CN202740985U - Rosin esterification tail gas absorbing device - Google Patents

Rosin esterification tail gas absorbing device Download PDF

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Publication number
CN202740985U
CN202740985U CN 201220443272 CN201220443272U CN202740985U CN 202740985 U CN202740985 U CN 202740985U CN 201220443272 CN201220443272 CN 201220443272 CN 201220443272 U CN201220443272 U CN 201220443272U CN 202740985 U CN202740985 U CN 202740985U
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China
Prior art keywords
surge tank
tank
tail gas
alcohol
oil
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Expired - Fee Related
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CN 201220443272
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Chinese (zh)
Inventor
石富华
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Individual
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Individual
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Priority to CN 201220443272 priority Critical patent/CN202740985U/en
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Publication of CN202740985U publication Critical patent/CN202740985U/en
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Expired - Fee Related legal-status Critical Current

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Abstract

The utility model in particular relates to a rosin esterification tail gas absorbing device which comprises a reaction kettle (1), a gas exhaust pipe (2), a buffering tank (3), a vacuum pump (5), a connecting pipe (6), an alcohol absorbing tank (7) and an oil and water separating pool (8), wherein the reaction kettle (1) is connected with the buffering tank (3) through the gas exhaust pipe (2); behind the buffering tank (3), the reaction kettle (1) is respectively connected with the alcohol absorbing tank (7) and the vacuum pump (5); through a condensing effect of the buffering tank (3), small molecular substances are condensed in the buffering tank (3), so that the problem that the small molecular substances are condensed to block a pipeline is effectively solved; meanwhile, sticky substances obtained in the buffering tank (3) can be recycled, the blocking problem of the vacuum pump (5) is also reduced, the service life of the vacuum pump (5) is prolonged, the discharge of waste oil in the oil and water separating pool (8) is also reduced, and purposes of environment protection and clean production are achieved.

Description

The rosin esterification device for absorbing tail gas
Technical field
The present invention relates to device for absorbing tail gas, relate in particular to the device for absorbing tail gas in the rosin esterification technical process.
Background technology
Rosin ester is one of product important in the rosin reprocessing product, in process of production, the small-molecule substance that contains in the rosin can volatilize, be discharged to from reactor that condensation becomes liquid or semisolid thick substances the process of pipeline, in the course of time, the thick substances accumulation, easy blocking pipe, simultaneously, after esterification of rosin esterification is complete, in order to improve the product quality of rosin ester, reactor is vacuumized operation, small-molecule substance in the esterification products is wherein thoroughly separated, existing technology is to add a vavuum pump at the reactor discharge duct, rosin esterification tail gas is retracted in the oil-water separation tank separates, equally in vacuum, the small-molecule substance of extracting out also can be condensed into liquid or semisolid thick substances, cause the obstruction of vacuum-pump line, the vacuum that affects vavuum pump descends, and causes that not only the rosin esterification product is extracted impurity out incomplete, reduce the quality of esterification products, and the service life that can also reduce vavuum pump.In order to address the above problem, the utility model provides the rosin esterification device for absorbing tail gas, can solve the problem that esterification of rosin esterification produces the condensation blocking pipe of small-molecule substance, simultaneously, small-molecule substance wherein can be separated, reduce the discharging of the waste oil in the oil-water separation tank, reached the purpose of environmental protection, cleaner production.
Summary of the invention
For addressing the above problem, the rosin esterification device for absorbing tail gas that provides of the present utility model, comprise: reactor, blast pipe, surge tank, vavuum pump, tube connector, the alcohol tourie, oil-water separation tank forms, reactor is connected with surge tank through blast pipe, in the surge tank back, respectively with the alcohol tourie, vavuum pump links to each other, it is characterized in that: vavuum pump and tube connector are connected in parallel between surge tank and the alcohol tourie, blast pipe is connected in surge tank top, the top of surge tank is the triangular funnel shape of a back-off, purpose can access sufficient condensation when being blast pipe tail gas out by surge tank, can prevent from stopping up the purpose of exhaust outlet, the liquid that tail gas condensing obtains or semisolid thick substances, then rest in the surge tank, the surge tank outlet is in the surge tank middle and upper part, and its mouth of pipe protrudes from the inwall of surge tank, and purpose is to prevent that liquid or semisolid thick substances that tail gas condensing obtains from stopping up outlet when the buffering tank skin flow to the surge tank bottom.
In order to solve the problem of small-molecule substance condensation blocking pipe, described blast pipe is insulating tube, so that tail gas is discharged to not condensation in the surge tank process at blast pipe.In the process of producing, close the front valve of vavuum pump, valve responds still, surge tank, tube connector, alcohol tourie, the oil-water separation tank of opening tube connector form a path, the small-molecule substance that reaction produces, the at first condensation by surge tank, major part is condensed into liquid or semisolid thick substances, and rest in the surge tank, the uncondensable tail gas of part, then enter into the alcohol tourie, absorbed by alcohol, remaining a small amount of insoluble tail gas then enters into oil-water separation tank to be separated.After esterification is complete, this closes the valve of tube connector, open the front valve of vavuum pump, so that reactor, surge tank, vavuum pump, alcohol tourie, oil-water separation tank form a path, the small-molecule substance of extracting out is by the condensation of surge tank, be condensed into liquid or semisolid thick substances, rest in the surge tank, the uncondensable tail gas of part, then be retracted to the alcohol tourie by vavuum pump and absorbed by alcohol, remaining a small amount of insoluble tail gas then enters into oil-water separation tank to be separated.
The utility model can solve the problem that esterification of rosin esterification produces the condensation blocking pipe of small-molecule substance, the thick substances that in surge tank, obtains simultaneously, can reclaim use, also reduced the blockage problem of vavuum pump, improved its service life, also reduce the discharging of the waste oil in the oil-water separation tank, reached the purpose of environmental protection, cleaner production.
Description of drawings
Fig. 1 is the utility model rosin esterification device for absorbing tail gas schematic diagram.
Wherein: 1-reactor, 2-blast pipe, 3-surge tank, 4-surge tank outlet, 5-vavuum pump, 6-tube connector, 7-alcohol tourie, 8-oil-water separation tank.
The specific embodiment
Shown in Figure 1, the utility model rosin esterification device for absorbing tail gas, comprise: reactor (1), blast pipe (2), surge tank (3), vavuum pump (5), tube connector (6), alcohol tourie (7), oil-water separation tank (8) forms, reactor (1) is connected 3 through blast pipe (2) with surge tank) connect, in surge tank (3) back, respectively with alcohol tourie (7), vavuum pump (5) links to each other, in the process of producing, close the front valve of vavuum pump (5), open the valve of tube connector (6), reactor (1), surge tank (3), tube connector (6), alcohol tourie (7), oil-water separation tank (8) forms a path, the small-molecule substance that reaction produces, at first pass through the condensation of surge tank (3), major part is condensed into liquid or semisolid thick substances, and rest in the surge tank (3), the uncondensable tail gas of part, then enter into alcohol tourie (7), absorbed by alcohol, remaining a small amount of insoluble tail gas then enters into oil-water separation tank (8) to be separated.After esterification is complete, this closes the valve of tube connector (6), open the front valve of vavuum pump (5), so that reactor (1), surge tank (3), vavuum pump (5), alcohol tourie (7), oil-water separation tank (8) forms a path, the small-molecule substance of extracting out is by the condensation of surge tank (3), be condensed into liquid or semisolid thick substances, rest in the surge tank (3), the uncondensable tail gas of part, then be retracted to alcohol tourie (7) by vavuum pump (5) and absorbed by alcohol, remaining a small amount of insoluble tail gas then enters into oil-water separation tank (8) to be separated.
The utility model can solve the problem that esterification of rosin esterification produces the condensation blocking pipe of small-molecule substance, the thick substances that in surge tank, obtains simultaneously, can reclaim use, also reduced the blockage problem of vavuum pump, improved its service life, also reduce the discharging of the waste oil in the oil-water separation tank, reached the purpose of environmental protection, cleaner production.

