CN202289495U - Evaporator for production of high-purity isoquinoline - Google Patents

Evaporator for production of high-purity isoquinoline Download PDF

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Publication number
CN202289495U
CN202289495U CN2011204142592U CN201120414259U CN202289495U CN 202289495 U CN202289495 U CN 202289495U CN 2011204142592 U CN2011204142592 U CN 2011204142592U CN 201120414259 U CN201120414259 U CN 201120414259U CN 202289495 U CN202289495 U CN 202289495U
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CN
China
Prior art keywords
distributing disc
disc
distributing
purity
distributor
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN2011204142592U
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Chinese (zh)
Inventor
谢解锋
杨泽静
周磊磊
孙迦宾
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
SHANGHAI XUMIN CHEMICAL TECHNOLOGY DEVELOPMENT Co Ltd
Original Assignee
SHANGHAI XUMIN CHEMICAL TECHNOLOGY DEVELOPMENT Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by SHANGHAI XUMIN CHEMICAL TECHNOLOGY DEVELOPMENT Co Ltd filed Critical SHANGHAI XUMIN CHEMICAL TECHNOLOGY DEVELOPMENT Co Ltd
Priority to CN2011204142592U priority Critical patent/CN202289495U/en
Application granted granted Critical
Publication of CN202289495U publication Critical patent/CN202289495U/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

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  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)

Abstract

The utility model discloses an evaporator for production of high-purity isoquinoline. The evaporator comprises a feed pipe, an end socket, a disc distributor and a downcomer, the feed pipe is connected with one end of the disc distributor through the end socket, the other end of the disc distributor is connected with the downcomer, the disc distributor consists of an initial distributor and a distribution disc group, the initial distributor consists of a dispersion disc and a check ring and the distribution disc group consists of a plurality of porous sieve plate distribution discs. The evaporator has the advantages of even liquid distribution and simple structure, is convenient to process and install, hard to scale, convenient to clean, stable and reliable to operate and quite suitable for large-flow operation.

