CN202460594U - Gas-solid phase catalytic reactor - Google Patents

Gas-solid phase catalytic reactor Download PDF

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Publication number
CN202460594U
CN202460594U CN2012200438493U CN201220043849U CN202460594U CN 202460594 U CN202460594 U CN 202460594U CN 2012200438493 U CN2012200438493 U CN 2012200438493U CN 201220043849 U CN201220043849 U CN 201220043849U CN 202460594 U CN202460594 U CN 202460594U
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CN
China
Prior art keywords
housing
heat exchanger
heat exchange
catalytic reactor
chuck
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Expired - Lifetime
Application number
CN2012200438493U
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Chinese (zh)
Inventor
徐荣良
赵金龙
楼韧
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Hangzhou Linda Chemical Technology Engineering Co ltd
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Hangzhou Linda Chemical Technology Engineering Co ltd
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Priority to CN2012200438493U priority Critical patent/CN202460594U/en
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  • Heat-Exchange Devices With Radiators And Conduit Assemblies (AREA)

Abstract

The utility model discloses a gas-solid phase catalytic reactor comprising a housing and heat exchanging internal parts, wherein an air inlet and an air outlet are formed in the top and the bottom of the housing respectively; the heat exchanging internal parts comprise a plurality of heat exchanging pipes; two ends of each heat exchanging pipe are connected with the inner wall of the housing respectively; jackets are arranged on the outer wall of the housing at the joints; and a central heat exchanging pipe group can be arranged in the internal center of the housing as required. Due to the housing with a flange coupling end socket, the gas-solid phase catalytic reactor also can be used for reconstruction of the conventional reactors with housings. Due to the special compact pipe arranging manner, the gas-solid phase catalytic reactor has the advantages that the heat exchanging capability is high; the structure is reliable; the manufacture is convenient to manufacture and maintain; the investment is low; and the suitability for new construction and reconstruction of the reactors is high.

