzle C, and be blocked in outside filter core J greater than the catalyst granules of 40 microns.
After running a period of time, the filter core J-shaped becomes filter cake, shuts air inlet adjustment valve D, opens ultrasonic vibration instrument L when separator, vibrates the filter core J dither that drives tube sheet K and be fixed on tube sheet K below, cleaning filter cake by ultrasonic vibration instrument L.
After isolated by filtration is completed, particle diameter is discharged recycling by discharging opening B greater than the catalyst granules of 40 microns.
Separator that the present embodiment adopts comprises air inlet adjustment valve D, charging chamber F, split cavity H and discharging chamber M from bottom to top successively; Wherein, described charging chamber F comprises gas distributor E, and described gas distributor E is expanded metal, is positioned at charging chamber F bottom, and described charging chamber F sidewall is provided with feed pipe A and discharging opening B; Described air inlet adjustment valve D is positioned on described charging chamber F bottom inflow pipeline; Described split cavity H comprises filter screen, vibration gauge L and fluidisation ventilation cone G, and described filter screen is positioned at split cavity H top, and described vibration gauge L is the mechanical oscillation instrument, is positioned at described filter cloth side, and described fluidisation ventilation cone G is positioned at split cavity H bottom; Discharging chamber M is positioned at above filter screen, and its sidewall is provided with discharge nozzle C.
Solid catalyst goes out feed pipe A and enters in charging chamber F from described, open bottom inflow control valve D, pass into nitrogen, and adjusting air inflow quantity progressively, until inflow-rate of water turbine, fluidizing gas scatter uniformly by gas distributor E, and the solid catalyst particle in the charging chamber F that packs into is carried out the continuous circulation blowback.The relative gas speed of the fluidized gas that air inlet adjustment valve D controls is greater than the critical fludization velocity of the solid catalyst particle of 20 ~ 100 microns.
Described aperture of filter screen is less than 60 microns.Carry out the continuous circulation blowback when described fluidizing gas in split cavity, pass filter screen less than the catalyst granules of 60 microns and enter discharging chamber M, and discharge by discharge nozzle C, and be blocked in outside filter screen greater than the catalyst granules of 60 microns.
After running a period of time, form filter cake when separator on filter screen, shut air inlet adjustment valve D, open vibration gauge L, by vibration gauge L shuttle belt electric filter dither, the cleaning filter cake.
After isolated by filtration is completed, particle diameter is discharged recycling by discharging opening B greater than the catalyst granules of 60 microns.
Application Example
Use the described device of embodiment 1, certain petro-chemical corporation's product oil adsorpting desulfurization device adsorbent (solid particle) is sieved, screening precision is 40 μ m, adopts laser particle analyzer before and after screening, adsorbent is carried out grain size analysis, and use electron microscopic observation.
Before screening, results of grain size analysis is as shown in table 1, and the Electronic Speculum result as shown in Figure 6 and Figure 7.
Table 1
After screening, results of grain size analysis is as shown in table 2, Electronic Speculum result such as Fig. 8 and shown in Figure 9.
Table 2
| Granularity μ m | 0.1 | 0.5 | 1 | 3 | 5 | 6 | 7 | 8 | 9 | 10 |
| The not enough % of volume | 0 | 0 | 0 | 0 | 0 | 0 | 0 | 0 | 0 | 0 |
| Granularity μ m | 12 | 14 | 16 | 18 | 20 | 25 | 30 | 35 | 40 | 45.8 |
| The not enough % of volume | 0 | 0 | 0 | 0 | 0 | 0 | 0 | 0 | 0.44 | 2.22 |
| Granularity μ m | 53.1 | 61.6 | 71.4 | 80 | 95.9 | 105 | 111 | 129 | 149 | 173 |
| The not enough % of volume | 6.86 | 15.32 | 27.67 | 39.28 | 59.19 | 68.67 | 74.02 | 86.08 | 93.83 | 98.18 |
| Granularity μ m | 201 | 233 | 270 | 312 | 362 | 420 | 487 | 564 | 600 | ? |
| The not enough % of volume | 99.94 | 100 | 100 | 100 | 100 | 100 | 100 | 100 | 100 | ? |
The filter core precision that this experimental provision is installed is 40 μ m, can see that by grain size analysis before screening the adsorbent of particle diameter below 40 μ m accounts for 40.51% of cumulative volume, and after screening, particle diameter accounts for cumulative volume less than 0.44% below 40 μ m.Electronic Speculum also can be observed the variation of the shared volume ratio of screening front and back different-grain diameter, and separating effect is comparatively remarkable.That is, device of the present invention can be with the solid particle high-purity separation.
