CN202447062U - Multifunctional fiber liquid membrane mass-transfer separation reactor - Google Patents

Multifunctional fiber liquid membrane mass-transfer separation reactor Download PDF

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Publication number
CN202447062U
CN202447062U CN2012200116837U CN201220011683U CN202447062U CN 202447062 U CN202447062 U CN 202447062U CN 2012200116837 U CN2012200116837 U CN 2012200116837U CN 201220011683 U CN201220011683 U CN 201220011683U CN 202447062 U CN202447062 U CN 202447062U
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CN
China
Prior art keywords
urceolus
outer barrel
tubulation
reactor
knockout drum
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
CN2012200116837U
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Chinese (zh)
Inventor
夏桂友
祁永生
徐振华
聂通元
王铭
喻武钢
童仁可
贺立明
施景
蔡喜洋
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NINGBO ZHONGYI PETROCHEMICAL TECHNOLOGY Co Ltd
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NINGBO ZHONGYI PETROCHEMICAL TECHNOLOGY Co Ltd
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Priority to CN2012200116837U priority Critical patent/CN202447062U/en
Application granted granted Critical
Publication of CN202447062U publication Critical patent/CN202447062U/en
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Abstract

The utility model relates to a multifunctional fiber liquid membrane mass-transfer separation reactor, which comprises a separation tank and an outer barrel arranged on the separation tank, wherein a material inlet is arranged on the top end of the outer barrel; an alkali liquor inlet is arranged on one side of the top part of the outer barrel; the bottom end of the outer barrel stretches into the separation tank; a plurality of conical tubes are uniformly distributed in the outer barrel; a tube fixing slope is arranged on a part, which is close to the top part, on an inner wall of the outer barrel; the conical tubes penetrate through the tube fixing slope; and a discharge pipeline is arranged on a connecting part of the bottommost end of the tube fixing slope and the inner wall of the outer barrel, and is communicated with a discharging port. The multifunctional fiber liquid membrane mass-transfer separation reactor has the beneficial effects that large grained impurities easily causing blockage subside on the bottom part of the tube fixing slope due to self-gravity; and the discharging pipeline on the bottom part of the slope is utilized to clean the impurities regularly, so that the large grained impurities in a reaction medium and impurities such as rust generated by corrosion of an inner wall of the reactor can be effectively prevented from entering the tubes of the fiber liquid membrane mass-transfer separation reactor.