Description

A kind of gas solid catalytic reactor
Technical field
The utility model relates to technical field of chemical, relates in particular to a kind of reactor that can be used for gas-solid catalysis.
Background technology
Fixed bed catalytic reactor is a kind of consersion unit in chemical industry and petroleum chemical industry extensive use, exothermic reactions such as, preparing methane by synthetic gas synthetic for synthetic ammonia, methyl alcohol, and fixed bed catalytic reactor commonly used has axial flow reactor and radial reactor.Wherein axial flow reactor is simple in structure, and plot ratio is high, but the restriction of fluid passage receiving unit cross section, bed resistance is bigger, simultaneously catalyst strength is had relatively high expectations.Reactor to axial, the bed resistance of radial reactor is little, but if use the water-cooled heat exchange, because of needs resort to coercive measures cooling water is circulated, and distribution of gas tube inside and outside for example being provided with makes capacity utilization little, complex structure, catalyst efficiency is low.
Chinese invention patent ZL93105920.8 discloses a kind of joint production that waits high-pressure type methyl alcohol and ammonia, but complex structure, resistance is bigger.
The utility model content
To the problems referred to above, the purpose of the utility model provides a kind of safety simple in structure, catalyst loading amount gas solid catalytic reactor big, effective, easy to maintenance.
A kind of gas solid catalytic reactor comprises housing and heat exchange internals, and described case top and bottom are respectively equipped with air inlet and gas outlet.Described heat exchange internals comprise some heat exchanger tubes, and the two ends of described heat exchanger tube are connected with inner walls respectively, and the housing outer wall of junction is provided with chuck.Described heat exchanger tube is the bend pipe of bending two ends.
As a kind of preferred; The inside center of described housing is provided with the center set of heat exchange tubes; Described center set of heat exchange tubes comprises upper tube box, lower tube box and some centers heat exchanger tube, and described upper tube box one end is connected with the center heat exchanger tube, and the other end is provided with center set of heat exchange tubes delivery port; Described lower tube box one end is connected with the center heat exchanger tube, and the other end is provided with center set of heat exchange tubes water inlet.The diameter of described upper tube box and lower tube box is less than the diameter of case top opening, and when for example case top was provided with manhole, the diameter of upper tube box and lower tube box made whole center set of heat exchange tubes can independently extract housing out less than people's bore dia.
Described chuck is single or a plurality of, can be along the housing single annular chuck in one week, also can be a plurality of chucks that are evenly distributed along one week of housing.According to the chuck position, be divided into outlet chuck and import chuck.
As a kind of preferred; Described outside also is provided with the shell of flanged connection end socket; Constitute the heat transferring medium chuck between shell and housing; The shell area that is connected with heat exchanger tube upper and lower side indent respectively constitutes import chuck and outlet chuck, and the bottom sealing of outlet chuck makes in the heat transferring medium chuck import chuck region and exports the chuck region and be not communicated with.This situation is applicable to the transformation project to existing band housing reactor, and the shell of existing reactor capable of using is used with shell after making housing and heat exchange internals separately, reduces improvement cost greatly.
When the utility model reactor used, catalyst was seated in space between heat exchanger tube, was that saturation boiling water is as heat transferring medium absorption reaction warm in the heat exchanger tube.Reaction gas gets into the reactor internal reaction from the air inlet on housing top; The reaction back goes out reactor from the gas outlet, bottom; Saturation boiling water gets into the import chuck and is distributed in each heat exchanger tube from the heat transferring medium import, and the reaction gas countercurrent flow that flows between pipe, is pooled to the outlet chuck after the heat exchange again; And export out reactor from heat transferring medium, remove the drum separate vapour.When being provided with the center set of heat exchange tubes in the housing; Most of saturation boiling water gets into each heat exchanger tube from the heat transferring medium import; With the reaction gas countercurrent flow; Fraction saturation boiling water gets into the center set of heat exchange tubes from the center set of heat exchange tubes water inlet of lower housing portion, lower tube box, countercurrent flow after upper tube box, center set of heat exchange tubes delivery port go out reactor and remove drum.
When the utility model reactor is used, can external drum and circulating pump, the heat transferring medium that goes out reactor is sent to the drum separate vapour, again Natural Circulation or get into reactor to the heat transferring medium import through the circulating pump forced circulation.
The utility model device has the following advantages:
1. adopt the stringing mode of special compactness, can arrange more heat exchanger tube, strengthen the heat energy power of moving.
2. the heat exchanger tube bending two ends is welded on the housing; Can solve the flexible problem of heat exchanger tube that thermal stress causes, its structural reliability is increased, be convenient to simultaneously make and maintenance; Only need open external jacket during maintenance gets final product; The center set of heat exchange tubes also can be extracted maintenance separately out, extracts out in the post-reactor and can advance the people, and bigger operating space is arranged.
3. cancel large tubesheet and big flange, reduced investment.
4. be applicable to the newly-built and transformation project of reactor, flexible.
Description of drawings
Fig. 1 is the structure of reactor sketch map of the utility model embodiment 1.
Fig. 2 is the process flow diagram of the reactor of the utility model embodiment 1 when using.
Fig. 3 is the structure of reactor sketch map of the utility model embodiment 2.
Fig. 4 is the process flow diagram of the reactor of the utility model embodiment 2 when using.
Description of reference numerals:
5-center, 1-housing 2-heat exchanger tube 3-air inlet 4-gas outlet set of heat exchange tubes delivery port
Set of heat exchange tubes water inlet 7a-upper tube box 7b-lower tube box 8-center, 6-center heat exchanger tube
The outlet of 9-heat transferring medium chuck 9a-outlet chuck 9b-import chuck 91-heat transferring medium
92-heat transferring medium import 10-manhole 11-catalyst unloads outlet 12-drum
13-circulating pump 14-shell 15-flange
The specific embodiment
Below in conjunction with accompanying drawing and embodiment the detailed description of carrying out to the utility model.
Embodiment 1
Gas solid catalytic reactor as shown in Figure 1; Comprise housing 1 and heat exchange internals; Case top is provided with air inlet 3 and manhole 10; Housing bottom is provided with gas outlet 4 and unloads outlet 11 with catalyst, and described heat exchange internals comprise the heat exchanger tube 2 and center set of heat exchange tubes of some bending two ends, and the two ends of described heat exchanger tube 2 are connected with lower inner wall with the housing upper inside wall respectively; Be respectively equipped with outlet chuck 9a and import chuck 9b on the housing outer wall of junction; Described outlet chuck 9a and import chuck 9b are the single annular chuck that is provided with around barrel, and outlet chuck 9a is provided with the heat transferring medium outlet 91 of two symmetrical distributions, and import chuck 9b is provided with the heat transferring medium import 92 of two symmetrical distributions.
Described center set of heat exchange tubes comprises upper tube box 7a, lower tube box 7b and some centers heat exchanger tube 8, and described upper tube box 7a one end is connected with center heat exchanger tube 8, and the other end is provided with center set of heat exchange tubes delivery port 5; Described lower tube box 7b one end is connected with center heat exchanger tube 8, and the other end is provided with center set of heat exchange tubes water inlet 6.The diameter of described upper tube box 7a and lower tube box 7b unloads the diameter of outlet 11 less than manhole on the housing 1 10 and catalyst, and the center set of heat exchange tubes of making can the whole independent housing of extracting out.
When reactor used, catalyst was seated in heat exchanger tube 2 gaps, was that saturation boiling water is as cooling medium absorption reaction warm in the heat exchanger tube 2.As shown in Figure 2, reaction gas gets into the reactor internal reaction from air inlet 3, and the reaction back goes out reactor from gas outlet, bottom 4; Saturation boiling water major part gets into import chuck 9b and is distributed to each heat exchanger tube 2 from heat transferring medium import 92; And the reaction gas countercurrent flow that flows between pipe is pooled to outlet chuck 9a again after the heat exchange, and goes out reactor from heat transferring medium outlet 91; Remove the drum separate vapour; Set of heat exchange tubes water inlet 6 gets into lower tube box 7b, center heat exchanger tube 8 to fraction saturation boiling water successively from the center, and goes out upper tube box 7b behind the reaction gas countercurrent flow, and set of heat exchange tubes delivery port 5 goes out reactor and removes drum 12 from the center.
Embodiment 2
Gas solid catalytic reactor as shown in Figure 3 comprises the shell 14 of housing 1, heat exchange internals and band upper cover 16, and described upper cover 16 is connected with shell 14 usefulness flanges 15.Constitute heat transferring medium chuck 9 between described housing 1 and shell 14, the upper cover 16, reactor head is provided with air inlet 3, heat transferring medium outlet 91 and manhole 10, and reactor bottom is provided with gas outlet 4, heat transferring medium import 92 and catalyst and unloads outlet 11.Described heat exchange internals comprise the heat exchanger tube 2 of some bending two ends; The two ends of described heat exchanger tube 2 are connected with lower inner wall with the housing upper inside wall respectively; The housing of junction concaves; Form outlet chuck 9a and import chuck 9b respectively, the bottom sealing of outlet chuck 9a makes in the heat transferring medium chuck 9 import chuck 9b region and exports chuck 9a region and be not communicated with.The reactor of this version can be used for the old tower transformation of the end socket and the shell of flanged connection.
Technological process when this reactor uses is as shown in Figure 4, and catalyst is seated in heat exchanger tube 2 gaps, and is hot as the heat transferring medium absorption reaction with saturation boiling water in the heat exchanger tube 2.Reaction gas gets into the reactor internal reaction from air inlet 3; The reaction back goes out reactor from gas outlet, bottom 4; Saturation boiling water gets into from heat transferring medium import 92, and distributing through import chuck 9b enters into each heat exchanger tube 2, and the reaction gas countercurrent flow that flows between pipe; Go out reactor through outlet chuck 9b from heat transferring medium outlet 91 again after the heat exchange, remove drum 12 separate vapours.
The upper cover 16 that the removable flange 15 of present embodiment connects is extracted the internals maintenance separately out, so need not to establish the center set of heat exchange tubes.

