CN202238011U - Process evaluation system for multifunctional gas-solid fluidized bed - Google Patents

Process evaluation system for multifunctional gas-solid fluidized bed Download PDF

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Publication number
CN202238011U
CN202238011U CN201120359905XU CN201120359905U CN202238011U CN 202238011 U CN202238011 U CN 202238011U CN 201120359905X U CN201120359905X U CN 201120359905XU CN 201120359905 U CN201120359905 U CN 201120359905U CN 202238011 U CN202238011 U CN 202238011U
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gas
liquid separator
level
liquid
fluidized
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CN201120359905XU
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Chinese (zh)
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吴道洪
王其成
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Beijing Shenwu Environmental and Energy Technology Co Ltd
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Beijing Shenwu Environmental and Energy Technology Co Ltd
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  • Fluidized-Bed Combustion And Resonant Combustion (AREA)

Abstract

The utility model discloses a process evaluation system for a multifunctional gas-solid fluidized bed, and the process evaluation system comprises a gas buffer tank and a steam generating furnace. Two paths of gas feeding materials enter a fluidized bed reactor to react with solid particle reactants through a gas heating furnace and a fixed bed reactor. After being cooled by a primary cooler, a gas product generated by the fluidized bed reactor enters a primary gas-liquid separator to realize gas-liquid separation. Liquid separated out by the primary gas-liquid separator is stored in a primary liquid storage tank and is weighed by a primary electronic weigher. Gas separated out by the primary gas-liquid separator enters a secondary cooler to be cooled to the room temperature and then enters a secondary gas-liquid separator to complete gas-liquid separation. Liquid separated out by the secondary gas-liquid separator is stored in a secondary liquid storage tank and is weighed by a secondary electronic weigher. Tail gas separated out by the secondary gas-liquid separator is metered by a tail gas meter. The system can be used for completing evaluation of various related processes of a gas-solid system fixed bed, a bubble fluidization bed, a turbulent bed, a circulating fluidized bed and the like, has low equipment investment and is easy to operate.

