CN202478916U - Production device for liquid water-soluble resin - Google Patents

Production device for liquid water-soluble resin Download PDF

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Publication number
CN202478916U
CN202478916U CN2012200345588U CN201220034558U CN202478916U CN 202478916 U CN202478916 U CN 202478916U CN 2012200345588 U CN2012200345588 U CN 2012200345588U CN 201220034558 U CN201220034558 U CN 201220034558U CN 202478916 U CN202478916 U CN 202478916U
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CN
China
Prior art keywords
tank
monomer
outlet
soluble resin
polymerization reaction
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
CN2012200345588U
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Chinese (zh)
Inventor
周贤永
丁立刚
张凤丽
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
JIANGSU TIGER INK CO Ltd
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JIANGSU TIGER INK CO Ltd
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Publication date
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Priority to CN2012200345588U priority Critical patent/CN202478916U/en
Application granted granted Critical
Publication of CN202478916U publication Critical patent/CN202478916U/en
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

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Abstract

The utility model provides a production device for liquid water-soluble resin. The production device for the liquid water-soluble resin comprises a monomer purification tank, a monomer feeding tank, an alcohol high position tank, a cooling tower, an alkali tank and a polymerization reaction still, wherein an outlet of the monomer purification tank is connected with a feeding inlet of the monomer feeding tank through a pipeline, a reflux pipe connected with the cooling tower is arranged on a reflux opening of the polymerization reaction still, and the feeding inlet is connected with a feeding outlet of the monomer feeding tank through a material pipeline. An auxiliary material opening is connected with an alcohol outlet of the alcohol high position tank through an auxiliary material pipeline and a raw material outlet of the alkali tank is connected with an inlet of the monomer purification tank through a transport pipeline. The production device for the liquid water-soluble resin achieves automatic production of the liquid water-soluble resin, and subsequent reaction time of washed monomer material in the alkali tank can be shortened, finished products have a light color and have no influence on colors of the down-stream products. A reaction cannot generatephenomena of implosion and is more stable, gel rate is low and filtration is easy, molecular weight distribution is narrower and various performance indexes of the products are enhanced.

Description

The process units of aqueous water soluble resin
Technical field
The utility model relates to a kind of process units, particularly a kind of process units of aqueous water soluble resin.
Background technology
The aqueous water soluble resin does not have complete automatic production device in the prior art when production and processing, and existing raw material monomer does not carry out alkali cleaning; The finished color of making like this is dark, can influence the form and aspect of downstream product, and monomer product impurity is many simultaneously; Reaction is unstable in manufacture process; Gel fraction is high, is not easy to filter, and influences each item performance indications of aqueous water soluble resin simultaneously easily.
Summary of the invention
The utility model technical problem to be solved is the deficiency to prior art, provides a kind of reasonable in design, easy to use, the process units of the aqueous water soluble resin that can enhance product performance.
The utility model technical problem to be solved is to realize through following technical scheme; The utility model is a kind of process units of aqueous water soluble resin; Be characterized in: comprise monomer purification tank, monomer addition groove, alcohol head tank and polymerization reaction kettle, the monomer purification tank is provided with import and outlet, and the monomer addition groove is provided with reinforced inlet and reinforced outlet; Be connected through pipeline between the reinforced inlet of the outlet of monomer purification tank and monomer addition groove; Described alcohol head tank is provided with alcohol charging aperture and alcohol discharging opening, and the top of described polymerization reaction kettle is provided with charging aperture, auxiliary material mouth and refluxing opening, and the bottom of polymerization reaction kettle is provided with discharging opening; Described refluxing opening is provided with the return duct that is connected with cooling tower; Be connected through material pipe between the reinforced outlet of the charging aperture of described polymerization reaction kettle and monomer addition groove, be connected through the auxiliary material pipeline between the auxiliary material mouth of polymerization reaction kettle and the alcohol discharging opening of alcohol head tank, described auxiliary material pipeline is provided with the resin feedback outlet; It also is provided with the alkali groove, and the alkali groove is provided with material inlet and material outlet, is connected through transfer pipeline between the import of the material outlet of alkali groove and monomer purification tank, and transfer pipeline is provided with control valve.
The utility model technical problem to be solved can also realize that further be connected with discharge nozzle on the discharging opening of described polymerization reaction kettle, discharge nozzle is provided with filter through following technical scheme.
The utility model uses through alkali groove, monomer purification tank, monomer addition groove, alcohol head tank, cooling tower and polymerization reaction kettle combination, realizes the automated production of aqueous water soluble resin, through the raw material monomer of alkali groove alkali cleaning; Can shorten the follow-up reaction time, the finished color of making is more shallow, does not influence the form and aspect of downstream product; Raw material monomer impurity is few simultaneously, instead would not gather cruelly, reacts more stable; And the gel fraction of finished product is low; Easy filtration, molecular weight distribution is narrower, and each item performance indications of product promote high.Compared with prior art, it is reasonable in design, and is simple to operate, easy to use, has improved production efficiency, has improved properties of product simultaneously.
Description of drawings
Fig. 1 is a kind of structural representation of the utility model.
The specific embodiment
Following with reference to accompanying drawing, further describe the concrete technical scheme of the utility model, so that those skilled in the art understands the present invention further, and do not constitute restriction to its right.
Embodiment 1; With reference to Fig. 1, a kind of process units of aqueous water soluble resin comprises monomer purification tank 1, monomer addition groove 2, alcohol head tank 3, cooling tower 5 and polymerization reaction kettle 6; Monomer purification tank 1 is provided with import and outlet; Monomer addition groove 2 is provided with reinforced inlet and reinforced outlet, is connected through pipeline between the reinforced inlet of the outlet of monomer purification tank 1 and monomer addition groove 2, and described alcohol head tank 3 is provided with alcohol charging aperture and alcohol discharging opening; The top of described polymerization reaction kettle 6 is provided with charging aperture, auxiliary material mouth and refluxing opening; The bottom of polymerization reaction kettle 6 is provided with discharging opening, and described refluxing opening is provided with the return duct that is connected with cooling tower 5, is connected through material pipe between the reinforced outlet of the charging aperture of described polymerization reaction kettle 6 and monomer addition groove 2; Be connected through the auxiliary material pipeline between the auxiliary material mouth of polymerization reaction kettle 6 and the alcohol discharging opening of alcohol head tank 3, described auxiliary material pipeline is provided with resin feedback outlet 4; It also is provided with alkali groove 8, and alkali groove 8 is provided with material inlet and material outlet, is connected through transfer pipeline between the import of the material outlet of alkali groove 8 and monomer purification tank 1, and transfer pipeline is provided with control valve.
Embodiment 2, in the process units of embodiment 1 described aqueous water soluble resin, are connected with discharge nozzle on the discharging opening of described polymerization reaction kettle 6, and discharge nozzle is provided with filter 7, can increase the degree of purity of water-soluble resin.