Description

The evaporimeter that high-purity isoquinolin is produced
[technical field]
The utility model relates to a kind of evaporimeter, especially relates to the evaporimeter that a kind of high-purity isoquinolin is produced.
[background technology]
The distributor kind of falling film evaporator is more, traditional distributor be broadly divided into overflow type and plug-in type (flow guiding type) etc.Wherein overflow type is simple in structure, and the operating flexibility of processing, high, the difficult obstruction of installation accuracy, cloth liquid is big, guarantees but the distribution effect is difficult, is applicable to the less demanding occasion that distributes; Plug-in type can guarantee that generally liquid cloth film in single tube is even; And be difficult for guaranteeing that liquid is evenly distributed on all heat exchanger tubes, and flow resistance is big, is prone to stop up; Processing, installation requirement height; Be suitable for handling the small-sized falling film evaporator of cleaning material, and all be not suitable for the evaporimeter that high-purity isoquinolin is produced, therefore be necessary to improve.
[utility model content]
The technical problem that the utility model solves provides the evaporimeter that a kind of high-purity isoquinolin is produced; The disc type distributor that is provided with in it is made up of initial distribution device and distributing disc group; The initial distribution device is realized the initial distribution of feed liquid; Have sieve aperture according to certain rules on the sieve plate of distributing disc bottom, the feed liquid sieve aperture of flowing through is realized the multiple spot cloth, reaches equally distributed purpose.
In order to solve the problems of the technologies described above; The technical scheme that the utility model adopts is: the evaporimeter that high-purity isoquinolin is produced, comprise feed pipe, end socket, disc type distributor and downspout, and said feed pipe is connected with disc type distributor one end through end socket; The said disc type distributor other end is connected with downspout; Said disc type distributor is made up of initial distribution device and distributing disc group, and said initial distribution device is made up of dispersion impeller and back-up ring, and said distributing disc group is made up of a plurality of porous sieve plate distributing discs.
Wherein, said porous sieve plate distributing disc is made up of last distributing disc, middle distributing disc and following distributing disc, saidly goes up distributing disc, middle distributing disc (and the spacing between the following distributing disc is by the distance sink tube location and fixed by the support bolt bottom.
Further, the said sieve aperture of going up on distributing disc, middle distributing disc and the following distributing disc is staggeredly arranged.
Further; It is said that upward distributing disc is identical with the pattern of middle distributing disc; All being equilateral triangle arranges; But the pitch of holes that staggers each other half, the hole on the said distributing disc down is regular hexagon arranges, and makes each downspout have six bursts of flows to fall realization to downspout multiple spot cloth from following distributing disc sieve aperture on every side.
Compared with prior art cloth liquid is even for the utility model, and is simple in structure, and processing, easy for installation, less scaling is convenient to clean, and stable operation is reliable, is particularly suitable for big flow operation.
[description of drawings]
Accompanying drawing described herein is the further understanding that is used to provide the utility model, constitutes the application's a part, but do not constitute improper qualification the utility model, in the accompanying drawings:
Fig. 1 is the structural representation of the utility model;
Fig. 2 be between each distributing disc of the utility model sieve aperture with position view.
Description of reference numerals: 1-feed pipe; The 2-end socket; The 3-back-up ring; The 4-dispersion impeller; The last distributing disc of 5-; Distributing disc among the 6-; Distributing disc under the 7-; The 8-distance sink tube; 9-supports bolt; The 10-downspout.
[specific embodiment]
The embodiment of the utility model is described below.
The evaporimeter that high-purity isoquinolin is produced; Comprise feed pipe 1, end socket 2, disc type distributor and downspout 10; Said feed pipe 1 is connected with disc type distributor one end through end socket 2, and the said disc type distributor other end is connected with downspout 10, and said disc type distributor is made up of initial distribution device and distributing disc group; Said initial distribution device is made up of dispersion impeller 4 and back-up ring 3, and said distributing disc dish group is made up of a plurality of porous sieve plate distributing discs.Said porous sieve plate distributing disc is made up of last distributing disc 5, middle distributing disc 6 and following distributing disc 7, saidly goes up spacing between distributing disc 5, middle distributing disc 6 and the following distributing disc 7 by distance sink tube 8 location and fix by supporting bolt 9 bottom.
In the design of disc type distributor, the pattern on the porous sieve plate distributing disc is extremely important to the performance of distributor.In general, the arrangement mode of the downspout on pattern and the falling film evaporator tube sheet is relevant, and feed liquid can be fallen on the slab bridge of tube sheet when sieve aperture falls from last distributing disc.When a plurality of distributing disc is arranged, should make that sieve aperture staggers mutually between each dish.When flow one timing, if perforate is many more, then the aperture is more little, is prone to stop up less being advisable in suggestion cloth hole.The said sieve aperture of going up on distributing disc 5, middle distributing disc 6 and the following distributing disc 7 is staggeredly arranged, and is as shown in Figure 2, following distributing disc hole 11; Last distributing disc hole 12, middle distributing disc hole 13, specifically; It is said that upward distributing disc 5 is identical with the pattern of middle distributing disc 6, and all be equilateral triangle and arrange, but the pitch of holes that staggers each other half; Hole on the said distributing disc 7 down is regular hexagon arranges, and makes each downspout 10 have six bursts of flows to fall realization to downspout 10 multiple spot clothes from following distributing disc 7 sieve apertures on every side.When low discharge was operated, for preventing to stop up sieve aperture, suggestion was cancelled the more following distributing disc 7 in cloth hole and is become two dish distributors.
The manufacturing of disc type distributor and installation quality have very big influence to cloth film effect.For making the disc type distributor obtain good performance, to guarantee that in manufacture process tube sheet and porous sieve plate distributing disc are smooth and keep good flatness and rigidity.Little sieve aperture will be done chamfered on the distributing disc, and burr must not be arranged, so that feed liquid can evenly flow on dish, prevents sieve aperture extension dirt.During installation, utilize specific purpose tool to make tube sheet and distributing disc sieve plate maintenance level.In a word, when only all being guaranteed, just can make distributor be able to stable operation, reach the purpose of even cloth film at aspects such as design, manufacturing, installation and operations.
Operation principle: during operation; Feed liquid gets into the slot overflow of dispersion impeller 4 backs from dispersion impeller 4 from feed pipe 1; Fall on the distributing disc 5 through the annular space of 3 of dispersion impeller 4 and back-up rings and to accomplish initial distribution, distributing disc 6 is fallen on the slab bridge of tube sheet with the sieve plate on the following distributing disc 7 in flowing through respectively again, and downspout 10 is gone in overflow; Wall is membranaceous and flows down within it, reaches the purpose of even cloth film.
The above in the spiritual category that does not break away from the utility model creation, is familiar with the protection domain that this technological various simple covert and modification that those skilled in the art did still belongs to the utility model only in order to the convenient the utility model of explaining.

