CN202903686U - Automatic distillation drop laser detection and quantitative separation device - Google Patents
Automatic distillation drop laser detection and quantitative separation device Download PDFInfo
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- CN202903686U CN202903686U CN 201220521229 CN201220521229U CN202903686U CN 202903686 U CN202903686 U CN 202903686U CN 201220521229 CN201220521229 CN 201220521229 CN 201220521229 U CN201220521229 U CN 201220521229U CN 202903686 U CN202903686 U CN 202903686U
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- laser detection
- distillation
- temperature sensor
- collecting bottle
- separation device
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Abstract
The utility model relates to the field of detection and analysis of contents of coal tar components and in particular relates to an automatic distillation drop laser detection and quantitative separation device. The device comprises a distillation flask, a condensation pipe, a condensation sleeve, a lifting bracket, a fractionating column, liquid collection flasks and a heating furnace. The device is characterized in that a laser detection device is arranged between the outlet of the condensation pipe and the inlet of the liquid collection flasks; a temperature sensor is arranged at the joint of the fractionating column and the condensation pipe; the laser detection device and the temperature sensor are respectively connected with an embedded computer control system; and the liquid collection flasks are supported on an electronic balance by a rotary bracket. Compared with the prior art, the device has the beneficial effects that (1) for counting the drop density, the device has high precision and stable data, good repeatability and high work efficiency; (2) the device achieves automatic analysis and automatic and flexible grouping in the distillation drop analysis process and achieves intelligentization of the distillation process; and (3) the device effectively eliminates manual measuring errors, reduces the labor intensity, avoids the harms of toxic chemical substances to body health and ensures environmental safety.
Description
Technical field
The utility model relates to component content of coal tar and detects analysis field, and particularly a kind of automatically heating up in a steamer dripped laser detection Quantitative Separation device.
Background technology
Containing in the coal tar has thousands of kinds of chemical substances, the light oil that wherein is commonly used to detect, carbolic oil, five kinds of chemical substances such as oil, washing oil, carbolineum how, and each distillates material has different vapo(u)rizing temperatures corresponding.At present do Measurement of distilled process with the artificial way of distillation, need experience accumulation for a long time, just can accomplish a certain medium Measurement of distilled process is wherein precisely controlled, such as the Measurement of distilled process rule of the multiple coking material of GPRS, the time cost that operating personnel pay is well imagined.
Because Traditional Man distillation pick-up unit is the drippage variable density by the method record distillation drop of artificial visual inspection and manual time-keeping.Pass through again the manual calculations data by artificial adjustment distillation speed, the distillation analysis process is rested in foozle worker's operation.
Summary of the invention
The purpose of this utility model provides a kind of automatically heating up in a steamer and drips laser detection Quantitative Separation device, utilize laser detector and Embedded computer system system, the distillation drop is detected automatically, five kinds of coking materials shared ratio in coal tar commonly used is carried out the automatically quantitative analysis detection and separated the accuracy rate of raising data analysis.
For solving the problems of the technologies described above, the technical solution of the utility model is:
A kind of automatically heating up in a steamer dripped laser detection Quantitative Separation device, comprise cucurbit, condenser pipe, condenser jacket, shears, still, liquid-collecting bottle and heating furnace, between condenser pipe outlet and liquid-collecting bottle entrance, be provided with laser detector, temperature sensor is positioned at the junction of still and condenser pipe, laser detector, temperature sensor are connected with the Embedded computer system system respectively, and rotary bracket holding liquid-collecting bottle is positioned on the electronic balance.
Described liquid-collecting bottle is arranged around even circumferential on rotary bracket, and described liquid-collecting bottle is no less than 5.
Compared with prior art, the beneficial effects of the utility model are: 1) laser detector heats up in a steamer at component content of coal tar and drips in the analytic process the counting of drop density, and precision is high, data stabilization, good reproducibility, high efficiency.2) the Embedded computer system system can be used to furnace temp is controlled in real time, so that distillation speed is regulated in the set quota scope automatically, realizes that component content of coal tar heats up in a steamer automatic analysis and the grouping of dripping in the analytic process, and still-process is intelligent.3) effectively eliminated the error that manual test link produces, reduced labour intensity, the harm of having avoided poisonous chemical confrontation health of human body to cause guarantees Environmental security.
Description of drawings
Fig. 1 is the utility model example structure schematic diagram.