Applicant's statement, the utility model illustrates detailed process equipment and process flow process of the present utility model by above-described embodiment, but the utility model is not limited to above-mentioned detailed process equipment and process flow process, does not mean that namely the utility model must rely on above-mentioned detailed process equipment and process flow process and could implement.The person of ordinary skill in the field should understand; to any improvement of the present utility model; to the interpolation of the equivalence replacement of each raw material of the utility model product and auxiliary element, the selection of concrete mode etc., within all dropping on protection domain of the present utility model and open scope.
Claims (10)
1. the separator of a separate solid particles, it comprises air inlet adjustment valve (D), charging chamber (F), split cavity (H) and discharging chamber (M) from bottom to top successively, wherein, described charging chamber (F) comprises gas distributor (E), and described split cavity (H) comprises filter element, vibration gauge (L) and fluidisation ventilation cone (G).
2. separator as claimed in claim 1, is characterized in that, described air inlet adjustment valve (D) is positioned on described charging chamber (F) bottom inflow pipeline.
3. separator as claimed in claim 1, is characterized in that, described gas distributor (E) is positioned at bottom charging chamber (F).
4. separator as claimed in claim 1, is characterized in that, described charging chamber (F) sidewall is provided with feed pipe (A) and discharging opening (B).
5. separator as claimed in claim 1, is characterized in that, described filter element is positioned at split cavity (H) top, and described vibration gauge (L) is positioned at described filter element side, and described fluidisation ventilation cone (G) is positioned at split cavity (H) bottom.
6. separator as claimed in claim 1, it is characterized in that, described filter element is comprised of tube sheet (K) and filter core (J), described tube sheet (K) is positioned at split cavity (H) top, described filter core (J) is fixed on described tube sheet (K) vertically downward, and described vibration gauge (L) is positioned at described tube sheet (K) side.
7. as claim 1, the 5 or 6 described separators of any one, it is characterized in that, described vibration gauge (L) is the ultrasonic vibration instrument.
8. separator as claimed in claim 6, is characterized in that, described filter core (J) adopts the wedge wire spiral winding structure.
9. separator as described in claim 6 or 8, is characterized in that, described filter core (J) inside is provided with the metal center pipe.
10. separator as claimed in claim 1, is characterized in that, described discharging chamber (M) is positioned at above filter element, and its sidewall is provided with discharge nozzle (C).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201220586535 CN202962887U (en) | 2012-11-08 | 2012-11-08 | Separating device for separating solid particles |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201220586535 CN202962887U (en) | 2012-11-08 | 2012-11-08 | Separating device for separating solid particles |
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| CN202962887U true CN202962887U (en) | 2013-06-05 |
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| CN 201220586535 Expired - Lifetime CN202962887U (en) | 2012-11-08 | 2012-11-08 | Separating device for separating solid particles |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102935428A (en) * | 2012-11-08 | 2013-02-20 | 品孚罗特过滤设备（北京）有限公司 | Device for separating solid particles and application thereof |
| CN103585818A (en) * | 2013-11-26 | 2014-02-19 | 博恩（南通）石化设备有限公司 | Three-stage amine liquid recovery device |
-
2012
- 2012-11-08 CN CN 201220586535 patent/CN202962887U/en not_active Expired - Lifetime
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102935428A (en) * | 2012-11-08 | 2013-02-20 | 品孚罗特过滤设备（北京）有限公司 | Device for separating solid particles and application thereof |
| CN102935428B (en) * | 2012-11-08 | 2016-01-20 | 品孚罗特过滤设备（北京）有限公司 | A kind of separator of separate solid particles and application thereof |
| CN103585818A (en) * | 2013-11-26 | 2014-02-19 | 博恩（南通）石化设备有限公司 | Three-stage amine liquid recovery device |
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Granted publication date: 20130605 |