CN202508882U - Device for preparing feed grade calcium phosphate dibasic through acid waste water - Google Patents

Device for preparing feed grade calcium phosphate dibasic through acid waste water Download PDF

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Publication number
CN202508882U
CN202508882U CN2012201218109U CN201220121810U CN202508882U CN 202508882 U CN202508882 U CN 202508882U CN 2012201218109 U CN2012201218109 U CN 2012201218109U CN 201220121810 U CN201220121810 U CN 201220121810U CN 202508882 U CN202508882 U CN 202508882U
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China
Prior art keywords
tank
outlet
filtering centrifuge
high rate
waste water
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Expired - Lifetime
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CN2012201218109U
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Chinese (zh)
Inventor
杨毅
周智武
李志坚
饶轶晟
刘海
胡国涛
丁川
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Wengfu Group Co Ltd
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Wengfu Group Co Ltd
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Priority to CN2012201218109U priority Critical patent/CN202508882U/en
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Abstract

The utility model discloses a device for preparing feed grade calcium phosphate dibasic through acid waste water. The device is formed by an adjusting tank, a defluorination and dearsenification reaction tank, an efficient settling tank A, a filtering centrifuge A, a neutral reaction tank, an efficient settling tank B, a filtering centrifuge B and a pipeline, wherein an inlet of the adjusting tank is communicated with a filtering centrifuge tank; an outlet of the adjusting tank is communicated with the defluorination and dearsenification reaction tank; an inlet of the efficient settling tank A is communicated with an outlet of the defluorination and dearsenification reaction tank through the pipeline; an outlet of the efficient settling tank A is connected with the neutral reaction tank; the filtering centrifuge A is connected between the efficient settling tank A and the neutral reaction tank through the pipeline; an outlet of the neutral reaction tank is communicated with the efficient settling tank B; and an outlet of the efficient settling tank B is connected with the filtering centrifuge B. The device has the advantages of simple structure, low production cost, high product value added, and stronger market competitiveness, and brings huge economic benefit for enterprises.

Description

A kind of device of producing calcium hydrophosphate fodder with acid waste water
Technical field
The utility model relates to acid waste water process for producing field, especially phosphorus-containing wastewater and produces the calcium hydrophosphate fodder device.
Background technology
In the treating processes of existing present high-density phosphorus, fluoric acid wastewater, adopt secondary lime acid-base neutralisation method more.And a large amount of sewage slag that will produce after the processing waste water, and the part addition material as phosphate fertilizer used after sewage slag can only adopt the slag dam heap to fill out or dry at present.
But these methods all do not have and can thoroughly use sewage slag, particularly in the slag contain a large amount of phosphor resources, not only caused the waste of resource, possibly cause simultaneously the pollution of environment.
Summary of the invention
The purpose of this device is the weak point to prior art; Provide a kind of acid waste water that is used for to handle the device of producing calcium hydrophosphate fodder; This device can effectively carry out sedimentation to acidic substance in implementation process; Guarantee that the water outlet quality reaches the requirement of calcium hydrophosphate fodder, the calcium hydrophosphate fodder of its production is up to state standards.
The technical scheme that the utility model adopts: a kind of device of producing calcium hydrophosphate fodder with acid waste water; It is made up of equalizing tank, defluorinate, arsenic reactive tank, high rate settling A, filtering centrifuge A, neutralization reaction groove, high rate settling B, filtering centrifuge B and pipeline; Wherein the inlet of equalizing tank is connected with pond, slag field; The outlet of equalizing tank is communicated with defluorinate, arsenic reactive tank; The inlet of high rate settling A is communicated with through pipeline with the outlet of defluorinate, arsenic reactive tank, and the outlet of high rate settling A connects the neutralization reaction groove, also has pipe connection filtering centrifuge A between said high rate settling A and the neutralization reaction groove; The outlet of neutralization reaction groove is connected with high rate settling B, and the outlet of high rate settling B connects filtering centrifuge B.
All be provided with pH meter and charging opening on above-mentioned defluorinate, arsenic reactive tank and the neutralization reaction groove.
The recyclable utilization of water after above-mentioned filtering centrifuge B filters.
Product after above-mentioned filtering centrifuge B filtration is centrifugal can obtain calcium monophosphate product after the drying machine drying.
The use flow process of this device is: phosphate fertilizer plant's waste water is added in the equalizing tank, add silicon-dioxide and sodium-chlor then, with supernatant liquid adding defluorinate, the arsenic reactive tank of preliminary defluorinate; Add defluorinate, dearsenic agent then, get into high rate settling A and add the flocculation agent sedimentation after reaction is accomplished, the overflow water of high rate settling A joins in the neutralization reaction groove and uses; Simultaneously; Filtering centrifuge A crosses the leaching supernatant liquid and also adds in the neutralization reaction groove, and to wherein adding milk of lime, reaction finishes the back and gets into high rate settling B sedimentation; Last centrifuging, drying obtains product.
The utlity model has following advantage: the Vanadium Pentoxide in FLAKES that adopts this device fully effectively to reclaim in phosphate fertilizer plant's waste water prepares calcium hydrophosphate fodder, improves the utilization ratio of resource; And this apparatus structure is simple, low production cost, and value-added content of product is high, has the stronger market competitiveness, for enterprise brings great economic benefit.
Description of drawings
Fig. 1 is the structural representation of the utility model.
Among the figure: 1, equalizing tank; 2, defluorinate, arsenic reactive tank; 3, high rate settling A; 4, filtering centrifuge A; 5, neutralization reaction groove; 6, high rate settling B; 7, filtering centrifuge B; 8, pond, slag field; 9, drying machine; Water after 10 filtrations.
Embodiment
Embodiment
A kind of device of producing calcium hydrophosphate fodder with acid waste water; It is made up of equalizing tank 1, defluorinate, arsenic reactive tank 2, high rate settling A 3, filtering centrifuge A 4, neutralization reaction groove 5, high rate settling B 6, filtering centrifuge B 7 and pipeline; Wherein the inlet of equalizing tank 1 is connected with pond, slag field 8; The outlet of equalizing tank 1 is communicated with defluorinate, arsenic reactive tank 2; The inlet of high rate settling A 3 is communicated with through pipeline with the outlet of defluorinate, arsenic reactive tank 2, and the outlet of high rate settling A 3 connects neutralization reaction groove 5, also has pipe connection filtering centrifuge A4 between said high rate settling A3 and the neutralization reaction groove 5; The outlet of neutralization reaction groove 5 is connected with high rate settling B 6, and the outlet of high rate settling B 6 connects filtering centrifuge B 7.
All be provided with pH meter and charging opening on above-mentioned defluorinate, arsenic reactive tank 2 and the neutralization reaction groove 5.
Water 10 recyclable utilizations after above-mentioned filtering centrifuge B 7 filters.
Product after above-mentioned filtering centrifuge B 7 filtrations are centrifugal can obtain calcium monophosphate product after drying machine 9 dryings.
The phosphorus content of the waste water in the pond, above-mentioned slag field 8 is 1.0 ~ 1.4%, and fluorine content is 0.50 ~ 0.80%.

