CN202844920U - Dispersing equipment for nanometer materials - Google Patents

Dispersing equipment for nanometer materials Download PDF

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Publication number
CN202844920U
CN202844920U CN 201220259661 CN201220259661U CN202844920U CN 202844920 U CN202844920 U CN 202844920U CN 201220259661 CN201220259661 CN 201220259661 CN 201220259661 U CN201220259661 U CN 201220259661U CN 202844920 U CN202844920 U CN 202844920U
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CN
China
Prior art keywords
nanometer
sand mill
baiting valve
dispersing apparatus
nano material
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
CN 201220259661
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Chinese (zh)
Inventor
邓惠山
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Shanghai Burning Day New Mstar Technology Ltd
Original Assignee
SHANGHAI JORLE FINE CHEM CO Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by SHANGHAI JORLE FINE CHEM CO Ltd filed Critical SHANGHAI JORLE FINE CHEM CO Ltd
Priority to CN 201220259661 priority Critical patent/CN202844920U/en
Application granted granted Critical
Publication of CN202844920U publication Critical patent/CN202844920U/en
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

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Abstract

The utility model provides dispersing equipment for nanometer materials. The dispersing equipment comprises a dispersion machine, a filter pump, a nanometer sand mill, a first discharge valve, a second discharge valve, a third discharge valve and a material pipeline, wherein the dispersion machine comprises an emulsifying device, a stirring device and a kettle body; the dispersion machine is connected with the filter pump by the material pipeline and the first discharge valve; the filter pump is connected with the nanometer sand mill by the material pipeline and the second discharge valve; and the nanometer sand mill is connected with the dispersion machine by the material pipeline and the third discharge valve. According to the dispersing equipment for the nanometer materials, the nanometer materials can be initially dispersed in resin to reach micron grade under the effect of high shearing force of the common dispersion machine, and then the materials are circularly milled through the common nanometer sand mill so as to reach the nanometer grade; the dispersing equipment for the nanometer materials is high in efficiency and good in effect; and furthermore, the median particle diameter is reduced to reach the one-hundred-nanometer grade, and thus the inherent characteristics of the nanometer materials can be fully realized, and various performance indexes of a nanometer material product such as the mechanical strength can be greatly improved when the dispersing equipment is used.

