CN202072637U - Ammonification pelleting cylinder - Google Patents

Ammonification pelleting cylinder Download PDF

Info

Publication number
CN202072637U
CN202072637U CN2011201299065U CN201120129906U CN202072637U CN 202072637 U CN202072637 U CN 202072637U CN 2011201299065 U CN2011201299065 U CN 2011201299065U CN 201120129906 U CN201120129906 U CN 201120129906U CN 202072637 U CN202072637 U CN 202072637U
Authority
CN
China
Prior art keywords
tube
acid
ammonia
vaporization chamber
distribution
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
CN2011201299065U
Other languages
Chinese (zh)
Inventor
赵强
赵菊明
石剑飞
徐志明
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Wuhan Zhongdong Phosphate Technology Co.,Ltd.
Original Assignee
JIANGSU ZHONGDONG FERTILIZER CO Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by JIANGSU ZHONGDONG FERTILIZER CO Ltd filed Critical JIANGSU ZHONGDONG FERTILIZER CO Ltd
Priority to CN2011201299065U priority Critical patent/CN202072637U/en
Application granted granted Critical
Publication of CN202072637U publication Critical patent/CN202072637U/en
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Images

Landscapes

  • Fertilizers (AREA)

Abstract

The utility model relates to the technical field of compound fertilizer production, in particular to equipment in ammonification pelleting process for compound fertilizer production. The ammonification pelleting cylinder comprises a cylinder body, a feeding port, an ammonia inlet tube and an acid inlet tube, wherein the ammonia inlet tube and the acid inlet tube are axially parallel to the cylinder body. The acid inlet tube is in a three segmented structure and formed by connecting three tube segments, namely a water inlet tube, a dilution tube and an acid distribution tube, various in inner diameters. An acid inlet is arranged on the wall of the dilution tube, and a plurality of sprayers are arranged on the wall of the acid distribution tube. The ammonia inlet tube is in a three segmented structure and comprises a liquid inlet tube, a vaporization cavity and a distribution tube, the vaporization cavity is a closed cylinder, an outlet end of the liquid inlet tube is arranged in the middle of the vaporization cavity, a tube body of the liquid inlet tube is axially parallel to the vaporization cavity, and the distribution tube is connected to the other end of the vaporization cavity.

