CN202214311U - Coil type reactor - Google Patents

Coil type reactor Download PDF

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Publication number
CN202214311U
CN202214311U CN2011203540658U CN201120354065U CN202214311U CN 202214311 U CN202214311 U CN 202214311U CN 2011203540658 U CN2011203540658 U CN 2011203540658U CN 201120354065 U CN201120354065 U CN 201120354065U CN 202214311 U CN202214311 U CN 202214311U
Authority
CN
China
Prior art keywords
necking down
type reactor
length
pipeline section
pipe section
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN2011203540658U
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Chinese (zh)
Inventor
李春海
程丽华
陈小平
周如金
梁智群
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Guangdong University of Petrochemical Technology
Original Assignee
Guangdong University of Petrochemical Technology
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Guangdong University of Petrochemical Technology filed Critical Guangdong University of Petrochemical Technology
Priority to CN2011203540658U priority Critical patent/CN202214311U/en
Application granted granted Critical
Publication of CN202214311U publication Critical patent/CN202214311U/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

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Abstract

The utility model discloses a coil type reactor. Necking down pipe sections (3) and straight pipe sections (2) are alternatively arranged at each coil of a pipe (1) rising spirally; necking down openings at two ends of the necking down pipe sections (3) are connected with the straight pipe sections (2) with the same caliber; the length of the necking down pipe section (3) is equal to that of the straight pipe section (2) and is 10 to 15 times of the diameter of the straight pipe section (2); and the diameter of the necking down pipe section (3) is 9/10 of that of the straight pipe section (2). The coil type reactor can change the flowing state and enhance the turbulence degree in the pipe so as to improve the polymerization degree of mixed materials. Especially, when being used for producing high pressure polyethylene and propathene, the reactor can solve the problem of enhancing the conversion per pass of ethylene or propene which is not thoroughly solved in the prior art.

Description

Coil pipe type reactor
Technical field
The utility model relates to a kind of reactor drum, is a kind of coil pipe type reactor specifically, and it is specially adapted to high-pressure polyethylene and Vestolen PP 7052 production is used.
Background technology
Traditional major equipment coil pipe type reactor that is used for high-pressure polyethylene and Vestolen PP 7052 production all is to adopt isometrical tubular reactor, and it is along the rising of spiraling clockwise or counterclockwise, the pipe reaction equipment of formation by an isometrical weldless steel tube.200510101516.0 a high yield production has ethene polymerization method and the tubular reactor that is used for this method of the product of various performances; Provide a kind of tubular reactor in order to improve the production efficiency of vinyl polymerization; It has been to use a kind of reaction zone that comprises first reaction zone and second reaction zone; The xsect of second reaction zone and length are greater than first reaction zone, and ethene is introduced into from two or more different points at second reaction zone with catalyzer.But still the per pass conversion of fail fundamentally to improve ethene or propylene reduces the reaction times, shortens the length of reaction tubes.
Summary of the invention
The purpose of the utility model provides and a kind ofly can strengthen turbulent flow to the material of flowing through, thereby improves the tubular reactor of mixture extent of polymerization.
The coil pipe type reactor that the utility model provides, the pipe that rises of formula in the shape of a spiral, every circle has been arranged alternately necking down pipeline section and straight length, and bore ground such as the contraction mouth at necking down pipeline section two ends and straight length are connected.
In addition, in the utility model, also has preferred example for the necking down pipeline section in above-mentioned; Specifically be; The equal in length of the length of necking down pipeline section and adjacent straight pipeline section, and equal 10~15 times of straight length diameter, necking down pipeline section diameter is equivalent to 9/10 of straight length diameter.
If the utility model is applied to high-pressure polyethylene and Vestolen PP 7052 production; Except above-mentioned structure; The coil pipe type reactor of the utility model can also comprise other parts; Like pre-reactor, pressure warning unit measuring device, TM measuring device, electrostatic detection appearance and sample divider etc., they necessarily randomly are included in the reactor drum of vinyl polymerization.
The utlity model has following advantage:
Strengthen raw material and initiator mixed effect, improve per pass conversion, shorten the reaction times, reduce tube length of reaction tube, reduce production costs.For reaction monomers ethene (or propylene) and catalyzer; Because different in kinds such as density; When flowing through the necking down pipeline section repeatedly with the interval straight length; Change flow state in the pipe, increased turbulent extent, and then solved the raising ethene that not have thoroughly solution in the prior art or the problem of propylene per pass conversion.It is applicable to oxygen or organo-peroxide to be the gas phase high pressure polymerisation reaction of catalyzer.
Description of drawings
Fig. 1 is the structure iron of the utility model.
Embodiment
With reference to Fig. 1, the coil pipe type reactor that the utility model provides, there are import and export (4,5) at pipe 1 two ends of formula rising in the shape of a spiral, and every circle has been arranged alternately necking down pipeline section 3 and straight length 2, and the contraction mouth at necking down pipeline section 3 two ends is connected with straight length 2 ground such as bore such as grade.
The equal in length of the length of necking down pipeline section 3 and straight length 2, and equal 10~15 times of straight length 2 diameters, the diameter of necking down pipeline section 3 is equivalent to 9/10 of straight length 2 diameters.
The utility model in use, for example when being used for the gas phase high pressure polymerisation of ethene or propylene, when ethene (or propylene) monomer and oxygen (or organo-peroxide) catalyzer repeatedly through necking down pipeline section 3 during with straight length 2; Because the difference of their character such as density, increased the difference of two kinds of differences or multiple flow of matter speed, strengthened the tube fluid turbulent extent; And then improved the per pass conversion of ethene or propylene; Shorten the reaction times, reduced tube length of reaction tube, reduced production cost.