Description

A kind of nano material dispersing apparatus
Technical field
The utility model relates to the nano material treatment facility, particularly relates to a kind of nano material dispersing apparatus.
Background technology
The dispersion of nano material in epoxy resin is very difficult, does not have at present good equipment with it dispersion, and general common high-speed dispersion equipment dispersing nanometer material meta particle diameter is generally the thinnest can only to reach tens microns.
Because the surface energy of nano material is very large, the shearing force of common dispersing apparatus is difficult to it is dispersed in the resin, often will prolong process time and causes the specific energy consumption of product to increase so will reach certain dispersion effect, does not reach desirable effect toward contact.
The utility model content
Based on this, be necessary for the problems referred to above, a kind of nano material dispersing apparatus is provided.
A kind of nano material dispersing apparatus, comprise dispersion machine, described dispersion machine comprises emulsifier unit, agitating device and is used for putting the kettle that holds meter material, it is characterized in that, also comprise filter pump, nanometer sand mill, the first baiting valve, the second baiting valve, the 3rd baiting valve and material pipeline, described dispersion machine is connected with filter pump by material pipeline and the first baiting valve, described filter pump is connected with nanometer sand mill by material pipeline and the second baiting valve, and described nanometer sand mill is connected with dispersion machine by material pipeline and the 3rd baiting valve.
Among embodiment, described emulsifier unit is connected by the single mechanical end face seal part with kettle therein.
Among embodiment, described agitating device is connected by packing seal element with kettle therein.
Among embodiment, described kettle and nanometer sand mill all are arranged with heating jacket outward, are perfused with conduction oil in the heating jacket therein, and this heating jacket is provided with the conduction oil gateway.
Among embodiment, described filter pump is the bag filter with membrane pump therein.
Among embodiment, the filter of described filter is the thick corrosion resistant plate of 5mm therein, and its filter bores is less than 30 microns.
Among embodiment, the inner chamber of described nanometer sand mill and rotating dog rod are zirconia ceramics inner chamber and zirconia ceramics rotating dog rod therein.
Among embodiment, described the first baiting valve, the second baiting valve and the 3rd baiting valve are stainless valve therein.
Among embodiment, described material pipeline peripheral hardware has insulation jacket therein.
Among embodiment, described material pipeline is stainless-steel pipe therein.
Above-mentioned nano material dispersing apparatus, utilize the powerful shearing force of common dispersion machine to realize that nano material tentatively is dispersed to micron order in resin, and then by common nanometer sand mill circular grinding material, material further being ground to Nano grade, efficient is high, effective; And the meta particle diameter is reduced to the rank of 100 nanometers, can give full play to the intrinsic characteristic of nano material, has significantly improved the various performance indications such as mechanical strength when the nano material product uses.
Description of drawings
Fig. 1 is structural representation of the present utility model.
The specific embodiment
As shown in Figure 1, a kind of nano material dispersing apparatus, comprise dispersion machine 1, filter pump 2, nanometer sand mill 3, the first baiting valve 4, the second baiting valve 5, the 3rd baiting valve 6 and material pipeline 7, described dispersion machine 1 comprises emulsifier unit 100, agitating device 101 and be used for putting the kettle 102 that holds meter material, described dispersion machine 1 is connected with filter pump 2 by material pipeline 7 and the first baiting valve 4, described filter pump 2 is connected with nanometer sand mill 3 by material pipeline 7 and the second baiting valve 5, and described nanometer sand mill 3 is connected with dispersion machine 1 by material pipeline 7 and the 3rd baiting valve 6.Utilize the powerful shearing force of common dispersion machine to realize that nano material tentatively is dispersed to micron order in resin, and then by common nanometer sand mill circular grinding material, material further is ground to Nano grade.
Among embodiment, described emulsifier unit 100 is connected by single mechanical end face seal part 8 with kettle 102, has guaranteed good air-tightness therein, can certainly connect by other sealing means, as long as can guarantee good air-tightness.
Therein among embodiment, described agitating device 101 and kettle 102 are connected by packing seal element, have guaranteed good sealing.
Among embodiment, described kettle 102 and the nanometer sand mill 3 outer heating jackets that all are arranged with are perfused with conduction oil in the heating jacket therein, and this heating jacket is provided with the conduction oil gateway, is convenient to heat.
Among embodiment, described filter pump 2 is the bag filter with membrane pump therein.
Among embodiment, the filter of described filter is the thick corrosion resistant plate of 5mm therein, and its filter bores is less than 30 microns, but the elimination bulky grain allows the material that meets the requirement of nanometer sand mill processing particle diameter enter sand mill.
Among embodiment, the inner chamber of described nanometer sand mill 3 and rotating dog rod 301 be that zirconia ceramics inner chamber and zirconia ceramics rotating dog are excellent therein, and wearability is better than metal material greatly, can not bring metal material into material.
Among embodiment, described the first baiting valve 4, the second baiting valve 5 and the 3rd baiting valve 6 are stainless valve therein.
Therein among embodiment, the described material pipeline 7 outer insulation jacket that are provided with.
Among embodiment, described material pipeline 7 is stainless-steel pipe therein.
The specific works flow process of present embodiment is as follows:
At first, resin and nano-powder are dropped in the kettle of common dispersion machine 1, the High Rotation Speed to the 100-130 degree of heating, the rotor outer end produces at least above linear velocity of 15m/s, the highest can be to 40m/s, and form strong machinery and fluid power shearing, liquid layer friction, bump is torn, and makes fully dispersion of aggregates of nanoparticles, emulsification, homogeneous, fragmentation, realizes that the micron order of nano material in resin disperses.
Then, open the first bleeder valve 4 material delivered to nanometer sand mill 3 by filter pump 2, material in the nanometer sand mill cavity with the abrasive material (zirconium oxide bead) of high-energy-density bump, fined grinding.
Afterwards, material flows into dispersion machine 1 by material pipeline 7 and the 3rd baiting valve 6.
Through above-mentioned repeatedly circulation, realize that finally the nanoscale of nano material in resin disperses.Low viscosity is to ensure homodisperse second key of nano material in addition, and the general viscosity of resin is very large, for the viscosity that viscosity is dropped to suitable emulsifying agent dispersion must be heated resin.
The above embodiment has only expressed several embodiment of the present utility model, and it describes comparatively concrete and detailed, but can not therefore be interpreted as the restriction to the utility model claim.Should be pointed out that for the person of ordinary skill of the art without departing from the concept of the premise utility, can also make some distortion and improvement, these all belong to protection domain of the present utility model.Therefore, the protection domain of the utility model patent should be as the criterion with claims.

