CN202570151U - Reaction unit suitable for photochemistry polymerization in closed system - Google Patents
Reaction unit suitable for photochemistry polymerization in closed system Download PDFInfo
- Publication number
- CN202570151U CN202570151U CN 201220194779 CN201220194779U CN202570151U CN 202570151 U CN202570151 U CN 202570151U CN 201220194779 CN201220194779 CN 201220194779 CN 201220194779 U CN201220194779 U CN 201220194779U CN 202570151 U CN202570151 U CN 202570151U
- Authority
- CN
- China
- Prior art keywords
- stand
- reaction
- base plate
- reaction unit
- polymerization
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Images
Landscapes
- Physical Or Chemical Processes And Apparatus (AREA)
Abstract
Provided is a reaction unit suitable for photochemistry polymerization in a closed system. The reaction unit suitable for the photochemistry polymerization in the closed system is characterized in that an upright frame is arranged on a base plate, an upright frame sliding groove is arranged on the base plate, fixing nuts are arranged below the upright frame, a lamp holder is sleeved on the upright frame, an ultraviolet generator is arranged on the lamp holder, and lamp holder fixing bolts are arranged on one side of the upright frame. A fixed reaction container frame with a motor is arranged on the other side of the base plate, a rotating shaft is arranged above the fixed reaction container frame with the motor, and a plurality of sealed reaction quartz bottles are fixed on the rotating shaft through iron wires. The reaction unit suitable for the photochemistry polymerization in the closed system is simple in structure, low in production cost and use cost, small in size and convenient to maintain.
Description
Technical field
The utility model relates to a kind of reaction unit of chemical polymerization, especially is suitable for the reaction unit of enclosed system photochemical polymerization.
Background technology
At present, it is varied to carry out the device of polymerisation.To the complexity of polymerization system, developed the polymerizing reactor of many special uses abroad successively.For guaranteeing the application of polymerization product at biomedicine field, people have inquired into the polymerizing reactor under the room temperature condition, and the ultraviolet irradiation polymerizing reactor promptly is wherein a kind of.Adopt this device, remove and can carry out conventional radical polymerization, also can trigger molecule in not double bond containing monomer polymerization.Now domesticly disclose the polymerizing reactor that a kind of ultraviolet ray irradiation causes, this device comprises that one can see through ultraviolet reaction vessel and one and is used to produce ultraviolet ray and be radiated at the ultraviolet ray generating apparatus on this reactor.This device mainly is suitable for the reaction system of open type, needs to add in addition mechanical stirring device to guarantee mixing of reaction system, in course of reaction, need constantly feed inert gas to guarantee the oxygen-free environment of reaction.Use this device not only can consume a large amount of inert gases, and isolated effect is not fine.
Summary of the invention
In order to overcome the in-problem deficiency of prior art; The utility model provides a kind of novel reaction unit that is suitable for the enclosed system photochemical polymerization, this reaction unit, and the ultraviolet irradiation that is provided is even, light intensity is controlled; And good heat dispersion performance can guarantee the medical quality of sample.
The utility model solves the technical scheme that its technical problem adopted: the reaction unit that is suitable for the enclosed system photochemical polymerization; The quartzy bottle of fixation reaction receptacle stand, turning cylinder, sealed reaction, ultraviolet generater, lamp bracket, stand, set bolt, hold-down nut, base plate, iron wire by translator are formed; On base plate, stand is housed, base plate is provided with the stand sliding tray; There is hold-down nut the stand below; Be with lamp bracket in the stand, ultraviolet generater is housed on the lamp bracket, a side of stand has the lamp bracket set bolt.The base plate opposite side is equipped with the fixation reaction receptacle stand of translator, and there is turning cylinder the fixation reaction receptacle stand top of translator, fixes the quartzy bottle of a plurality of sealed reactions with iron wire on the turning cylinder.
