CN202440321U - Preparation device for polymeric aluminum chloride with high content of A113 - Google Patents
Preparation device for polymeric aluminum chloride with high content of A113 Download PDFInfo
- Publication number
- CN202440321U CN202440321U CN2012200672999U CN201220067299U CN202440321U CN 202440321 U CN202440321 U CN 202440321U CN 2012200672999 U CN2012200672999 U CN 2012200672999U CN 201220067299 U CN201220067299 U CN 201220067299U CN 202440321 U CN202440321 U CN 202440321U
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- CN
- China
- Prior art keywords
- peristaltic pump
- water bath
- thermal
- thermostat water
- insulation coat
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
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- Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
Abstract
The utility model relates to a preparation device for polymeric aluminum chloride with high content of A113, which comprises an iron-frame platform, a reactor, a heat-preservation jacket, a mixer, a peristaltic pump and a thermostat water bath. The reactor is arranged in the heat-preservation jacket, a mixing propeller part of the mixer goes deep into the reactor, a motor part of the mixer is arranged on the upper end of the reactor, an upper opening of the heat-preservation jacket goes deep into a position below the liquid surface of the thermostat water bath through a PVC (Poly Vinyl Chloride) hose, a lower opening of the heat-preservation jacket is connected with an effluent end of the peristaltic pump through a PVC pipe, and a water inlet end of the peristaltic pump goes deep into the position below the liquid surface of the thermostat water bath through the PVC hose. The preparation device has the advantages of reasonable structure, convenience in operation, stable working performance and simpleness in maintenance.
Description
Technical field
The utility model relates to a kind of high Al that under the condition of high temperature, prepares
13The device of content Poly aluminum Chloride (PAC).
Background technology
Coagulating agent is one of core of coagulation technology, and the coagulating agent form is formed, physicochemical characteristic is the key point of decision coagulation process high efficiency.In recent decades, Poly aluminum Chloride (PAC) just progressively becomes the main product of inorganic polymer flocculant, wherein Al
13Form is considered to one of optimal modality of PACl.At present, use the polymerization chlorating Al of traditional method preparation
13Content generally lower (being lower than 30%).Therefore, how to prepare high Al
13Content (being higher than 70%) Poly aluminum Chloride (PAC) becomes the problem that water treatment agent manufacturing enterprise and researcher face jointly.
Summary of the invention
It is a kind of rational in infrastructure, easy to operate, stable that the purpose of the utility model is to provide, and safeguards simple high Al
13The preparation facilities of content Poly aluminum Chloride (PAC).
The high Al of the utility model
13The preparation facilities of content Poly aluminum Chloride (PAC) is made up of iron stand 1, reactor drum 2, thermal-insulation coat 3, whisking appliance 4, peristaltic pump 5, thermostat water bath 6.Its structure is as shown in Figure 1; Thermal-insulation coat 3 and peristaltic pump 4 are positioned over the lower plane of iron stand 1, and reactor drum 2 places in the thermal-insulation coat 3, and whisking appliance 4 stirring rakes partly go deep in the reactor drum 2; Whisking appliance 4 motor section are placed in reactor drum 2 upper ends also through iron stand 1 admittedly; The upper shed of thermal-insulation coat 3 is goed deep under thermostat water bath 6 liquid levels through the PVC flexible pipe, and the lower opening of thermal-insulation coat 3 is connected with peristaltic pump 5 water sides through pvc pipe, and peristaltic pump 5 feed-water ends go deep under thermostat water bath 6 liquid levels through the PVC flexible pipe.
The working process of the utility model is following:
Confirm that all parts connect as requested.At first in thermostat water bath 6, add a certain amount of water, open thermostat water bath 6, and design temperature.After the temperature of thermostat water bath 6 reaches assigned temperature, open peristaltic pump 5 and make the water in the thermostat water bath 6 thermal-insulation coat 3 in, realize circulating.Add after a certain amount of Poly aluminum Chloride (PAC) prepares raw material at reactor drum 2, turn on agitator 4 (rotating speed generally is set in 150-200 rev/min) makes entire reaction course maintain high temperature and has under the state of stirring and carries out.Behind the end of processing to be prepared (the about 1-2 of this process hour; By preparation amount decision once); Close whisking appliance 4 and stop to stir, close peristaltic pump 5 and stop constant temperature, in thermal-insulation coat 3, take out reactor drum 2 finished product the reactor drum 2 is transferred to other containers preservations with thermostat water bath 6.
