CN202412518U - Equipment for producing ultrathin talcum powder polypropylene filling master batch - Google Patents

Equipment for producing ultrathin talcum powder polypropylene filling master batch Download PDF

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Publication number
CN202412518U
CN202412518U CN201220037428XU CN201220037428U CN202412518U CN 202412518 U CN202412518 U CN 202412518U CN 201220037428X U CN201220037428X U CN 201220037428XU CN 201220037428 U CN201220037428 U CN 201220037428U CN 202412518 U CN202412518 U CN 202412518U
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China
Prior art keywords
equipment
continuous mixer
talcum powder
machine
rotor continuous
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Expired - Fee Related
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CN201220037428XU
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Chinese (zh)
Inventor
唐宇航
黄方元
叶南飚
王大中
钱永红
宁凯军
蔡彤旻
刘奇祥
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Kingfa Science and Technology Co Ltd
Shanghai Kingfa Science and Technology Co Ltd
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Kingfa Science and Technology Co Ltd
Shanghai Kingfa Science and Technology Co Ltd
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Priority to CN201220037428XU priority Critical patent/CN202412518U/en
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Publication of CN202412518U publication Critical patent/CN202412518U/en
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Abstract

The utility model discloses equipment for producing ultrathin talcum powder polypropylene filling master batch. The equipment comprises a mixing machine, a feeding machine, a double-rotator continuous mixing mill, a single-screw extruder and a die surface hot cutting granulating machine, wherein the mixing machine is arranged above the feeding machine; the material outlet of the feeding machine is connected with the material inlet of the double-rotator continuous mixing mill; the material outlet of the double-rotator continuous mixing mill is connected with the material inlet of the single-screw extruder; and the material outlet of the single-screw extruder is connected with the material inlet of the die surface hot cutting granulating machine. According to the utility model, a proper raw material formula and a novel double-rotator continuous mixing and granulating machine are adopted so as to ensure continuous mixing and granulating; and due to use of the double-rotator continuous mixing and granulating equipment, the volume and the weight (the total weight of the equipment models with the same output is about half of that of an internal mixer) of the equipment are greatly reduced, and the power consumption of the equipment is greatly reduced. In addition, the double-rotator continuous mixing and granulating equipment disclosed by the utility model is high in automation degree, simple to operate and relatively low in use and maintenance costs.

