CN202465292U - Device for producing molten obtuse quartz sand by taking waste quartz crucible as raw material - Google Patents
Device for producing molten obtuse quartz sand by taking waste quartz crucible as raw material Download PDFInfo
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- CN202465292U CN202465292U CN2012201002053U CN201220100205U CN202465292U CN 202465292 U CN202465292 U CN 202465292U CN 2012201002053 U CN2012201002053 U CN 2012201002053U CN 201220100205 U CN201220100205 U CN 201220100205U CN 202465292 U CN202465292 U CN 202465292U
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- crucible
- quartz
- transfer roller
- quartz sand
- obtuse
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Abstract
The utility model discloses a device for producing molten obtuse quartz sand by taking a waste quartz crucible as a raw material, and belongs to the field of processing of molten quartz. The device consists of a crushing machine, an acid pond, a washing machine, a high-temperature sintering furnace, a vibration sieve and a magnetic separator. A production process of the molten obtuse quartz sand comprises the following steps of: crushing, pickling, washing, sintering at high temperature, melting and cooling the waste quartz crucible material, then performing crushing, screening and magnetic separation, and thus obtaining the molten obtuse quartz sand used by a quartz crucible. The specification of the quartz sand is 0.075 to 4.5 millimeters.. The device has the advantages that the investment is small because general equipment is used; a batch of high-quality molten obtuse quartz sand for the quartz crucible can be produced; and the quartz sand can replace imported high-purity quartz sand from the abroad and is used for producing the quartz crucible.
Description
Technical field
The utility model belongs to the fused quartz manufacture field, and relating in particular to a kind of is the production equipment of primary industry production crucible with fusion obtuse angle silica sand with barren rock English crucible.
Background technology
Crucible is with fireproof material made vessel or melting pot, by the starting material of making can be divided into, plumbago crucible, quartz crucible, porcelain crucible, corundum crucible, silicon carbide crucible, platinum crucible, nickel crucible.Quartz crucible is an important kind of crucible, can have high purity, high temperature resistant, advantages such as size is big, precision is high, good heat preservation performance, save energy, steady quality using below 1450 ℃.Quartz crucible is to produce polysilicon, drawing large-diameter monocrystalline silicon, the requisite base mateiral of development large-scale integrated circuit.The production technique of crucible is: 1. with the glass sand vacuum graphite forming mould of packing into; 2. vacuum arc is founded; 3. the naturally cooling demoulding; 4. cold working sandblast; 5. ultra-clean cleaning, high-pressure spraying, oven dry automatically; 6 heat bakings, vacuum packaging obtain finished product.But the main raw material glass sand of domestic production quartz crucible use at present needs produce following problem like this by external import, and 1. the imported raw material expensive causes the production cost of quartz crucible to increase greatly, also makes the selling price of quartz crucible higher; 2. the source of raw material, quantity and time can not get ensureing; Though as use homemade silica sand to overcome cost of material height, source, quantity and time all to can not get the defective that ensures, the quartz crucible quality of homemade glass sand production is restricted, its stability is poor slightly when pulling monocrystal silicon.For cost and the utilization of waste material that reduces the domestic production quartz crucible; It is that raw material production prepares the production equipment of quartz crucible with fusion obtuse angle silica sand with barren rock English crucible that the utility model has been developed a kind of; Form by crusher, sour pond, rinsing machine, high temperature sintering furnace, vibratory screening apparatus, magnetic separator; Its production technique is: with obtaining making the fusion obtuse angle silica sand that quartz crucible uses after the fragmentation of barren rock English crucible material, pickling, washing, high temperature sintering fusion, cooling back fragmentation, screening, the magnetic separation; The specification of silica sand is 0.075mm-4.5mm; The advantage of this production equipment is: use general-purpose equipment, investment little, can mass-produce high-quality quartz crucible with fusion obtuse angle silica sand, the alternative external import glass sand of this silica sand is produced quartz crucible, both utilization of waste material; Produce bigger economic benefit, produced the huge social benefit again.
Summary of the invention
It is the production equipment of primary industry production crucible with fusion obtuse angle silica sand with barren rock English crucible that the problem that the utility model mainly solves provides a kind of; The advantage of this device is: use general-purpose equipment, little, the no toxic and harmful of investment and liquid discharge, the alternative external import glass sand of product to produce quartz crucible; But this device utilization of waste material; Produce bigger economic benefit, produced the huge social benefit again.
The technical scheme that the utility model adopts is:
A kind of is the production equipment of primary industry production crucible with fusion obtuse angle silica sand with barren rock English crucible, comprising: crusher 1, sour pond 2, rinsing machine 3, high temperature sintering furnace 4, vibratory screening apparatus 5, magnetic separator 6; Crusher 1 is provided with barren rock English crucible material import 7, and crusher 1 is provided with transfer roller 8 between sour pond 2, and sour pond 2 is provided with hydrochloric acid import 9, hydrofluoric acid import 10; Acid pond 2 is provided with transfer roller 11 to 3 of rinsing machines, and rinsing machine 3 is provided with water-in 12, water outlet 13, and rinsing machine 3 is provided with transfer roller 14 to 4 of high temperature sintering furnaces; High temperature sintering furnace 4 is provided with power input end mouth 15; High temperature sintering furnace 4 is provided with transfer roller 16 between the crusher 1, and crusher 1 is provided with transfer roller 17 between the vibratory screening apparatus 5, and vibratory screening apparatus 5 is provided with transfer roller 18 between the crusher 1; Vibratory screening apparatus 5 is provided with transfer roller 19 between the magnetic separator 6, and magnetic separator 6 is provided with product outlet 20.
The further technical scheme of the utility model is:
Described whole transfer roller is a rotary conveyor.
