CN202061516U - Associated gas hydrogen sulfide adsorption analog device for crude oil storage tank opening - Google Patents

Associated gas hydrogen sulfide adsorption analog device for crude oil storage tank opening Download PDF

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Publication number
CN202061516U
CN202061516U CN2011200988588U CN201120098858U CN202061516U CN 202061516 U CN202061516 U CN 202061516U CN 2011200988588 U CN2011200988588 U CN 2011200988588U CN 201120098858 U CN201120098858 U CN 201120098858U CN 202061516 U CN202061516 U CN 202061516U
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China
Prior art keywords
gas
hydrogen sulfide
crude oil
outlet
storage tank
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Expired - Lifetime
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CN2011200988588U
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Chinese (zh)
Inventor
周立辉
任建科
李岩
张璇
冀忠伦
张海玲
赵敏
任小荣
杨琴
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China Petroleum and Natural Gas Co Ltd
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China Petroleum and Natural Gas Co Ltd
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Priority to CN2011200988588U priority Critical patent/CN202061516U/en
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Abstract

An associated gas hydrogen sulfide adsorption analog device for a crude oil storage tank opening is applied to associated gas analog detection for oil-field crude oil. One of two gas cylinders contains a hydrogen sulfide standard gas, and the other gas cylinder contains a crude-oil associated gas. Outlets of the gas cylinders are respectively in series connection with a pressure-reducing valve, a needle valve and a rotor flow meter, and the other end of the rotor flow meter is respectively connected with inlets of a gas mixing tank. The gas mixing tank is connected with a pressure measurement meter, a temperature measurement meter and a safety valve, and a drying tower and an adsorption tower are in series connected with an outlet pipeline of the gas mixing tank. An outlet of the adsorption tower is connected with a hydrogen sulfide concentration analytical instrument, and an outlet of the hydrogen sulfide concentration analytical instrument is connected with a tail gas treatment tank. The associated gas hydrogen sulfide adsorption analog device for the crude oil storage tank opening has the advantages of being capable of performing quick analog of efficiency of hydrogen sulfide removing through a desulfurizing agent under the conditions of different associated gas compositions, different flows, different water containing and different temperatures of associated gases in a laboratory, realizing indoor assessment of desulfurizing efficiency, and simultaneously studying the release characteristics of formed crude-oil associated gas.