Claims (2)

1. the process units of an aqueous water soluble resin; It is characterized in that: it comprises monomer purification tank, monomer addition groove, alcohol head tank, cooling tower and polymerization reaction kettle; The monomer purification tank is provided with import and outlet; The monomer addition groove is provided with reinforced inlet and reinforced outlet, is connected through pipeline between the reinforced inlet of the outlet of monomer purification tank and monomer addition groove, and described alcohol head tank is provided with alcohol charging aperture and alcohol discharging opening; The top of described polymerization reaction kettle is provided with charging aperture, auxiliary material mouth and refluxing opening; The bottom of polymerization reaction kettle is provided with discharging opening, and described refluxing opening is provided with the return duct that is connected with cooling tower, is connected through material pipe between the reinforced outlet of the charging aperture of described polymerization reaction kettle and monomer addition groove; Be connected through the auxiliary material pipeline between the auxiliary material mouth of polymerization reaction kettle and the alcohol discharging opening of alcohol head tank, described auxiliary material pipeline is provided with the resin feedback outlet; It also is provided with the alkali groove, and the alkali groove is provided with material inlet and material outlet, is connected through transfer pipeline between the import of the material outlet of alkali groove and monomer purification tank, and transfer pipeline is provided with control valve.
2. according to the process units of the described aqueous water soluble resin of root claim 1, it is characterized in that: be connected with discharge nozzle on the discharging opening of described polymerization reaction kettle, discharge nozzle is provided with filter.
CN2012200345588U 2012-02-03 2012-02-03 Production device for liquid water-soluble resin Expired - Lifetime CN202478916U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN2012200345588U CN202478916U (en) 2012-02-03 2012-02-03 Production device for liquid water-soluble resin

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN2012200345588U CN202478916U (en) 2012-02-03 2012-02-03 Production device for liquid water-soluble resin

Publications (1)

Publication Number Publication Date
CN202478916U true CN202478916U (en) 2012-10-10

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN2012200345588U Expired - Lifetime CN202478916U (en) 2012-02-03 2012-02-03 Production device for liquid water-soluble resin

Country Status (1)

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CN (1) CN202478916U (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103191689A (en) * 2013-04-26 2013-07-10 青岛中科荣达新材料有限公司 Production device of potassium dimethyldithiocarbamate and preparation method thereof
CN104307424A (en) * 2014-09-29 2015-01-28 张家港市三联化工科技有限公司 High-concentration caustic soda liquid preparation device

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103191689A (en) * 2013-04-26 2013-07-10 青岛中科荣达新材料有限公司 Production device of potassium dimethyldithiocarbamate and preparation method thereof
CN103191689B (en) * 2013-04-26 2015-12-09 青岛中科荣达新材料有限公司 The process units of the U.S. potassium of a kind of liquid good fortune and production method thereof
CN104307424A (en) * 2014-09-29 2015-01-28 张家港市三联化工科技有限公司 High-concentration caustic soda liquid preparation device

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CX01 Expiry of patent term

Granted publication date: 20121010

CX01 Expiry of patent term