Description

The ammoniation-granulation tube
Technical field
The utility model relates to composite fertilizer's production technical field, especially a kind of equipment that is used for the ammoniation-granulation technological process of composite fertilizer's production.
Background technology
Ammoniation-granulation explained hereafter composite fertilizer is the main flow production technique that current composite fertilizer manufacturing enterprise extensively adopts.This technology is to send in the cylinder tablets press after pulverizing by the plurality of raw materials of metering, adds sulfuric acid and ammonia in the granulation process, keeps material that certain temperature and water ratio are arranged simultaneously, utilizes the granulating method granulating.Advantages such as ammoniation-granulation technology has the production capacity height, energy consumption is low, investment is little, operation cost is low, strong operability.The adding of sulfuric acid and ammonia mainly contains following effect: one, sulfuric acid and ammonia generation chemical reaction, the one side water generation reaction, can reduce the interpolation of water in the granulation process, the heat of chemical reaction release can improve temperature of charge on the other hand, increase balling ratio, be accelerated into the ball particle moisture evaporation simultaneously, alleviate drying pressure; Two, the add-on of control sulfuric acid and the ammonia pH value that can regulate compound fertilizer granules is in the suitable scope; Three, sulfuric acid and raw material DMP effect improve water-soluble phosphorus content; Four, add sulfuric acid in the ammoniation-granulation process, make compound fertilizer granules contain this kind of plant essential nutrient element of sulphur.
Be necessary for dilute sulphuric acid owing to enter the sulfuric acid of ammoniation granulator.Current is that the vitriol oil is passed through specific equipment---sulfuric acid dilution device dilutes, so not only increased the equipment input, increase equipment working cost, also increased energy expenditure, cause the increase of production cost, and a large amount of heats that discharge in the diluting concentrated sulfuric acid process can't utilize, and cause energy dissipation.
Enter material bed ammonia by 3 liquid and two kinds of forms of gasiform are arranged.Liquid ammonia enters the granulation kiln, and the liquid ammonia absorption heat that need gasify reduces local temperature of charge, influences the material balling-up; Liquid ammonia concentration height is difficult in and sprays in the material evenly, can not with the abundant complete reaction of dilute sulphuric acid, cause partial material the phenomenon of sulfuric acid or ammonia to occur too much absorbing, not only can influence the potential of hydrogen of composite fertilizer, also can increase ammonia loss by volatilization.Liquid ammonia enters tablets press, must so must drop into and running cost by increase equipment through the vaporization of liquefied ammonia vaporizer, increases production cost.
The utility model content
The technical problems to be solved in the utility model is: overcome the deficiency in the prior art, a kind of ammoniation-granulation tube is provided.
The technical scheme that its technical problem that solves the utility model adopts is: a kind of ammoniation-granulation tube with ammonia sparger, have cylindrical shell, opening for feed, ammonia-feeding pipe and acid inlet tube, acid inlet tube and ammonia-feeding pipe and cylindrical shell axially parallel, the structure of wherein said acid inlet tube is a syllogic, the pipe connection that is had nothing in common with each other by three sections internal diameters together, be followed successively by water inlet pipe, dilution tube and sour distribution pipe, the tube wall of dilution tube is provided with acid inlet, and acid distribution tube wall is provided with a plurality of shower nozzles; Wherein said ammonia-feeding pipe is a three stage structure, be divided into liquid-inlet pipe, vaporization chamber and distribution piping, vaporization chamber is a containment cylinder, and the exit end of liquid-inlet pipe is arranged on the middle part of vaporization chamber, the body of liquid-inlet pipe and vaporization chamber axially parallel are connecting distribution piping at the other end of vaporization chamber.
The sidewall of described vaporization chamber is provided with steam inlet, and it is vertical with the liquefied ammonia liquid-inlet pipe that steam enters the direction of vaporization chamber, the liquefied ammonia of can effectively vaporizing.
For more uniform distribution ammonia, described distribution tube wall is provided with thrust-augmenting nozzle, and thrust-augmenting nozzle is vertically mounted on the distribution piping.
The beneficial effects of the utility model are: one, the enforcement by this device is owing to following reason can improve temperature of charge.At first, the heat release that is produced during the dilution of the vitriol oil and washing tail gas water can improve an interior temperature of charge in granulating cylinder, and the high temperature dilute sulphuric acid directly is sprayed on the material surface, can improve temperature of charge; Secondly, sulfuric acid and ammonia generation chemical reaction, release of heat.The raising of temperature of charge not only can increase balling ratio, makes balling ratio increase by 25%~35%, can also be accelerated into the ball particle moisture evaporation, makes dry kiln ingress moisture content drop to 2.0%~3.5%; Two, MAP can reduce citric acid soluble phosphorus content about 5% under the vitriolic effect; Three, reduce ammonia loss by volatilization, approximately reduce 10% as calculated.The direct benefit that more than brings is: the production capacity of ammoniation granulator improves 6%, and bunker coal consumption reduces by 10%, and production cost reduces by 25 yuan/ton.
Description of drawings
Below in conjunction with drawings and embodiments the utility model is further specified.
Fig. 1 is a structural representation of the present utility model.
Embodiment.
In conjunction with the accompanying drawings the utility model is further described now.The synoptic diagram that these accompanying drawings are simplification only illustrates basic structure of the present utility model in a schematic way, so it only shows the formation relevant with the utility model.
Ammoniation-granulation tube as shown in Figure 1 as shown in Figure 1, has cylindrical shell, opening for feed 1, ammonia-feeding pipe 3 and acid inlet tube 2, cylindrical shell links to each other with the gas solid separation chamber, on the gas solid separation chamber, be useful on the tail gas that absorbs tail gas and absorb mouth, in the bottom in gas solid separation chamber is material outlet, acid inlet tube 2 and cylindrical shell axially parallel, ammonia-feeding pipe 3 and cylindrical shell axially parallel, the structure of wherein said acid inlet tube 2 is a syllogic, the pipe connection that is had nothing in common with each other by three sections internal diameters is followed successively by water inlet pipe 21, dilution tube 22 and sour distribution pipe 23 together, the tube wall of dilution tube 22 is provided with acid inlet 24, and acid distribution tube wall is provided with a plurality of shower nozzles; Wherein said ammonia-feeding pipe 3 is a three stage structure, be divided into liquid-inlet pipe 31, vaporization chamber 33 and distribution piping 34, vaporization chamber 33 is a containment cylinder, the exit end of liquid-inlet pipe 31 is arranged on the middle part of vaporization chamber 33, the axially parallel of the body of liquid-inlet pipe 31 and vaporization chamber 33 is connecting distribution piping 34 at the other end of vaporization chamber 33.
The sidewall of vaporization chamber is provided with steam inlet, and steam inlet is fixed with steam-pipe 32, and it is vertical with liquefied ammonia liquid-inlet pipe 31 that steam enters the direction of vaporization chamber 33, the liquefied ammonia of can effectively vaporizing.
Described distribution tube wall is provided with thrust-augmenting nozzle 35, and thrust-augmenting nozzle 35 is vertically mounted on the distribution piping 34, is offset in order to prevent thrust-augmenting nozzle 35, is provided with baffle plate 36 at the sidewall of thrust-augmenting nozzle 35, and baffle plate 36 is also fixedlyed connected with distribution piping 34.
Water inlet pipe 21 internal diameters of acid inlet tube 2 are 20~50mm, and the internal diameter of sour distribution pipe 23 is identical with the internal diameter of water inlet pipe 21, and the internal diameter of dilution tube 22 is 1.25~1.5 times of internal diameter of water inlet pipe 21, and the length of dilution tube 21 is 1500~2000mm; The diameter of acid distribution pipe 23 is 20~40mm, and length is about 1/3~1/4 of dilution tube 22 length.
The liquid-inlet pipe internal diameter is 40~80mm, and the length that liquid-inlet pipe feeds in the vaporization chamber is about 1/3~1/2 of vaporization chamber length; The steam inlet internal diameter is 80~150mm; The vaporization chamber internal diameter is 150~240mm, length 2000~3000mm; The top closure of distribution piping, internal diameter are 30~90mm, and length is 1000~1500mm.The thrust-augmenting nozzle internal diameter is 30~50mm, and length is than the short 50~100mm of the radius of granulation cylinder, and there is shower nozzle on the top, to the bending of cylinder sense of rotation.
Above-mentioned embodiment only is explanation technical conceive of the present utility model and characteristics; its purpose is to allow the personage that is familiar with this technology can understand content of the present utility model and is implemented; can not limit protection domain of the present utility model with this; all equivalences of being done according to the utility model spirit change or modify, and all should be encompassed in the protection domain of the present utility model.