The beneficial effect of the utility model is to be applicable to high Al on a small scale
13The production of content Poly aluminum Chloride (PAC), rational in infrastructure, easy to operate, stable, safeguard simple.
Description of drawings
Fig. 1 is the structural diagrams of the utility model.
Label among Fig. 1: 1 is iron stand, and 2 is reactor drum, and 3 is thermal-insulation coat, and 4 is whisking appliance, and 5 is peristaltic pump, and 6 is thermostat water bath.
Embodiment
Combine accompanying drawing to further specify the utility model through embodiment below.
Embodiment: reactor drum 2 is a 1L standard beaker, and thermal-insulation coat 3 is 2L standard synthetic glass beaker and process processing, opens two openings up and down, and whisking appliance 4 is portable coagulation experiment device stirring-head.Thermal-insulation coat 3 and peristaltic pump 4 are positioned over the lower plane of iron stand 1; Reactor drum 2 places in the thermal-insulation coat 3; Whisking appliance 4 stirring rakes partly go deep in the reactor drum 2, and whisking appliance 4 motor section are placed in reactor drum 2 upper ends also through iron stand 1 admittedly, and the upper shed of thermal-insulation coat 3 is goed deep under thermostat water bath 6 liquid levels through the PVC flexible pipe; The lower opening of thermal-insulation coat 3 is connected with peristaltic pump 5 water sides through pvc pipe, and peristaltic pump 5 feed-water ends go deep under thermostat water bath 6 liquid levels through the PVC flexible pipe.
Each assembly connect the back by, at first thermostat water bath 6 in, add a certain amount of water, unlatching thermostat water bath 6, and design temperature is 90 ℃.After the temperature of thermostat water bath 6 reaches, open peristaltic pump 5 and make the water in the thermostat water bath 6 thermal-insulation coat 3 in, realize circulating.After reactor drum 2 adds the preparation raw materials, turn on agitator 4, setting rotating speed is 150 rev/mins, makes entire reaction course maintain high temperature and have under the state of stirring to carry out.After 2 hours, the preparation end of processing is closed whisking appliance 4 and is stopped to stir, and closes peristaltic pump 5 and stops constant temperature with thermostat water bath 6, from thermal-insulation coat 3 interior taking-up reactor drums 2 finished product the reactor drum 2 is transferred to other containers and preserves.
Claims (1)
1. high Al
13The preparation facilities of content Poly aluminum Chloride (PAC); It is characterized in that: this preparation facilities is made up of iron stand (1), reactor drum (2), thermal-insulation coat (3), whisking appliance (4), peristaltic pump (5), thermostat water bath (6); Wherein thermal-insulation coat (3) and peristaltic pump (4) are positioned over the lower plane of iron stand (1); Reactor drum (2) places in the thermal-insulation coat (3); Whisking appliance (4) stirring rake partly gos deep in the reactor drum (2), whisking appliance (4) motor section reactor drum (2) upper end and fixing that is placed in through iron stand (1), and the upper shed of thermal-insulation coat (3) is goed deep under thermostat water bath (6) liquid level through the PVC flexible pipe; The lower opening of thermal-insulation coat (3) is connected with peristaltic pump (5) water side through pvc pipe, and peristaltic pump (5) feed-water end gos deep under thermostat water bath (6) liquid level through pvc pipe.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2012200672999U CN202440321U (en) | 2012-02-28 | 2012-02-28 | Preparation device for polymeric aluminum chloride with high content of A113 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2012200672999U CN202440321U (en) | 2012-02-28 | 2012-02-28 | Preparation device for polymeric aluminum chloride with high content of A113 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN202440321U true CN202440321U (en) | 2012-09-19 |
Family
ID=46821775
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2012200672999U Expired - Lifetime CN202440321U (en) | 2012-02-28 | 2012-02-28 | Preparation device for polymeric aluminum chloride with high content of A113 |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN202440321U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111659482A (en) * | 2020-06-11 | 2020-09-15 | 南昌航空大学 | Device for quickly and accurately controlling temperature of quartz microbalance flow cell and construction method thereof |
-
2012
- 2012-02-28 CN CN2012200672999U patent/CN202440321U/en not_active Expired - Lifetime
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111659482A (en) * | 2020-06-11 | 2020-09-15 | 南昌航空大学 | Device for quickly and accurately controlling temperature of quartz microbalance flow cell and construction method thereof |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CX01 | Expiry of patent term | ||
| CX01 | Expiry of patent term |
Granted publication date: 20120919 |