Claims (5)

1. gas solid catalytic reactor; Comprise housing and heat exchange internals; Described case top and bottom are respectively equipped with air inlet and gas outlet, and described heat exchange internals comprise some heat exchanger tubes, it is characterized in that: the bending two ends of described heat exchanger tube; Described heat exchanger tube two ends are connected with inner walls respectively, and the housing outer wall of said junction is provided with chuck.
2. gas solid catalytic reactor as claimed in claim 1 is characterized in that: the inside center of described housing is provided with the center set of heat exchange tubes.
3. gas solid catalytic reactor as claimed in claim 2; It is characterized in that: described center set of heat exchange tubes comprises upper tube box, lower tube box and some centers heat exchanger tube; Described upper tube box one end is connected with the center heat exchanger tube, and the other end is provided with center set of heat exchange tubes delivery port; Described lower tube box one end is connected with the center heat exchanger tube, and the other end is provided with center set of heat exchange tubes water inlet.
4. like the arbitrary described gas solid catalytic reactor of claim 1~3, it is characterized in that: described chuck is single or a plurality of.
5. gas solid catalytic reactor as claimed in claim 1 is characterized in that: described outside is provided with shell, constitutes the heat transferring medium chuck between described shell and the housing.
CN2012200438493U 2012-02-10 2012-02-10 Gas-solid phase catalytic reactor Expired - Lifetime CN202460594U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN2012200438493U CN202460594U (en) 2012-02-10 2012-02-10 Gas-solid phase catalytic reactor

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Application Number Priority Date Filing Date Title
CN2012200438493U CN202460594U (en) 2012-02-10 2012-02-10 Gas-solid phase catalytic reactor

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CN202460594U true CN202460594U (en) 2012-10-03

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103240035A (en) * 2012-02-10 2013-08-14 杭州林达化工技术工程有限公司 Gas-solid phase catalytic reactor

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103240035A (en) * 2012-02-10 2013-08-14 杭州林达化工技术工程有限公司 Gas-solid phase catalytic reactor

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Granted publication date: 20121003