Description

A kind of equipment that is used to produce superfine talcum powder polypropylene filling master batch
Technical field
The utility model relates to the superfine talcum powder polypropylene and fills the master batch preparing technical field, particularly a kind of equipment that is used to produce superfine talcum powder polypropylene filling master batch.
Background technology
Talcum powder is cheap inorganic filler commonly used in the plastics industry, and it can improve the dimensional stability of rigidity, modulus and the goods thereof of material effectively, and its cost is significantly reduced; Therefore, talcum powder extensively is used in the modifying plastics industry.But, owing to the bulk density of talcum powder especially superfine talcum powder is little; In the modifying plastics production process, very easily produce dust, pollute workshop, have a strong impact on the healthy of Manufacturing Worker.In addition, because talcous bulk density is little, when modified plastics adopted the processing mode of screw extruder to add talcum powder, the difficult feeding of material had a strong impact on production efficiency.Therefore, how to prepare the high filled polypropylene master batch of superfine talcum powder, for solving dust pollution, seeming very crucial enhancing productivity.
When producing talcum powder filling PP master batch, adopt following two kinds of methods at present in the industry usually: one, elder generation is mixing in banbury; Adding screw extruder again extrudes; Form through the fervent granulation mode of die face at last; Two, through high-speed mixer former material is mixed to more than 100 ℃ earlier, makes material become little lumps; Extrude through double screw extruder again; Finally form through the fervent granulation of water ring die face.
Open day is that the Chinese utility model patent of CN101955604 A discloses " a kind of polyolefin-based nanoscale talcum powder functional agglomerate and manufacturing approach and equipment " for 2011.1.26, publication number.Mentioning method in the literary composition is present typical preparation method: adopt mixer mixing earlier; Adding screw extruder again extrudes; The preparation method who forms through the fervent granulation mode of die face at last.The work characteristics of banbury is: in the banburying chamber, add a certain amount of material, material is the mixing one long period in the banburying chamber, all is delivered to screw extruder then and carries out granulation; Then, pour certain material into toward the banburying chamber again, so successively circulation.In mixing, the process of carrying, material is in a kind of discontinuous state; In addition, because that material is in the mixing chamber of sealing is mixing, the plastifying state of material, fusion time are difficult to accurate assurance.Therefore, the automaticity of whole production line is low, and personnel labor is big, and production efficiency is low.
Open day is that the Chinese utility model patent of CN102040774A discloses " a kind of polypropylene is filled master batch and preparation method thereof " for 2011.5.4, publication number; Mention high-speed mixer in the literary composition and add prepared in twin-screw extruder polypropylene filling master batch: function powder is mainly powdered whiting and blanc fixe; Its bulk density surpasses 1.0g/cm3 (bulk density of superfine talcum powder is less than 0.3g/ cm3), and powdered whiting content is no more than 70%; Therefore, in the production process of the high filling of superfine talcum powder PP, powder is difficult to coated by matrix resin; In addition, adopt high-speed mixer that the raw material premixed time is surpassed 15min, greatly reduce the batch mixing efficient of high-speed mixer.
The Chinese utility model patent of CN 1966562A.Adopt high-speed mixer to add the preparation method of double screw extruder in the literary composition: the mixed function powder agglomerate of 25 ~ 50 parts of calcium carbonate contents, 5 ~ 30 parts of superfine talcum powders; Because the bulk density of calcium carbonate is three times of bulk density of superfine talcum powder; Therefore, the coating problem of such powder basically can be through the mixing solution of twin-screw.But before getting into double screw extruder, this former material need be through high-speed mixer with pre-composition high-speed stirred to 100 ℃ ~ 130 ℃.There are two defectives in such processing technology: 1) mixture temperature reaches the mixing time that needs more than 100 ℃ long (maybe needing heating); 2), and the partial material fusing point is arranged in the middle of the raw material of this series products about 100 ℃ owing to the temperature of high-speed mixer is controlled than difficult; Therefore, there is the agglomerating danger of caking in material, and the normal discharging of high-speed mixer is had a strong impact on.
The day for announcing is that 2011.10.12, notification number are that the Chinese patent of CN101792536 A discloses " a kind of preparation method of carrier-free talcum powder master batch ".Adopt volatile alcohol or ketone diluent in the literary composition, at first bonding agent is diluted to more than 10 times; Bonding agent after will diluting again and talcum powder premixed by a certain percentage; At last at normal temperatures through the extruder extruding pelletization.There is following defective in the method: 1) diluent is difficult to reclaim, and is prone to cause environmental pollution and physical waste, and since the ratio that institute adds diluent up to 15% ~ 35%, follow-up stoving process is difficulty comparatively, the increase manufacturing cost; 2) adopt this processing method resultant that the hardness of particle is very low, in follow-up transportation and use, cause the secondary dust pollution easily; 3) use this extruder equipment pelletizing, make that the product of being cut is different in size, the outward appearance of whole particle is very ugly, and the client is difficult to accept.
In sum, there are above-mentioned all deficiencies in the preparation method and the equipment of the master batch of polypropylene filling at present.
The utility model content
The utility model patent technical problem to be solved provides a kind of manufacturing equipment of the superfine talcum powder filled polypropylene master batch of raising the efficiency of cutting down the consumption of energy.
For solving the problems of the technologies described above, the technical scheme that the utility model adopts is: a kind of being used to produced the equipment that the superfine talcum powder polypropylene is filled master batch, comprises the fervent comminutor of mixer, feeding machine, two-rotor continuous mixer, single screw extrusion machine and die face; Said mixer is located at the top of feeding machine; The discharging opening of said feeding machine is connected with the charging aperture of two-rotor continuous mixer; The discharging opening of said two-rotor continuous mixer is connected with the charging aperture of single screw extrusion machine, and the discharging opening of said single screw extrusion machine is connected with the charging aperture of the fervent comminutor of die face.
Preferably; Said two-rotor continuous mixer comprises first two-rotor continuous mixer, second two-rotor continuous mixer; The charging aperture of said two-rotor continuous mixer is connected with first two-rotor continuous mixer; Said first two-rotor continuous mixer, second two-rotor continuous mixer are connected, and said second two-rotor continuous mixer is connected with the discharging opening of two-rotor continuous mixer.
Preferably, be provided with storage bin between the charging aperture of said two-rotor continuous mixer and first two-rotor continuous mixer.