Description

The solid fluid bed technology assessment of Multifunctional, air system
Technical field
The utility model relates to a kind of fluidization application technology, relates in particular to the solid fluid bed technology assessment of a kind of Multifunctional, air system.
Background technology
Fluidization technology has been widely applied to various fields such as chemical industry, petrochemical industry, metallurgy, the energy, material, biochemical environmental protection, pharmacy.Yet, because the inhomogeneities of the interior two-phase flow structure of fluidized-bed reactor and the polymorphism in basin make the fluidized-bed process of different field have salient feature.Therefore, fluidized-bed process all need be estimated it before every field is used, even in same territory, because the difference of process conditions also need be estimated related process.
In the prior art; The traditional design thinking of fluidized-bed process evaluation system is according to technological requirement fluidized-bed reactor to be fixed as a certain type, and relevant operating condition (as: temperature, pressure, gas flow, mass of solid particles flow rate etc.) is limited in the very narrow interval, in case after technology assessment is accomplished; This technology assessment system is difficult to be used further to estimate other technologies; The result causes the serious waste of experimental resources, and R&D costs increase considerably, and is unfavorable for the sound development of enterprise.
The utility model content
The purpose of the utility model provides the solid fluid bed technology assessment of a kind of Multifunctional, air system, and this system can accomplish the evaluation of multiple related process such as gas-solid system fixed bed, bubbling bed, turbulent bed and recirculating fluidized bed, and equipment investment is few, and is easy to operate.
The purpose of the utility model realizes through following technical scheme:
The solid fluid bed technology assessment of the Multifunctional, air of the utility model system; Comprise gas buffer jar, Steam generating furnace; The import of said gas buffer jar is connected with the unstripped gas pipeline; The import of said Steam generating furnace is connected with the deionized water pipeline through measuring pump; The outlet of said gas buffer jar converges the back with the outlet of said Steam generating furnace and is connected with the import of gas heating stove, and the outlet of said gas heating stove is connected with the import of fixed bed reactors bottom, and the outlet at said fixed bed reactors top is connected with the import of fluidized-bed reactor bottom; The bottom of said fluidized-bed reactor is provided with the solid discharge port, and the top of said fluidized-bed reactor is connected with the vacuum feed pipe;
The outlet at said fluidized-bed reactor top is connected with one-level cooler, one-level gas-liquid separator, one-level fluid reservoir successively, and the bottom of said one-level fluid reservoir is provided with the one-level electronic scale;
The gas vent of said one-level gas-liquid separator is connected with secondary coolers, secondary gas-liquid separator, secondary fluid reservoir successively, and the bottom of said secondary fluid reservoir is provided with the secondary electrons scale;
The gas vent of said secondary gas-liquid separator is connected with the tail gas table.
Technical scheme by above-mentioned the utility model provides can be found out; The solid fluid bed technology assessment of the Multifunctional, air that the utility model provides system; Owing to comprise gas buffer jar and Steam generating furnace two-way gas feed, react through gas heating stove, fixed bed reactors entering fluidized-bed reactor and solid particulate reagent.The gaseous product that fluidized-bed reactor produces is after the cooling of one-level cooler; Get into the one-level gas-liquid separator and realize gas-liquid separation, liquid separated is stored in the one-level fluid reservoir and by the metering of one-level electronic scale, the gas that the one-level gas-liquid separator separates is come out gets into the secondary coolers cool to room temperature again; Get into the secondary gas-liquid separator then and accomplish gas-liquid separation; Liquid separated is stored in the secondary fluid reservoir and by the metering of secondary electrons scale, the tail gas of secondary gas-liquid separator separates can be accomplished the evaluation of multiple related process such as gas-solid system fixed bed, bubbling bed, turbulent bed and recirculating fluidized bed by the metering of tail gas table; Equipment investment is few, and is easy to operate.
Description of drawings
Fig. 1 is the structural representation of the solid fluid bed technology assessment of the Multifunctional, air of the utility model system.
Among the figure: 1, gas buffer jar, 2, measuring pump, 3, Steam generating furnace, 4, gas heating stove; 5, fixed bed reactors, 6, fluidized-bed reactor, 7, the one-level cooler, 8, the one-level gas-liquid separator; 9, one-level fluid reservoir, 10, the one-level electronic scale, 11, secondary coolers, 12, the secondary gas-liquid separator; 13, secondary fluid reservoir, 14, the secondary electrons scale, 15, the tail gas table.
The specific embodiment
To combine accompanying drawing that the utility model embodiment is done to describe in detail further below.
The solid fluid bed technology assessment of the Multifunctional, air of the utility model system, its preferable specific embodiment is as shown in Figure 1:
Comprise gas buffer jar, Steam generating furnace; The import of said gas buffer jar is connected with the unstripped gas pipeline; The import of said Steam generating furnace is connected with the deionized water pipeline through measuring pump; The outlet of said gas buffer jar converges the back with the outlet of said Steam generating furnace and is connected with the import of gas heating stove, and the outlet of said gas heating stove is connected with the import of fixed bed reactors bottom, and the outlet at said fixed bed reactors top is connected with the import of fluidized-bed reactor bottom; The bottom of said fluidized-bed reactor is provided with the solid discharge port, and the top of said fluidized-bed reactor is connected with the vacuum feed pipe;
The outlet at said fluidized-bed reactor top is connected with one-level cooler, one-level gas-liquid separator, one-level fluid reservoir successively, and the bottom of said one-level fluid reservoir is provided with the one-level electronic scale;
The gas vent of said one-level gas-liquid separator is connected with secondary coolers, secondary gas-liquid separator, secondary fluid reservoir successively, and the bottom of said secondary fluid reservoir is provided with the secondary electrons scale;
The gas vent of said secondary gas-liquid separator is connected with the tail gas table.
The said fixed bed reactors outside and the said fluidized-bed reactor outside are respectively equipped with heating furnace.
Said one-level fluid reservoir and secondary fluid reservoir are respectively equipped with the liquid sampling mouth; The gas outlet of said secondary gas-liquid separator is provided with the gas sample mouth.
The solid fluid bed technology assessment of the Multifunctional, air of the utility model system realizes the method for gas-solid fluidized bed technology assessment, comprises processing step:
A, through the two-way gas feed; One the tunnel is the mixed material gas of pressure≤10MPa; Mist through the voltage stabilizing of gas buffer jar after, in gas heating stove, be heated to temperature≤900 ℃, get into fluidized-bed reactor through fixed bed reactors then and solid particulate reagent reacts; Another road is the water charging; Deionized water is after the measuring pump metering and being pressurized to pressure≤5MPa; In Steam generating furnace, be converted into water vapour; In gas heating stove, be heated to temperature≤900 ℃ then, get into fluidized-bed reactor through fixed bed reactors at last and solid particulate reagent reacts;
Said two-way gas feeding manner uses simultaneously or uses separately;
The gaseous product that B, said fluidized-bed reactor produce is after the cooling of one-level cooler; Get into the one-level gas-liquid separator and realize gas-liquid separation; Liquid separated is stored in the one-level fluid reservoir, and the amount of liquid of one-level fluid reservoir is by the metering of one-level electronic scale, and the gas that the one-level gas-liquid separator separates is come out gets into the secondary coolers cool to room temperature again; Get into the secondary gas-liquid separator then and accomplish gas-liquid separation; Liquid separated is stored in the secondary fluid reservoir, and the amount of liquid of secondary fluid reservoir is by the metering of secondary electrons scale, and the tail gas of secondary gas-liquid separator separates is measured by the tail gas table.
In the said steps A, loading catalyst uses or empty bed use in the said fixed bed reactors;
Said fluidized-bed reactor can be operated under fixed bed, bubbling bed, turbulent bed or recirculating fluidized bed condition;
Said solid particle can adopt the charging of negative pressure of vacuum mode, granularity≤10mm.
Among the said step B, the cooling medium of said one-level cooler can be cold process gas, and the cooling medium of said secondary coolers can be the room temperature demineralized water.
Specific embodiment:
Referring to Fig. 1, be example with powdered coal fluidized bed gasification technology assessment system again, coal dust is loaded in the fluidized-bed reactor 6 through the negative pressure of vacuum mode, and fluidized-bed reactor 6 is operated under the recirculating fluidized bed condition.Gasifying medium is selected oxygen and water vapour; Pressure is that the oxygen of 4MPa is introduced into 1 voltage stabilizing of gas buffer jar; Deionized water is converted into water vapour through measuring pump 2 metering and after being pressurized to pressure and being 4MPa in Steam generating furnace 3, after the water vapour that Steam generating furnace 3 produces and the oxygen mix from gas buffer jar 1; Get into together and be heated to 900 ℃ in the gas heating stove 4, get in the fluidized-bed reactor 6 through unloaded fixed bed reactors 5 at last and react with the coal dust generating gasification; The gasification gas that fluidized-bed reactor 6 produces is earlier after 7 coolings of one-level cooler; Get into one-level gas-liquid separator 8 and realize gas-liquid separation; Liquid separated is stored in the one-level fluid reservoir 9, and the amount of liquid of one-level fluid reservoir 9 is by 10 meterings of one-level electronic scale, and the gas that one-level gas-liquid separator 8 is separated gets into secondary coolers 11 cool to room temperature again; Get into secondary gas-liquid separator 12 then and accomplish gas-liquid separation; Liquid separated is stored in the secondary fluid reservoir 13, and the amount of liquid of secondary fluid reservoir 13 is by 14 meterings of secondary electrons scale, and the coal gas that secondary gas-liquid separator 13 separates is measured by tail gas table 15.
The above; Be merely the preferable specific embodiment of the utility model; But the protection domain of the utility model is not limited thereto; Any technical staff who is familiar with the present technique field is in the technical scope that the utility model discloses, and the variation that can expect easily or replacement all should be encompassed within the protection domain of the utility model.Therefore, the protection domain of the utility model should be as the criterion with the protection domain of claims.