Claims (3)

1. rosin esterification device for absorbing tail gas, comprise: reactor (1), blast pipe (2), surge tank (3), vavuum pump (5), tube connector (6), alcohol tourie (7), oil-water separation tank (8) forms, reactor (1) is connected 3 through blast pipe (2) with surge tank) connect, in surge tank (3) back, respectively with alcohol tourie (7), vavuum pump (5) links to each other, it is characterized in that: vavuum pump (5) and tube connector (6) are connected in parallel between surge tank (3) and the alcohol tourie (7), blast pipe (6) is connected in surge tank (3) top, and the top of surge tank (3) is the triangular funnel shape of a back-off.
2. described rosin esterification device for absorbing tail gas according to claim 1, it is characterized in that: described surge tank outlet (4) is in surge tank (3) middle and upper part, and its mouth of pipe protrudes from the inwall of surge tank (3).
3. described rosin esterification device for absorbing tail gas according to claim 1, it is characterized in that: described blast pipe (2) is insulating tube.
CN 201220443272 2012-09-01 2012-09-01 Rosin esterification tail gas absorbing device Expired - Fee Related CN202740985U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN 201220443272 CN202740985U (en) 2012-09-01 2012-09-01 Rosin esterification tail gas absorbing device

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN 201220443272 CN202740985U (en) 2012-09-01 2012-09-01 Rosin esterification tail gas absorbing device

Publications (1)

Publication Number Publication Date
CN202740985U true CN202740985U (en) 2013-02-20

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CN 201220443272 Expired - Fee Related CN202740985U (en) 2012-09-01 2012-09-01 Rosin esterification tail gas absorbing device

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CN (1) CN202740985U (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103349953A (en) * 2013-07-15 2013-10-16 江苏长乐纤维科技有限公司 Hydrolyzing furnace with emptying buffer device
CN104564770A (en) * 2014-11-28 2015-04-29 江门谦信化工发展有限公司 Submersible centrifugal pump for adding buffer tank in front of water pump of waste disposal basin in butyl acrylate production
CN105032111A (en) * 2014-11-26 2015-11-11 安徽嘉智信诺化工有限公司 Condensation recycling device

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103349953A (en) * 2013-07-15 2013-10-16 江苏长乐纤维科技有限公司 Hydrolyzing furnace with emptying buffer device
CN105032111A (en) * 2014-11-26 2015-11-11 安徽嘉智信诺化工有限公司 Condensation recycling device
CN105032111B (en) * 2014-11-26 2018-03-02 安徽嘉智信诺化工股份有限公司 A kind of condensate recycling device
CN104564770A (en) * 2014-11-28 2015-04-29 江门谦信化工发展有限公司 Submersible centrifugal pump for adding buffer tank in front of water pump of waste disposal basin in butyl acrylate production

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C17 Cessation of patent right
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20130220

Termination date: 20130901