Claims (2)

1. a coil pipe type reactor is characterized in that the every circle of pipe (1) of formula rising has been arranged alternately necking down pipeline section (3) and straight length (2) in the shape of a spiral, and the contraction mouth at necking down pipeline section (3) two ends is connected with straight length bore ground such as (2).
2. coil pipe type reactor according to claim 1 is characterized in that the length of necking down pipeline section (3) and the equal in length of straight length (2), and equals 10~15 times of straight length (2) diameter, and the diameter of necking down pipeline section (3) is equivalent to 9/10 of straight length (2) diameter.
CN2011203540658U 2011-09-21 2011-09-21 Coil type reactor Expired - Fee Related CN202214311U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN2011203540658U CN202214311U (en) 2011-09-21 2011-09-21 Coil type reactor

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN2011203540658U CN202214311U (en) 2011-09-21 2011-09-21 Coil type reactor

Publications (1)

Publication Number Publication Date
CN202214311U true CN202214311U (en) 2012-05-09

Family

ID=46013574

Family Applications (1)

Application Number Title Priority Date Filing Date
CN2011203540658U Expired - Fee Related CN202214311U (en) 2011-09-21 2011-09-21 Coil type reactor

Country Status (1)

Country Link
CN (1) CN202214311U (en)

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109593151A (en) * 2017-09-30 2019-04-09 中国石油化工股份有限公司 Prepare the method and system, poly alpha olefin and flow reactor of poly alpha olefin
CN111434377A (en) * 2019-01-11 2020-07-21 中国石油化工股份有限公司 Coil microreactor and microreactor system
CN111527110A (en) * 2018-01-02 2020-08-11 巴塞尔聚烯烃股份有限公司 High pressure ethylene polymerization manufacturing facility and emergency shutdown method
CN111692898A (en) * 2020-05-07 2020-09-22 广东百思特管业科技有限公司 Stainless steel sleeve heat exchanger

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109593151A (en) * 2017-09-30 2019-04-09 中国石油化工股份有限公司 Prepare the method and system, poly alpha olefin and flow reactor of poly alpha olefin
CN111527110A (en) * 2018-01-02 2020-08-11 巴塞尔聚烯烃股份有限公司 High pressure ethylene polymerization manufacturing facility and emergency shutdown method
CN111527110B (en) * 2018-01-02 2021-01-08 巴塞尔聚烯烃股份有限公司 High pressure ethylene polymerization manufacturing facility and emergency shutdown method
CN111434377A (en) * 2019-01-11 2020-07-21 中国石油化工股份有限公司 Coil microreactor and microreactor system
CN111434377B (en) * 2019-01-11 2022-07-15 中国石油化工股份有限公司 Coil microreactor and microreactor system
CN111692898A (en) * 2020-05-07 2020-09-22 广东百思特管业科技有限公司 Stainless steel sleeve heat exchanger
CN111692898B (en) * 2020-05-07 2021-09-21 广东百思特管业科技有限公司 Stainless steel sleeve heat exchanger

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Date Code Title Description
C14 Grant of patent or utility model
GR01 Patent grant
C17 Cessation of patent right
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20120509

Termination date: 20120921