Description

Multifunctional fibre liquid film mass transfer separate reactor
Technical field
The utility model relates to a kind of multifunctional fibre liquid film mass transfer separate reactor.
Background technology
Fiber liquid film mass transfer reaction device can be used for liquid--the various reactions between the liquid medium of industries such as chemical industry, metallurgy, papermaking, environmental protection, like extraction, catalysis, course of reaction such as remove.Traditional fiber liquid film mass transfer reaction device at present petrochemical refining's industry product use aspect refining more, like projects such as the depriving hydrogen sulphide of liquefied gas, gasoline, naphtha etc., removal of mercaptans.At present this piece technology project at home mainly is that the tame unit with domestic a few family units and the U.S. is main, and reaction mechanism is the same basically with the reactor moulding, is exactly reactor internal components existence difference more or less; But all having a common shortcoming, is exactly the problem of reactor plugs, and one of reactor plugs is the obstruction that the solid large granular impurity that carries in the reaction medium causes; One is the obstruction that reactant or reaction product cause in the inside reactor crystallization; Thereby cause the fiber liquid film mass transfer reaction device cycle of operation short,, cause parking maintenance often along with the increase of reactor pressure decrease; A lot of unfavorable factors such as enterprise energy consumption is big, and production capacity is low.
The utility model content
The purpose of the utility model provides a kind of multifunctional fibre liquid film mass transfer separate reactor, to overcome the above-mentioned deficiency that present prior art exists.
The purpose of the utility model is to realize through following technical scheme:
A kind of multifunctional fibre liquid film mass transfer separate reactor comprises knockout drum and is arranged at the urceolus on the knockout drum that one end of said knockout drum end face is provided with material outlet; One end of knockout drum bottom surface is provided with the alkali lye outlet, and the top of urceolus is provided with material inlet, and a side at urceolus top is provided with the alkali lye import; Knockout drum inside is stretched in the bottom of urceolus; The inside of urceolus is the some taper tubulations of distribution evenly, are provided with tubulation fixed ramp face near the place, top on the outer tube inner wall, and some taper tubulations pass tubulation fixed ramp face; The lowermost end of tubulation fixed ramp face and the inwall junction of urceolus are provided with blowdown pipeline, and blowdown pipeline is communicated with sewage draining exit.
The set inside of said taper tubulation has some stainless steel wires.
Said tubulation fixed ramp face is arranged at the below of alkali lye import.
Angle between said tubulation fixed ramp face and the outer tube inner wall is the 70-80 degree.
The beneficial effect of the utility model is:
1, utilization is prone to cause that the large granular impurity that the utility model stops up is deposited in fixedly tubulation slope bottom of the utility model internals by self gravitation; Utilize the blowdown pipeline of slope bottom regularly the impurity cleaning to be got rid of again; Can prevent effectively that the impurity such as iron rust that the corrosion of granule foreign big in the reaction medium and reactor wall produces from entering into fiber liquid film reactor tubulation; Thereby effectively reduced the obstruction of fiber liquid film mass transfer reaction device; Finely solved that the pressure drop increase that reactor causes because of obstruction, treating capacity descend, energy consumption increases, the equipment cycle of operation shortens etc. and to cause the equipment parking maintenance frequent, the shortcoming that loss of enterprises is big.
2, the utility model internals tubulation makes stainless concentric reducing conical pipe into by traditional cylinder stainless steel tube; Making reactor tubulation internals is that a tubulation internals space constantly becomes big stainless steel wire filling environment from the top to the bottom; The closer to the bottom; Stainless steel wire in the tubulation is just fluffy more, and the impurity of the stainless steel wire surface attachment in the tubulation is easy to be with from fiber liquid film mass transfer reaction device with flowing of reaction medium, has well solved traditional fibre liquid film mass transfer reaction device tubulation internals and has been difficult for breaking away from the device blockage of accumulating over a long period and causing because of the stainless steel wire surface that the reaction medium crystal adheres to; Thereby effectively reduced the pressure drop of equipment; Improved the cycle of operation of equipment, reduced energy consumption, the production capacity of increase.
Description of drawings
According to accompanying drawing the utility model is done further explain below.
Fig. 1 is the structural representation of the described multifunctional fibre liquid film of the utility model embodiment mass transfer separate reactor;
Fig. 2 is the structural representation of taper tubulation among Fig. 1;
Fig. 3 is the structural representation of tubulation fixed ramp face among Fig. 1.
Among the figure:
1, knockout drum; 2, urceolus; 3, material outlet; 4, alkali lye outlet; 5, material inlet; 6, alkali lye import; 7, taper tubulation; 8, tubulation fixed ramp face; 9, blowdown pipeline; 10, sewage draining exit; 11, stainless steel wire.
The specific embodiment
Shown in Fig. 1-3, the described a kind of multifunctional fibre liquid film mass transfer separate reactor of the utility model embodiment comprises knockout drum 1 and is arranged at the urceolus 2 on the knockout drum 1; One end of said knockout drum 1 end face is provided with material outlet 3; One end of knockout drum 1 bottom surface is provided with alkali lye outlet 4, and the top of urceolus 2 is provided with material inlet 5, and a side at urceolus 2 tops is provided with alkali lye import 6; Knockout drum 1 inside is stretched in the bottom of urceolus 2; The inside of urceolus 2 is the some taper tubulations 7 of distribution evenly, are provided with tubulation fixed ramp face 8 near the place, top on urceolus 2 inwalls, and some taper tubulations 7 pass tubulation fixed ramp face 8; The lowermost end of tubulation fixed ramp face 8 and the inwall junction of urceolus 2 are provided with blowdown pipeline 9, and blowdown pipeline 9 is communicated with sewage draining exit 10; The set inside of said taper tubulation 7 has some stainless steel wires 11; Said tubulation fixed ramp face 8 is arranged at the below of alkali lye import 6; Angle between said tubulation fixed ramp face 8 and urceolus 2 inwalls is the 70-80 degree.
The utility model makes traditional fiber liquid film mass transfer reaction device internals tubulation horizontal plane into tubulation fixed ramp face 8; Tubulation fixed ramp face 8 parts are extended at taper tubulation 7 tops; Align with urceolus 2 tops; Form a large granular impurity settling zone between tubulation fixed ramp face 8 and the urceolus 2 thereby make, make its taper tubulation 7 that is not easy to enter into the utility model, reduce the phenomenon that bulky grain stops up reactor.In addition, tubulation fixed ramp face 8 is connected the regularly blowdown of blowdown pipeline 9 that bottommost increases newly, the large granular impurity in the cleaning urceolus 2 with urceolus 2.Again fiber liquid film mass transfer reaction device internals tubulation is made into the taper tubulation 7 of stainless concentric reducing by traditional cylindrical stainless steel tube; Making taper tubulation 7 is that an internals space constantly becomes big stainless steel wire filling environment from the top to the bottom; The closer to the bottom; Stainless steel wire in the taper tubulation 7 is just fluffy more, and the impurity of the stainless steel wire surface attachment in the taper tubulation 7 is just easier to be with from the utility model with the reaction medium that flows.
The utility model is not limited to above-mentioned preferred forms; Anyone can draw other various forms of products under the enlightenment of the utility model; No matter but on its shape or structure, do any variation; Every have identical with a application or akin technical scheme, all drops within the protection domain of the utility model.