Claims (4)

1. ammonia granulating cylinder, have cylindrical shell, opening for feed, ammonia-feeding pipe and acid inlet tube, acid inlet tube and ammonia-feeding pipe and cylindrical shell axially parallel, it is characterized in that: wherein said acid inlet tube structure is a syllogic, the pipe connection that is had nothing in common with each other by three sections internal diameters together, be followed successively by water inlet pipe, dilution tube and sour distribution pipe, the tube wall of dilution tube is provided with acid inlet, and acid distribution tube wall is provided with a plurality of shower nozzles; Described ammonia-feeding pipe is a three stage structure, be divided into liquid-inlet pipe, vaporization chamber and distribution piping, vaporization chamber is a containment cylinder, and the exit end of liquid-inlet pipe is arranged on the middle part of vaporization chamber, the body of liquid-inlet pipe and the axially parallel of vaporization chamber are connecting distribution piping at the other end of vaporization chamber.
2. ammoniation-granulation tube according to claim 1 is characterized in that: the sidewall of described vaporization chamber is provided with steam inlet.
3. ammoniation-granulation tube according to claim 1 and 2 is characterized in that: described distribution tube wall is provided with thrust-augmenting nozzle.
4. ammoniation-granulation tube according to claim 3 is characterized in that: described thrust-augmenting nozzle is vertically mounted on the distribution piping.
CN2011201299065U 2011-04-28 2011-04-28 Ammonification pelleting cylinder Expired - Lifetime CN202072637U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN2011201299065U CN202072637U (en) 2011-04-28 2011-04-28 Ammonification pelleting cylinder

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN2011201299065U CN202072637U (en) 2011-04-28 2011-04-28 Ammonification pelleting cylinder