This reaction unit that is suitable for the enclosed system photochemical polymerization; In use; At first the quartzy bottle of sealed reaction is fixed on the turning cylinder, ultraviolet generater is fixed on the lamp bracket, the height of the lamp bracket of ultraviolet generater is housed through regulating the adjustment of set bolt and hold-down nut; Regulate the position of stand in the base plate sliding tray, guarantee that the quartzy bottle of lamp bracket and sealed reaction is on the same horizontal plane.Open motor switch on the fixation reaction receptacle stand of translator, adjustment turning cylinder rotating speed is opened the switch of ultraviolet generater then, begins reaction.Behind the reaction setting-up time, close motor switch on the fixation reaction receptacle stand of switch and translator of ultraviolet generater, the position of lamp bracket in the adjustment base plate sliding tray is so that unload ultraviolet generater, and the quartzy bottle of sealed reaction unloads from turning cylinder then.
This base plate that is suitable for the reaction unit of enclosed system photochemical polymerization is a rectangular rigid plastic sheet, and it can also have other shape.The quartzy bottle of sealed reaction is 8-10 centimetre apart from the fixation reaction receptacle stand horizontal range of translator.The quartzy bottle of sealed reaction can well see through ultraviolet ray, can guarantee good air-tightness, in course of reaction, need not to charge into continuously nitrogen.Ultraviolet generater can comprise one or more ultraviolet generaters.
The beneficial effect of the utility model is, this reaction unit that is suitable for the enclosed system photochemical polymerization, simple in structure, manufacturing and use cost is low, volume is less; Be convenient to maintenance; The ultraviolet irradiation that is provided is even, light intensity is controlled, and good heat dispersion performance, because the dominant wavelength of employed low-pressure steam mercury lamp is 253.7 nanometers; Various bacteria and virus can be killed, the medical quality of sample can be guaranteed.Be particularly conducive to the preparation of big particle diameter spherical polymer.
Description of drawings
Below in conjunction with accompanying drawing and embodiment the utility model is further specified.
Fig. 1 is the reaction unit front view that is suitable for the enclosed system photochemical polymerization.
Fig. 2 is the reaction unit vertical view that is suitable for the enclosed system photochemical polymerization.
The fixation reaction receptacle stand of 1. translators among the figure, 2. turning cylinder, the 3. quartzy bottle of sealed reaction, 4. ultraviolet generater, 5. lamp bracket, 6. stand, 7. set bolt, 8. hold-down nut, 9. base plate, 10 iron wires.
The specific embodiment
In Fig. 1,2, be suitable for the reaction unit of enclosed system photochemical polymerization, on rectangle base plate 9; Stand 6 is housed, and base plate is provided with the stand sliding tray, and there is hold-down nut 8 the stand below; Be with lamp bracket 5 in the stand, ultraviolet generater 4 is housed on the lamp bracket, a side of stand has lamp bracket set bolt 7.The base plate opposite side is equipped with the fixation reaction receptacle stand 1 of translator, and there is turning cylinder 2 the fixation reaction receptacle stand top of translator, with 10 fixing bundles on iron wire the quartzy bottle 3 of four sealed reactions is arranged on the turning cylinder.
Claims (3)
1. be suitable for the reaction unit of enclosed system photochemical polymerization; The quartzy bottle of fixation reaction receptacle stand, turning cylinder, sealed reaction, ultraviolet generater, lamp bracket, stand, set bolt, hold-down nut, base plate, iron wire by translator are formed, and it is characterized in that: on base plate (9), stand (6) is housed; There is hold-down nut (8) the stand below; Be with lamp bracket (5) in the stand, ultraviolet generater (4) is housed on the lamp bracket, the base plate opposite side is equipped with the fixation reaction receptacle stand (1) of translator; There is turning cylinder (2) the fixation reaction receptacle stand top of translator, fixes the quartzy bottles of a plurality of sealed reactions (3) with iron wire (10) on the turning cylinder.
2. the reaction unit that is suitable for the enclosed system photochemical polymerization according to claim 1 is characterized in that: base plate is provided with the stand sliding tray.