Claims (10)

1. nano material dispersing apparatus, comprise dispersion machine, described dispersion machine comprises emulsifier unit, agitating device and is used for putting the kettle that holds meter material, it is characterized in that, also comprise filter pump, nanometer sand mill, the first baiting valve, the second baiting valve, the 3rd baiting valve and material pipeline, described dispersion machine is connected with filter pump by material pipeline and the first baiting valve, described filter pump is connected with nanometer sand mill by material pipeline and the second baiting valve, and described nanometer sand mill is connected with dispersion machine by material pipeline and the 3rd baiting valve.
2. a kind of nano material dispersing apparatus according to claim 1 is characterized in that, described emulsifier unit is connected by the single mechanical end face seal part with kettle.
3. a kind of nano material dispersing apparatus according to claim 1 and 2 is characterized in that described agitating device is connected by packing seal element with kettle
4. a kind of nano material dispersing apparatus according to claim 1 is characterized in that, described kettle and nanometer sand mill all are arranged with heating jacket outward, are perfused with conduction oil in the heating jacket, and this heating jacket is provided with the conduction oil gateway.
5. a kind of nano material dispersing apparatus according to claim 1 is characterized in that, described filter pump is the bag filter with membrane pump.
6. a kind of nano material dispersing apparatus according to claim 5 is characterized in that, the filter of described filter is the thick corrosion resistant plate of 5mm, and its filter bores is less than 30 microns.
7. a kind of nano material dispersing apparatus according to claim 1 is characterized in that, the inner chamber of described nanometer sand mill and rotating dog rod are zirconia ceramics inner chamber and zirconia ceramics rotating dog rod.
8. a kind of nano material dispersing apparatus according to claim 1 is characterized in that, described the first baiting valve, the second baiting valve and the 3rd baiting valve are stainless valve.
9. a kind of nano material dispersing apparatus according to claim 1 is characterized in that, described material pipeline peripheral hardware has insulation jacket.
10. according to claim 1 or 9 described a kind of nano material dispersing apparatus, it is characterized in that described material pipeline is stainless-steel pipe.
CN 201220259661 2012-06-04 2012-06-04 Dispersing equipment for nanometer materials Expired - Lifetime CN202844920U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN 201220259661 CN202844920U (en) 2012-06-04 2012-06-04 Dispersing equipment for nanometer materials

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Application Number Priority Date Filing Date Title
CN 201220259661 CN202844920U (en) 2012-06-04 2012-06-04 Dispersing equipment for nanometer materials

Publications (1)

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CN202844920U true CN202844920U (en) 2013-04-03

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CN 201220259661 Expired - Lifetime CN202844920U (en) 2012-06-04 2012-06-04 Dispersing equipment for nanometer materials

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103240018A (en) * 2013-05-03 2013-08-14 南通金陵农化有限公司 Emulsifying and shearing device of suspending agent
CN103531761A (en) * 2013-10-28 2014-01-22 上海利物盛企业集团有限公司 Preparation method for nanometer silicon
CN104971802A (en) * 2015-05-22 2015-10-14 广西有色金属集团汇元锰业有限公司 Nanometer bead milling system and nanocrystalline microsphere preparation method
CN105032580A (en) * 2015-06-03 2015-11-11 安徽省铜陵县牛山矿业有限责任公司 Continuous grinding device for mineral extender

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103240018A (en) * 2013-05-03 2013-08-14 南通金陵农化有限公司 Emulsifying and shearing device of suspending agent
CN103531761A (en) * 2013-10-28 2014-01-22 上海利物盛企业集团有限公司 Preparation method for nanometer silicon
CN104971802A (en) * 2015-05-22 2015-10-14 广西有色金属集团汇元锰业有限公司 Nanometer bead milling system and nanocrystalline microsphere preparation method
CN104971802B (en) * 2015-05-22 2017-11-03 广西有色金属集团汇元锰业有限公司 A kind of preparation method of nano-beads grinding system and nano-crystalline microsphere
CN105032580A (en) * 2015-06-03 2015-11-11 安徽省铜陵县牛山矿业有限责任公司 Continuous grinding device for mineral extender

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Date Code Title Description
C14 Grant of patent or utility model
GR01 Patent grant
CP01 Change in the name or title of a patent holder

Address after: 201600 Shanghai Songjiang District Shihudang mayor road No. 85 building -2

Patentee after: Shanghai burning day new Mstar Technology Ltd

Address before: 201600 Shanghai Songjiang District Shihudang mayor road No. 85 building -2

Patentee before: Shanghai Jorle Fine Chem. Co., Ltd.

CX01 Expiry of patent term

Granted publication date: 20130403

CX01 Expiry of patent term