The beneficial effect of the utility model is: providing a kind of is the production equipment of primary industry production crucible with fusion obtuse angle silica sand with barren rock English crucible; The advantage of this production equipment is: use general-purpose equipment, little, the no toxic and harmful of investment and liquid discharge; Can mass-produce high-quality quartz crucible with fusion obtuse angle silica sand; The alternative external import glass sand of this silica sand is produced quartz crucible; Both utilization of waste material have produced bigger economic benefit, have produced the huge social benefit again.
Description of drawings:
Like figure is the utility model principle schematic.
Embodiment
Further specify this device of use below in conjunction with accompanying drawing and produce the particular content of crucible with fusion obtuse angle silica sand most preferred embodiment:
1. barren rock English crucible material is sent into crusher 1 fragmentation through 7, be broken for the particulate state that granularity is 5mm-10mm.
2. the barren rock English crucible particle after the fragmentation is sent into sour pond 2 through transfer roller 8; With concentration be the Hydrogen chloride of 10%-15% through 9, concentration is that 47% hydrofluoric acid is through 10; And add sour pond in the ratio of Hydrogen chloride: hydrofluoric acid=4:1; Mixing acid soaked barren rock English crucible material 72-74 hour, and the purpose of pickling is to remove contained dirt settling and oxide compound in the barren rock English crucible particle.
3. after the barren rock English crucible particle after mixing acid in the sour pond 2 being soaked is pulled out, send in the rinsing machine 3 through transfer roller 11, through 12 water sent into 3 pairs of pickling of rinsing machine after barren rock English crucible particle clean; Sewage is discharged through water outlet 13; Barren rock English crucible particle after the deacidification is sent into high temperature sintering furnace 4 through transfer roller 14, and through power input end mouth 15 input electric power, transferring the interior temperature of stove is 1800 ℃-1900 ℃; Fusing time is 11-15 hour, obtains crucible material molten mass.
4. fusing stops to supply power to high temperature sintering furnace after finishing; Be cooled to the solid fusion crucible material that obtains bulk after normal temperature cools off; Earlier after physical shock becomes fritter, send into crusher 1 fragmentation through transfer roller 16, the material after the fragmentation is sent into vibratory screening apparatus 5 through transfer roller 17, after screening; The quartz particles of particle specification more than 4.5mm returns crusher 1 through transfer roller 18 and continues broken; Specification is that the fusion obtuse angle silica sand between 0.075mm-4.5mm is sent into magnetic separator 6 through 19, under magnetic separator 6 internal magnetic field effects, will contain and obtain finished product after silica sand magnetic, that contain metal is removed.
Claims (2)
1. one kind is the production equipment of raw material production fusion obtuse angle silica sand with barren rock English crucible, it is characterized in that: comprise crusher (1), sour pond (2), rinsing machine (3), high temperature sintering furnace (4), vibratory screening apparatus (5), magnetic separator (6); Crusher (1) is provided with barren rock English crucible material import (7); Crusher (1) is provided with transfer roller (8) between sour pond (2); Acid pond (2) is provided with hydrochloric acid import (9), hydrofluoric acid import (10); Acid pond (2) is provided with transfer roller (11) between rinsing machine (3), and rinsing machine (3) is provided with water-in (12), water outlet (13), and rinsing machine (3) is provided with transfer roller (14) between high temperature sintering furnace (4); High temperature sintering furnace (4) is provided with power input end mouth (15); High temperature sintering furnace (4) is provided with transfer roller (16) between the crusher (1), and crusher (1) is provided with transfer roller (17) between the vibratory screening apparatus (5), and vibratory screening apparatus (5) is provided with transfer roller (18) between the crusher (1); Vibratory screening apparatus (5) is provided with transfer roller (19) between the magnetic separator (6), and magnetic separator (6) is provided with product outlet (20).
2. according to claim 1 a kind of be the production equipment of raw material production fusion obtuse angle silica sand with barren rock English crucible, it is characterized in that: described whole transfer rollers are rotary conveyor.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN2012201002053U CN202465292U (en) | 2012-03-16 | 2012-03-16 | Device for producing molten obtuse quartz sand by taking waste quartz crucible as raw material |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN2012201002053U CN202465292U (en) | 2012-03-16 | 2012-03-16 | Device for producing molten obtuse quartz sand by taking waste quartz crucible as raw material |
Publications (1)
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CN202465292U true CN202465292U (en) | 2012-10-03 |
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CN2012201002053U Expired - Fee Related CN202465292U (en) | 2012-03-16 | 2012-03-16 | Device for producing molten obtuse quartz sand by taking waste quartz crucible as raw material |
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103896285A (en) * | 2014-04-21 | 2014-07-02 | 江苏凯达石英有限公司 | Method for preparing high-purity superfine quartz powder through waste quartz crucible |
CN114659367A (en) * | 2022-03-24 | 2022-06-24 | 南城县福鸿高纯硅材料有限公司 | Quartz sand manufacturing device with purification function and method for purifying quartz sand |
-
2012
- 2012-03-16 CN CN2012201002053U patent/CN202465292U/en not_active Expired - Fee Related
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103896285A (en) * | 2014-04-21 | 2014-07-02 | 江苏凯达石英有限公司 | Method for preparing high-purity superfine quartz powder through waste quartz crucible |
CN114659367A (en) * | 2022-03-24 | 2022-06-24 | 南城县福鸿高纯硅材料有限公司 | Quartz sand manufacturing device with purification function and method for purifying quartz sand |
CN114659367B (en) * | 2022-03-24 | 2023-11-24 | 南城县福鸿高纯硅材料有限公司 | Quartz sand manufacturing device with purification function and method for purifying quartz sand |
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Legal Events
Date | Code | Title | Description |
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C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
C17 | Cessation of patent right | ||
CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20121003 Termination date: 20130316 |