Publications (1)

Publication Number Publication Date
CN202072637U true CN202072637U (en) 2011-12-14

Family

ID=45110743

Family Applications (1)

Application Number Title Priority Date Filing Date
CN2011201299065U Expired - Lifetime CN202072637U (en) 2011-04-28 2011-04-28 Ammonification pelleting cylinder

Country Status (1)

Country Link
CN (1) CN202072637U (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102249822A (en) * 2011-04-28 2011-11-23 江苏中东化肥股份有限公司 Ammonization granulation cylinder

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102249822A (en) * 2011-04-28 2011-11-23 江苏中东化肥股份有限公司 Ammonization granulation cylinder
CN102249822B (en) * 2011-04-28 2013-06-12 江苏中东化肥股份有限公司 Ammonization granulation cylinder

Similar Documents

Publication Publication Date Title
CN103848670B (en) A kind of with the technique of phosphorus ammonium thickened pulp One-step production high-concentration compound fertilizer
CN101391934B (en) Ammoniation granulator and composite fertilizer production novel technique
CN100371238C (en) Method for producing diammonium phosphate by concentrating acid slime, and secondary ammoniation reactor
CN101428196A (en) In-hollow column intercrystalline ammonia process of desulfurization, recovery system and method thereof
CN103396195B (en) Urea sulfate reactor and application thereof
CN101717278A (en) Method for producing diammonium phosphate by concentrating semi-acidic slurry and secondary ammonization and concentration integrated device
CN202072637U (en) Ammonification pelleting cylinder
CN102249822B (en) Ammonization granulation cylinder
CN205011670U (en) Continuous production device of rotten phytic acid slowly -releasing fertilizer of sulphuric acid urea activation
CN102311294B (en) Ammonified granulation tube provided with acid distributor
CN202063847U (en) Ammonization-granulating barrel with ammonia distributor
CN102249776B (en) Ammonification granulation cylinder with ammonia distributor
CN105236369A (en) Continuously-producing system of h-type P2O5
CN202030677U (en) Ammoniation granulation cylinder with acid distributor
CN1807367A (en) Tubular reactor for sulfuric acid and ammonia
CN206108901U (en) A highly efficient reaction cauldron for diammonium phosphate production
CN203777925U (en) System for processing ammonium-containing tail gas
CN200943062Y (en) Sulfuric acid ammonia tubular reactor
CN201626923U (en) Tubular reactor for compound fertilizer granulation
CN203715529U (en) Compound fertilizer granulating machine
CN203498274U (en) Urea sulfate reactor
CN201321433Y (en) Energy-saving environmental-protection fertilizer production equipment without fuels
CN102924128B (en) Neutralization apparatus for nitric phosphate fertilizer production mother liquid ammonia neutralization process
CN203222558U (en) Cooling and dehumidification cooler for producing high-tower nitro-S-based compound fertilizer
CN215196964U (en) Tubular reactor for producing compound fertilizer by humic acid and ammonia acid method

Legal Events

Date Code Title Description
C14 Grant of patent or utility model
GR01 Patent grant
ASS Succession or assignment of patent right

Owner name: WUHAN ZHONGDONG PHOSPHATE TECHNOLOGY CO., LTD.

Free format text: FORMER OWNER: JIANGSU ZHONGDONG FERTILIZER CO., LTD.

Effective date: 20120426

C41 Transfer of patent application or patent right or utility model
COR Change of bibliographic data

Free format text: CORRECT: ADDRESS; FROM: 213153 CHANGZHOU, JIANGSU PROVINCE TO: 430415 WUHAN, HUBEI PROVINCE

TR01 Transfer of patent right

Effective date of registration: 20120426

Address after: 430415 No. 196, steam Road, Yangluo Economic Development Zone, Hubei, Wuhan

Patentee after: Wuhan Zhongdong Phosphate Technology Co.,Ltd.

Address before: Jiaxing Jiaze town Wujin District Road 213153 Jiangsu city of Changzhou province No. 138

Patentee before: Jiangsu Zhongdong Fertilizer Co., Ltd.

AV01 Patent right actively abandoned

Granted publication date: 20111214

Effective date of abandoning: 20130612

RGAV Abandon patent right to avoid regrant