Claims (2)

1. device of producing calcium hydrophosphate fodder with acid waste water; It is made up of equalizing tank (1), defluorinate, arsenic reactive tank (2), high rate settling A (3), filtering centrifuge A (4), neutralization reaction groove (5), high rate settling B (6), filtering centrifuge B (7) and pipeline; Wherein the inlet of equalizing tank (1) is connected with pond, slag field (8); The outlet of equalizing tank (1) is communicated with defluorinate, arsenic reactive tank (2); The inlet of high rate settling A (3) is communicated with through pipeline with the outlet of defluorinate, arsenic reactive tank (2); The outlet of high rate settling A (3) connects neutralization reaction groove (5), also has pipe connection filtering centrifuge A (4) between said high rate settling A (3) and the neutralization reaction groove (5); The outlet of neutralization reaction groove (5) is connected with high rate settling B (6), and the outlet of high rate settling B (6) connects filtering centrifuge B (7).
2. according to claim 1ly produce the device of calcium hydrophosphate fodder, it is characterized in that all being provided with pH meter and charging opening on said defluorinate, arsenic reactive tank (2) and the neutralization reaction groove (5) with acid waste water.
CN2012201218109U 2012-03-28 2012-03-28 Device for preparing feed grade calcium phosphate dibasic through acid waste water Expired - Lifetime CN202508882U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN2012201218109U CN202508882U (en) 2012-03-28 2012-03-28 Device for preparing feed grade calcium phosphate dibasic through acid waste water

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN2012201218109U CN202508882U (en) 2012-03-28 2012-03-28 Device for preparing feed grade calcium phosphate dibasic through acid waste water

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CN202508882U true CN202508882U (en) 2012-10-31

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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103435024A (en) * 2013-08-08 2013-12-11 瓮福(集团)有限责任公司 Method for producing feed grade calcium hydrophosphate
CN103449393A (en) * 2013-08-21 2013-12-18 瓮福(集团)有限责任公司 Feed-grade dicalcium phosphate production device
CN103738931A (en) * 2013-11-26 2014-04-23 瓮福(集团)有限责任公司 Method for production of potassium dihydrogen phosphate from phosphorus-containing acidic wastewater
CN110078039A (en) * 2019-06-04 2019-08-02 瓮福(集团)有限责任公司 A kind of low-concentration phosphorus-containing wastewater step produces the method and device of calcium hydrophosphate fodder
CN111747390A (en) * 2020-08-10 2020-10-09 朱宇杰 Feed-grade calcium phosphate salt production system and method

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103435024A (en) * 2013-08-08 2013-12-11 瓮福(集团)有限责任公司 Method for producing feed grade calcium hydrophosphate
CN103449393A (en) * 2013-08-21 2013-12-18 瓮福(集团)有限责任公司 Feed-grade dicalcium phosphate production device
CN103738931A (en) * 2013-11-26 2014-04-23 瓮福(集团)有限责任公司 Method for production of potassium dihydrogen phosphate from phosphorus-containing acidic wastewater
CN110078039A (en) * 2019-06-04 2019-08-02 瓮福(集团)有限责任公司 A kind of low-concentration phosphorus-containing wastewater step produces the method and device of calcium hydrophosphate fodder
CN110078039B (en) * 2019-06-04 2023-09-22 瓮福(集团)有限责任公司 Method and device for preparing feed-grade calcium hydrophosphate in low-concentration phosphorus-containing wastewater step manner
CN111747390A (en) * 2020-08-10 2020-10-09 朱宇杰 Feed-grade calcium phosphate salt production system and method

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Granted publication date: 20121031

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