Claims (4)

1. multifunctional fibre liquid film mass transfer separate reactor; Comprise knockout drum (1) and be arranged at the urceolus (2) on the knockout drum (1); One end of said knockout drum (1) end face is provided with material outlet (3); One end of knockout drum (1) bottom surface is provided with alkali lye outlet (4), and it is characterized in that: the top of urceolus (2) is provided with material inlet (5), and a side at urceolus (2) top is provided with alkali lye import (6); Knockout drum (1) inside is stretched in the bottom of urceolus (2); The inside of urceolus (2) is evenly distributed with some taper tubulations (7), is provided with tubulation fixed ramp face (8) near the place, top on urceolus (2) inwall, and described some taper tubulations (7) pass tubulation fixed ramp face (8); The inwall junction of the lowermost end of tubulation fixed ramp face (8) and urceolus (2) is provided with blowdown pipeline (9), and blowdown pipeline (9) is communicated with sewage draining exit (10).
2. multifunctional fibre liquid film mass transfer separate reactor according to claim 1, it is characterized in that: the set inside of said taper tubulation (7) has some stainless steel wires (11).
3. multifunctional fibre liquid film mass transfer separate reactor according to claim 2, it is characterized in that: said tubulation fixed ramp face (8) is arranged at the below of alkali lye import (6).
4. according to each described multifunctional fibre liquid film mass transfer separate reactor of claim 1-3, it is characterized in that: the angle between said tubulation fixed ramp face (8) and urceolus (2) inwall is the 70-80 degree.
CN2012200116837U 2012-01-11 2012-01-11 Multifunctional fiber liquid membrane mass-transfer separation reactor Expired - Lifetime CN202447062U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN2012200116837U CN202447062U (en) 2012-01-11 2012-01-11 Multifunctional fiber liquid membrane mass-transfer separation reactor

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN2012200116837U CN202447062U (en) 2012-01-11 2012-01-11 Multifunctional fiber liquid membrane mass-transfer separation reactor

Publications (1)

Publication Number Publication Date
CN202447062U true CN202447062U (en) 2012-09-26

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Family Applications (1)

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CN2012200116837U Expired - Lifetime CN202447062U (en) 2012-01-11 2012-01-11 Multifunctional fiber liquid membrane mass-transfer separation reactor

Country Status (1)

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CN (1) CN202447062U (en)

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C56 Change in the name or address of the patentee
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Address after: 315040, Zhejiang, Ningbo province National hi tech Zone Lingyun road 1177 Lingyun Industrial Park, building 10, north 2 floor

Patentee after: Ningbo Zhongyi Petrochemical Technology Co., Ltd.

Address before: 1618, room 1558, 315040 Jiangnan Road, Ningbo science and Technology Park, Zhejiang, China

Patentee before: Ningbo Zhongyi Petrochemical Technology Co., Ltd.

PE01 Entry into force of the registration of the contract for pledge of patent right

Denomination of utility model: Multifunctional fiber liquid membrane mass-transfer separation reactor

Effective date of registration: 20130809

Granted publication date: 20120926

Pledgee: China Co truction Bank Corp Ningbo national hi tech Zone sub branch

Pledgor: Ningbo Zhongyi Petrochemical Technology Co., Ltd.

Registration number: 2013990000564

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C56 Change in the name or address of the patentee
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Address after: 315040, 1, 2 North Zone, 10 Lingyun Road, 1177 hi tech Zone, Zhejiang, Ningbo

Patentee after: NINGBO ZHONGYI PETROCHEMICAL TECHNOLOGY CO., LTD.

Address before: 315040, Zhejiang, Ningbo province National hi tech Zone Lingyun road 1177 Lingyun Industrial Park, building 10, north 2 floor

Patentee before: Ningbo Zhongyi Petrochemical Technology Co., Ltd.

C56 Change in the name or address of the patentee
CP02 Change in the address of a patent holder

Address after: 315040, Zhejiang, Ningbo province National hi tech Zone Lingyun road 1177 Lingyun Industrial Park, building 10, north 2 floor

Patentee after: NINGBO ZHONGYI PETROCHEMICAL TECHNOLOGY CO., LTD.

Address before: 315040, 1, 2 North Zone, 10 Lingyun Road, 1177 hi tech Zone, Zhejiang, Ningbo

Patentee before: NINGBO ZHONGYI PETROCHEMICAL TECHNOLOGY CO., LTD.

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Registration number: 2013990000564

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