Claims (3)

1. the solid fluid bed technology assessment of Multifunctional, air system; It is characterized in that; Comprise gas buffer jar, Steam generating furnace; The import of said gas buffer jar is connected with the unstripped gas pipeline, and the import of said Steam generating furnace is connected with the deionized water pipeline through measuring pump, and the outlet of said gas buffer jar converges the back with the outlet of said Steam generating furnace and is connected with the import of gas heating stove; The outlet of said gas heating stove is connected with the import of fixed bed reactors bottom; The outlet at said fixed bed reactors top is connected with the import of fluidized-bed reactor bottom, and the bottom of said fluidized-bed reactor is provided with the solid discharge port, and the top of said fluidized-bed reactor is connected with the vacuum feed pipe;
The outlet at said fluidized-bed reactor top is connected with one-level cooler, one-level gas-liquid separator, one-level fluid reservoir successively, and the bottom of said one-level fluid reservoir is provided with the one-level electronic scale;
The gas vent of said one-level gas-liquid separator is connected with secondary coolers, secondary gas-liquid separator, secondary fluid reservoir successively, and the bottom of said secondary fluid reservoir is provided with the secondary electrons scale;
The gas vent of said secondary gas-liquid separator is connected with the tail gas table.
2. the solid fluid bed technology assessment of Multifunctional, air according to claim 1 system is characterized in that, the said fixed bed reactors outside and the said fluidized-bed reactor outside are respectively equipped with heating furnace.
3. the solid fluid bed technology assessment of Multifunctional, air according to claim 2 system is characterized in that said one-level fluid reservoir and secondary fluid reservoir are respectively equipped with the liquid sampling mouth; The gas outlet of said secondary gas-liquid separator is provided with the gas sample mouth.
CN201120359905XU 2011-09-23 2011-09-23 Process evaluation system for multifunctional gas-solid fluidized bed Withdrawn - After Issue CN202238011U (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102389752A (en) * 2011-09-23 2012-03-28 北京神雾环境能源科技集团股份有限公司 Multifunctional gas-solid fluidized bed process evaluation system and method

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102389752A (en) * 2011-09-23 2012-03-28 北京神雾环境能源科技集团股份有限公司 Multifunctional gas-solid fluidized bed process evaluation system and method

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