Claims (4)

1. the evaporimeter produced of high-purity isoquinolin; Comprise feed pipe (1), end socket (2), disc type distributor and downspout (10); Said feed pipe (1) is connected with disc type distributor one end through end socket (2), and the said disc type distributor other end is connected with downspout (10), it is characterized in that: said disc type distributor is made up of initial distribution device and distributing disc group; Said initial distribution device is made up of dispersion impeller (4) and back-up ring (3), and said distributing disc group is made up of a plurality of porous sieve plate distributing discs.
2. the evaporimeter that high-purity isoquinolin according to claim 1 is produced; It is characterized in that: said porous sieve plate distributing disc is made up of last distributing disc (5), middle distributing disc (6) and following distributing disc (7), and the said spacing that goes up between distributing disc (5), middle distributing disc (6) and the following distributing disc (7) is located by distance sink tube (8) and be fixing by supporting bolt (9) bottom.
3. the evaporimeter that high-purity isoquinolin according to claim 2 is produced is characterized in that: the said sieve aperture of going up on distributing disc (5), middle distributing disc (6) and the following distributing disc (7) is staggeredly arranged.
4. the evaporimeter of producing according to claim 2 or 3 described high-purity isoquinolin; It is characterized in that: said upward distributing disc (5) is identical with the pattern of middle distributing disc (6); All being equilateral triangle arranges; But the pitch of holes that staggers each other half, the hole on the said distributing disc (7) down is regular hexagon arranges, and makes each downspout (10) have six bursts of flows to fall realization to downspout (10) multiple spot cloth from following distributing disc (7) sieve aperture on every side.
CN2011204142592U 2011-10-26 2011-10-26 Evaporator for production of high-purity isoquinoline Expired - Fee Related CN202289495U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN2011204142592U CN202289495U (en) 2011-10-26 2011-10-26 Evaporator for production of high-purity isoquinoline

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN2011204142592U CN202289495U (en) 2011-10-26 2011-10-26 Evaporator for production of high-purity isoquinoline

Publications (1)

Publication Number Publication Date
CN202289495U true CN202289495U (en) 2012-07-04

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CN2011204142592U Expired - Fee Related CN202289495U (en) 2011-10-26 2011-10-26 Evaporator for production of high-purity isoquinoline

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103861301A (en) * 2014-03-12 2014-06-18 无锡力马化工机械有限公司 Material concentration desolvation heat exchanger with multi-stage distribution
CN108854120A (en) * 2018-07-01 2018-11-23 李晓娟 A kind of organo silane coupling agent rectifying filter device

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103861301A (en) * 2014-03-12 2014-06-18 无锡力马化工机械有限公司 Material concentration desolvation heat exchanger with multi-stage distribution
CN108854120A (en) * 2018-07-01 2018-11-23 李晓娟 A kind of organo silane coupling agent rectifying filter device

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C14 Grant of patent or utility model
GR01 Patent grant
DD01 Delivery of document by public notice

Addressee: Shanghai Xumin Chemical Technology Development Co., Ltd.

Document name: Notification to Pay the Fees

DD01 Delivery of document by public notice

Addressee: Shanghai Xumin Chemical Technology Development Co., Ltd.

Document name: Notification of Termination of Patent Right

CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20120704

Termination date: 20151026

EXPY Termination of patent right or utility model