Among the figure: the 1-laser detector 2-Embedded computer system 3-of system liquid-collecting bottle 4-cucurbit 5-heating radiator 6-condenser jacket 7-heating furnace 8-electronic balance 9-constant temperature cover 10-still 11-temperature sensor 12-shears 13-rotary bracket 14-condenser pipe
Embodiment
Below in conjunction with accompanying drawing embodiment of the present utility model is described further:
See Fig. 1, that a kind of automatically heating up in a steamer of the utility model dripped laser detection Quantitative Separation device example structure schematic diagram, by cucurbit 4, liquid-collecting bottle 3, heating furnace 7, condenser pipe 14, heating radiator 5, electronic balance 8, constant temperature cover 9, still 10, temperature sensor 11, shears 12, heating up in a steamer that rotary bracket 13 forms dripped in the automatic detection analysis system, the condenser jacket 6 of condenser pipe 14 peripheries links to each other with water inlet with the water delivering orifice of heating radiator 5 respectively with high point at low spot and consists of the cooling loop, laser detector 1 is arranged between condenser pipe 14 outlets and liquid-collecting bottle 3 entrances, temperature sensor 11 is positioned at the junction of still 10 and condenser pipe 14, laser detector 1, temperature sensor 11 is connected with Embedded computer system system 2 respectively, and rotary bracket 13 holding liquid-collecting bottles 3 are positioned on the electronic balance 8.Laser detector 1 is made for resistant to elevated temperatures quartz glass fibre light-guide material, and its stable operation environment temperature is not less than 300 ℃.
Adopt laser detection and Embedded computer system technology in component content of coal tar analysis mensuration process, droplet number density of distillate within the unit interval be Detection and adjustment automatically, precision is high, data stabilization, when drop density is evacuated, heating furnace 7 heats up, when drop density is intensive, and heating furnace 7 coolings, by the real-time control to vapo(u)rizing temperature, so that distillation speed is regulated in the set quota scope automatically.
In addition, the valid analysing range of temperature sensor 11 is 50～600 ℃, under the control of Embedded computer system system 2, to light oil, carbolic oil, how oil, washing oil, carbolineum vapo(u)rizing temperature section detect in real time by temperature sensor 11.Liquid-collecting bottle 3 is arranged around even circumferential on rotary bracket, the component kind of each temperature section in the corresponding experiment, and liquid-collecting bottle is no less than 5.When vapo(u)rizing temperature arrives 80～180 ℃ of light oil separation temperature sections, rotary bracket 13, system places a liquid-collecting bottle with the distillate of this temperature section automatically, and quantity of distillate is carried out weighing.By that analogy, quantity of distillate with 180～210 ℃, 210～230 ℃, 230～270 ℃, 270～360 ℃ institute's corresponding temperature sections carries out weighing calculating respectively, form data report, the distillate of each temperature section is put into respectively different liquid-collecting bottles, thereby, realize the quantitative automatic analysis in the component content of coal tar analysis mensuration process, and by the component grouping.
Claims (2)
1. one kind is heated up in a steamer a laser detection Quantitative Separation device automatically, comprise cucurbit, condenser pipe, condenser jacket, shears, still, liquid-collecting bottle and heating furnace, it is characterized in that, between condenser pipe outlet and liquid-collecting bottle entrance, be provided with laser detector, temperature sensor is positioned at the junction of still and condenser pipe, laser detector, temperature sensor are connected with the Embedded computer system system respectively, and rotary bracket holding liquid-collecting bottle is positioned on the electronic balance.
2. a kind of automatically heating up in a steamer according to claim 1 dripped laser detection Quantitative Separation device, it is characterized in that, described liquid-collecting bottle is arranged around even circumferential on rotary bracket, and described liquid-collecting bottle is no less than 5.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201220521229 CN202903686U (en) | 2012-10-12 | 2012-10-12 | Automatic distillation drop laser detection and quantitative separation device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201220521229 CN202903686U (en) | 2012-10-12 | 2012-10-12 | Automatic distillation drop laser detection and quantitative separation device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN202903686U true CN202903686U (en) | 2013-04-24 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 201220521229 Expired - Fee Related CN202903686U (en) | 2012-10-12 | 2012-10-12 | Automatic distillation drop laser detection and quantitative separation device |
Country Status (1)
| Country | Link |
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| CN (1) | CN202903686U (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103983657A (en) * | 2014-05-26 | 2014-08-13 | 江苏鑫露新材料股份有限公司 | Quenching oil cooling-rate attenuation rapid simulation device and simulation method |
| CN104020070A (en) * | 2014-04-29 | 2014-09-03 | 辽宁万泓激光科技股份有限公司 | Coal tar ingredient analysis instrument |
| CN115825402A (en) * | 2023-02-23 | 2023-03-21 | 东营胜瑞石油科技有限公司 | Oil shale oil saturation detection device and use method thereof |
-
2012
- 2012-10-12 CN CN 201220521229 patent/CN202903686U/en not_active Expired - Fee Related
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104020070A (en) * | 2014-04-29 | 2014-09-03 | 辽宁万泓激光科技股份有限公司 | Coal tar ingredient analysis instrument |
| CN103983657A (en) * | 2014-05-26 | 2014-08-13 | 江苏鑫露新材料股份有限公司 | Quenching oil cooling-rate attenuation rapid simulation device and simulation method |
| CN103983657B (en) * | 2014-05-26 | 2016-03-30 | 江苏鑫露新材料股份有限公司 | A kind of quenching oil cooling rate decline rapid simulation method |
| CN115825402A (en) * | 2023-02-23 | 2023-03-21 | 东营胜瑞石油科技有限公司 | Oil shale oil saturation detection device and use method thereof |
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Legal Events
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| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20130424 Termination date: 20181012 |
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| CF01 | Termination of patent right due to non-payment of annual fee |