Preferably, the charging aperture of said two-rotor continuous mixer is a funnel-form.
Preferably, said mixer comprises tilting discharging mouth, and said tilting discharging mouth places the top of feeding bin.
Preferably, said feeding machine comprises feeding bin, and said feeding bin is a funnel-form.
Preferably, said feeding machine also comprises horizontal feeding machine and vertical feeding machine, and the charging aperture of said horizontal feeding machine is connected with the discharging opening of feeding bin, and the discharging opening of said horizontal feeding machine is connected with the charging aperture of vertical feeding machine.
The utility model has following beneficial effect with respect to prior art:
1) produce superfine talcum powder master batch compared with techniques with banbury, the utility model adopts appropriate raw material formula, novel birotor continuous mixing and comminutor to guarantee continuous mixing and granulation; Birotor continuous mixing and Granulation Equipments greatly reduce the volume and weight (the equipment type gross weight of identical output has only about half of banbury) of equipment simultaneously, and greatly reduce equipment power dissipation; In addition, birotor continuous mixing of the utility model and Granulation Equipments automaticity are high, simple to operate, the O&M cost is all relatively low.
2) compare with the preparation method who adopts high-speed mixer to add double screw extruder, the superfine talcum powder of the utility model is easy to by the polypropylene matrix resin-coated; And superfine talcum powder is filled content and is higher than 70%; In addition, can effectively feed in the double screw extruder though the superfine talcum powder bulk density is low, the utility model can make the filling content of superfine talcum powder up to 85%.
3) with the adhesive treatment of dilution after superfine talcum powder, compare through the extruder granulation of normal temperature, thereby there is not diluent recovery difficulty protection environment border in the utility model; In addition, the extra fine talc powder filling master can not produce the secondary dust pollution question in transportation, use; And the product particle of preparation is even, outward appearance is neat and artistic, meets customer need.
Description of drawings
Fig. 1 is the structural representation that the utility model superfine talcum powder polypropylene is filled the manufacturing equipment of master batch.
Fig. 2 is the birotor continuous mixing structural representation of the utility model superfine talcum powder filled polypropylene master batch.
The specific embodiment
Below in conjunction with embodiment and accompanying drawing the utility model is described in further detail, but the embodiment of utility model is not limited thereto.
As illustrated in fig. 1 and 2, be used to produce the equipment that the superfine talcum powder polypropylene is filled master batch, comprise mixer 1, feeding machine, two-rotor continuous mixer 5, single screw extrusion machine 6 and the fervent comminutor 7 of die face.Mixer is located at the top of feeding machine; The discharging opening of feeding machine is connected with the charging aperture 54 of two-rotor continuous mixer 5; The discharging opening of two-rotor continuous mixer 5 is connected with the charging aperture of single screw extrusion machine 6, and the discharging opening of said single screw extrusion machine 6 is connected with the charging aperture of the fervent comminutor 7 of die face.Two-rotor continuous mixer 5 comprises first two-rotor continuous mixer 51, second two-rotor continuous mixer 52; The charging aperture of two-rotor continuous mixer 5 is connected with first two-rotor continuous mixer 51; First two-rotor continuous mixer 51, second two-rotor continuous mixer 52 are connected, and second two-rotor continuous mixer 52 is connected with the discharging opening of two-rotor continuous mixer 5.Be provided with storage bin 53 between the charging aperture 54 of two-rotor continuous mixer 5 and first two-rotor continuous mixer 51.The charging aperture 54 of said two-rotor continuous mixer 5 is a funnel-form.Mixer comprises tilting discharging mouth, and tilting discharging mouth places the top of feeding bin 2.Feeding machine comprises feeding bin 2, and this feeding bin 2 is a funnel-form.Feeding machine also comprises horizontal feeding machine 3 and vertical feeding machine 4, and the charging aperture of horizontal feeding machine 3 is connected with the discharging opening of feeding bin 2, and the discharging opening of horizontal feeding machine 3 is connected with the charging aperture of vertical feeding machine 4.
The superfine talcum powder polypropylene of this device fabrication is filled master batch, and its composition and weight percentage are: the extra fine talc powder content is 75 ~ 85%; Polypropylene material content is 10 ~ 15%; Antioxidant is 0.5 ~ 0.7%; Processing aid is 1 ~ 5%.This processing aid is stearic acid and Chinese wax; Its weight percentage is: stearic acid is 1 ~ 3%, and Chinese wax is 1 ~ 2%.This superfine talcum powder average grain diameter is 2 ~ 5 microns.This polypropylene material is the composite material of polypropylene or polypropylene, polyolefin elastomer.
This superfine talcum powder polypropylene is filled the preparation method of master batch, may further comprise the steps:
Step 1) drops into polypropylene or polypropylene, the composite material of polyolefin elastomer, talcum powder, antioxidant, processing aid in proportion in the mixer 1 and mixes;
Step 2), with in the mixed material input feeding machine;
Step 3), material is indoor through the continuous birotor continuous mixing that is admitted to preset temperature of feeding machine, and the indoor material that has mixed of birotor continuous mixing is constantly extruded simultaneously;
Step 4), the material in the step 3) is extruded through single screw extrusion machine 6, is prepared from through 7 granulations of die face hot cut pellet machine again.
In this step 1), said material mixed on low speed 0.5 ~ 1min at first in mixer 1; Follow high-speed mixing 5 ~ 10min; Said high speed is 600 ~ 1200rpm.
Particularly, get 19 parts of polypropylene powders, 2.5 parts of Chinese wax, 3 parts of stearic acid, 0.5 part in antioxidant, 75 parts of superfine talcum powders.Above-mentioned material is all dropped in the mixer, go to high speed 1000RPM mixing 8min behind the mixed on low speed 1min; Mixed material is unloaded to the feeding bin of feeding machine; Then material is by continuous delivering in the birotor continuous mixing chamber, and the temperature in this birotor continuous mixing chamber is set at 80 ℃ and 220 ℃, successively mixing by birotor in reaching the mixing chamber of preheat temperature, the plasticizing of material; The material that is finally plastified type of one-tenth dough is admitted in the barrel of the good single screw extrusion machine of preheating under the extruding of birotor and material, and each warm area of this single screw extrusion machine is set at 100 ℃, 180 ℃, 160 ℃ respectively; The material of class dough is under the extruding of the screw rod with certain rotating speed, uniformly through the typing nib; Then, the cutter of the high speed rotation be close at the die face place of the material of such dough constantly cuts off and is prepared into qualified particle.
The foregoing description is merely the preferred embodiment of the utility model, is not the practical range that is used for limiting the utility model.Be that all equalizations of being done according to the utility model content change and modification, all contained by the utility model claim scope required for protection.