3. the reaction unit that is suitable for the enclosed system photochemical polymerization according to claim 1 is characterized in that: a side of stand has lamp bracket set bolt (7).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201220194779 CN202570151U (en) | 2012-05-03 | 2012-05-03 | Reaction unit suitable for photochemistry polymerization in closed system |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201220194779 CN202570151U (en) | 2012-05-03 | 2012-05-03 | Reaction unit suitable for photochemistry polymerization in closed system |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN202570151U true CN202570151U (en) | 2012-12-05 |
Family
ID=47239607
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 201220194779 Expired - Fee Related CN202570151U (en) | 2012-05-03 | 2012-05-03 | Reaction unit suitable for photochemistry polymerization in closed system |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN202570151U (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103145885A (en) * | 2013-03-19 | 2013-06-12 | 中国海洋石油总公司 | Experimental instrument for photo-initiated solution polymerization |
| CN103145883A (en) * | 2013-03-19 | 2013-06-12 | 中国海洋石油总公司 | Experimental instrument for photo-initiated solution polymerization |
| CN103265657A (en) * | 2013-05-27 | 2013-08-28 | 德州学院 | Method for preparing monodisperse polymer microspheres by photo-initiation precipitation polymerization |
-
2012
- 2012-05-03 CN CN 201220194779 patent/CN202570151U/en not_active Expired - Fee Related
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103145885A (en) * | 2013-03-19 | 2013-06-12 | 中国海洋石油总公司 | Experimental instrument for photo-initiated solution polymerization |
| CN103145883A (en) * | 2013-03-19 | 2013-06-12 | 中国海洋石油总公司 | Experimental instrument for photo-initiated solution polymerization |
| CN103145883B (en) * | 2013-03-19 | 2015-06-17 | 中国海洋石油总公司 | Experimental instrument for photo-initiated solution polymerization |
| CN103265657A (en) * | 2013-05-27 | 2013-08-28 | 德州学院 | Method for preparing monodisperse polymer microspheres by photo-initiation precipitation polymerization |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN202570151U (en) | Reaction unit suitable for photochemistry polymerization in closed system | |
| Liu et al. | Edge activation of an inert polymeric carbon nitride matrix with boosted absorption kinetics and near-infrared response for efficient photocatalytic CO 2 reduction | |
| AR007504A1 (en) | A PROCEDURE FOR PRODUCING A POLYMER IN A GAS FLUIDIZED BED REACTION CONTAINER WITH A POLYMERIZATION ZONE CONTAINING A BED OF DEVELOPING POLYMERIC PARTICLES UNDER CONDITIONS OF POLYMERIZATION | |
| CN109772357B (en) | Copper bismuthate/tungsten oxide composite film material, preparation method and application in preparing methane by photocatalytic carbon dioxide | |
| CN201223794Y (en) | Multifunctional photochemistry reactor | |
| CN103586463A (en) | Method of green synthesis of nanogold through kiwi fruit juice | |
| CN107081139B (en) | A kind of cuprous oxide-non-woven fabrics nanocomposite and its preparation method and application | |
| Chen et al. | 3D‐Printed Light‐Driven Microswimmer with Built‐In Micromotors | |
| Liu et al. | Rice husk biochar mediated red phosphorus for photocatalysis and photothermal removal of E. coli | |
| CN114573825A (en) | Ligand-exchanged hollow MIL-101 metal organic framework material and preparation method and application thereof | |
| CN110280195A (en) | A kind of light-catalyzed reaction system and its application during artificial fixed nitrogen | |
| Wu et al. | Influence of molecular weight of chitosan on the microstructures and photocatalytic property of ZrO2 prepared by chitosan templates method | |
| CN108439488B (en) | A kind of preparation method and application of amorphous oxide cobalt nanometer sheet | |
| CN211189886U (en) | Portable stirring device for high-molecular product burdening containing HQEE | |
| CN105399137B (en) | The preparation method and products obtained therefrom of a kind of spherical self-assembled structures of buergerite phase CdS | |
| CN110433858B (en) | Ag/PANI/graphene composite photocatalyst, and preparation method and application thereof | |
| CN203829357U (en) | Ultraviolet disinfection device | |
| CN110856816B (en) | Surface-regulated plasma catalyst and preparation method and application thereof | |
| Rusinque | Hydrogen production by photocatalytic water splitting under near-UV and visible light using doped Pt and Pd TiO2 | |
| CN106206398A (en) | A kind of silicon chip translation placement mechanism | |
| CN213633116U (en) | Micro-plastic ultraviolet aging test device | |
| CN213022559U (en) | Device for simulating plastic particle aging in natural environment | |
| CN110665025B (en) | Ultraviolet disinfection device | |
| CN209187621U (en) | A kind of elevating mechanism of pulse bactericidal unit | |
| CN215350822U (en) | Multifunctional steam sterilizer |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20121205 Termination date: 20160503 |