Claims (7)

1. one kind is used to produce the equipment that the superfine talcum powder polypropylene is filled master batch, it is characterized in that: comprise mixer (1), feeding machine, two-rotor continuous mixer (5), single screw extrusion machine (6) and the fervent comminutor of die face (7); Said mixer is located at the top of feeding machine; The discharging opening of said feeding machine is connected with the charging aperture (54) of two-rotor continuous mixer (5); The discharging opening of said two-rotor continuous mixer (5) is connected with the charging aperture of single screw extrusion machine (6), and the discharging opening of said single screw extrusion machine (6) is connected with the charging aperture of the fervent comminutor of die face (7).
2. the equipment that is used to produce superfine talcum powder polypropylene filling master batch according to claim 1; It is characterized in that: said two-rotor continuous mixer (5) comprises first two-rotor continuous mixer (51), second two-rotor continuous mixer (52); The charging aperture (54) of said two-rotor continuous mixer (5) is connected with first two-rotor continuous mixer (51); Said first two-rotor continuous mixer (51), second two-rotor continuous mixer (52) are connected, and said second two-rotor continuous mixer (52) is connected with the discharging opening of two-rotor continuous mixer (5).
3. according to claim 2 being used to produced the equipment that the superfine talcum powder polypropylene is filled master batch, it is characterized in that: be provided with storage bin (53) between the charging aperture (54) of said two-rotor continuous mixer (5) and first two-rotor continuous mixer (51).
4. according to claim 2 being used to produced the equipment that the superfine talcum powder polypropylene is filled master batch, it is characterized in that: the charging aperture (54) of said two-rotor continuous mixer (5) is funnel-form.
5. according to each described equipment that is used to produce superfine talcum powder polypropylene filling master batch of claim 1-4, it is characterized in that: said mixer comprises tilting discharging mouth, and said tilting discharging mouth places the top of feeding bin (2).
6. according to claim 5 being used to produced the equipment that the superfine talcum powder polypropylene is filled master batch, and it is characterized in that: said feeding machine comprises feeding bin (2), and said feeding bin (2) is a funnel-form.
7. the equipment that is used to produce superfine talcum powder polypropylene filling master batch according to claim 6; It is characterized in that: said feeding machine also comprises horizontal feeding machine (3) and vertical feeding machine (4); The charging aperture of said horizontal feeding machine (3) is connected with the discharging opening of feeding bin (2), and the discharging opening of said horizontal feeding machine (3) is connected with the charging aperture of vertical feeding machine (4).
CN201220037428XU 2012-02-06 2012-02-06 Equipment for producing ultrathin talcum powder polypropylene filling master batch Expired - Fee Related CN202412518U (en)

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CN201220037428XU CN202412518U (en) 2012-02-06 2012-02-06 Equipment for producing ultrathin talcum powder polypropylene filling master batch

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CN201220037428XU CN202412518U (en) 2012-02-06 2012-02-06 Equipment for producing ultrathin talcum powder polypropylene filling master batch

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103707487A (en) * 2013-12-30 2014-04-09 南京诚盟机械有限公司 Multifunctional adjustable two-stage extrusion unit

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103707487A (en) * 2013-12-30 2014-04-09 南京诚盟机械有限公司 Multifunctional adjustable two-stage extrusion unit
CN103707487B (en) * 2013-12-30 2016-04-13 江苏诚盟装备股份有限公司 A kind of multifunctional adjustable Dual inoculation group

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CF01 Termination of patent right due to non-payment of annual fee
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Granted publication date: 20120905

Termination date: 20190206