Description

Crude oil storage tank mouth associated gas hydrogen sulfide absorption analogue means
Technical field
The utility model relates to oil recovery technique field, oil field, particularly a kind of analogue means of crude oil accompanying gas detection.
Background technology
Hydrogen sulfide is the extremely strong toxic gas of a kind of harmfulness, when containing low in hydrogen sulphide in the air, can work the mischief to the person, can produce life harm when concentration reaches certain value, so hydrogen sulfide is one of important hidden danger of safety in production.The hydrogen sulfide gas that contains in some oil field produced crude oil, the point of release of hydrogen sulfide gas is a lot, follows a plurality of positions of crude oil production and link, crude oil storage tank open position such as particularly all kinds of storage tank gauge hatch, breather valve.Discharge in a large number because oil storage tank heating causes in the crude oil solubilised state hydrogen sulfide to be converted into gas, open wide device by tank deck and be released into atmosphere, employee's person is caused potential danger.But be to efflux just in a organized way by associated gas gases such as hydrogen sulfide are transferred to other zone at oil storage tank associated gas hydrogen sulfide administration way at present, fundamentally do not eliminate safe hidden trouble, still have potential risk.
Therefore very important to the improvement of oil storage tank associated gas hydrogen sulfide, particularly at oil storage tank mouth association air chamber, context of detection does not also have practical analogue means.
The utility model content
The purpose of this utility model is: a kind of crude oil storage tank mouth associated gas hydrogen sulfide absorption analogue means is provided, can simulates under different component associated gas composition, associated gas different flow, different water cut, the different temperatures desulfurizing agent fast to hydrogen sulfide removal efficient in the laboratory; Realize indoorly to the desulfuration efficiency evaluation, research simultaneously forms the accompanying gas with crude oil release characteristic, improves the hydrogen sulfide regulation effect.
The technical solution adopted in the utility model is: crude oil storage tank mouth associated gas hydrogen sulfide absorption analogue means, mainly form by gas cylinder, pressure-reducing valve, needle valve, spinner flowmeter, gas blending tank, drying tower, adsorption tower, pressure-measuring device, temperature measuring set, safety valve, concentration of hydrogen sulfide analytical instrument and vent gas treatment jar, it is characterized in that: described gas cylinder has two, one of them gas cylinder is equipped with hydrogen sulfide standard gas, and a gas cylinder is equipped with accompanying gas with crude oil; Outlet at two gas cylinders is in series with pressure-reducing valve, needle valve and spinner flowmeter respectively; The other end of spinner flowmeter connects the inlet of gas blending tank respectively by pipeline.Two needle valves are controlled gas flow respectively, open back gas and feed in the gas blending tank through spinner flowmeter, and two kinds of gases fully mix in the gas blending tank.The gas blending tank is connected with pressure-measuring device, temperature measuring set and safety valve by pipeline, can measure the pressure and temperature of gas in the gas blending tank.Be in series with drying tower and adsorption tower on the outlet line of gas blending tank, have pipeline to connect the inlet of concentration of hydrogen sulfide analytical instrument in the outlet of adsorption tower, the outlet of concentration of hydrogen sulfide analytical instrument connects the vent gas treatment jar by pipeline; The outlet of safety valve connects the vent gas treatment jar by pipeline.Emit from the gas blending tank through even mixed gas, by the drying tower drying, lead to adsorption tower again, gas falls hydrogen sulfide stripping to the suction-operated of hydrogen sulfide through desulfurizing agent in adsorption tower; The gas behind the adsorption tower of flowing through enters the concentration of hydrogen sulfide analytical instrument and analyzes, and discharges gas from the concentration of hydrogen sulfide analytical instrument and is introduced into the vent gas treatment jar by pipeline, removes the hydrogen sulfide gas that is not adsorbed in the gas.
Desulfurizing agent is housed in the adsorption tower.In the gas blending tank flow-stopping plate is set, increases the time that gas is flowed through in jar, the import of gas and outlet all be arranged on the gas blending tank on cover.Described pipeline adopts lucite tube; Pressure-reducing valve, needle valve, spinner flowmeter valve must have the anti-H 2 S antiseptic property.
The beneficial effects of the utility model: the utility model crude oil storage tank mouth associated gas hydrogen sulfide absorption analogue means, can in the laboratory, simulate under different component associated gas composition, associated gas different flow, different water cut, the different temperatures desulfurizing agent fast to hydrogen sulfide removal efficient, realize indoor to the desulfuration efficiency evaluation, research simultaneously forms the accompanying gas with crude oil release characteristic, and efficiently and effectively improves the hydrogen sulfide regulation effect.
Description of drawings
Fig. 1 is the utility model crude oil storage tank mouth associated gas hydrogen sulfide absorption analogue means structural representation.
Among the figure, 1-gas cylinder, 2-pressure-reducing valve, 3-needle valve, 4-spinner flowmeter, 5-gas blending tank, 6-drying tower, 7-adsorption tower, 8-pressure-measuring device, 9-temperature measuring set, 10-safety valve, 11-concentration of hydrogen sulfide analytical instrument, 12-vent gas treatment jar.
The specific embodiment
Embodiment 1: with a crude oil storage tank mouth associated gas hydrogen sulfide absorption analogue means is example, and the utility model is described in further detail.
Consult Fig. 1.The utility model crude oil storage tank mouth associated gas hydrogen sulfide absorption analogue means mainly is made up of gas cylinder 1, pressure-reducing valve 2, needle valve 3, spinner flowmeter 4, gas blending tank 5, drying tower 6, adsorption tower 7, pressure-measuring device 8, temperature measuring set 9, safety valve 10, concentration of hydrogen sulfide analytical instrument 11 and vent gas treatment jar 12.Gas blending tank 5 is cylindrical cans, and internal diameter is 400mm, jar high 400mm, and wall thickness 10mm, airtight by loam cake.In the gas blending tank 5 flow-stopping plate is set, the gas feed of gas blending tank 5 and the outlet all be arranged on gas blending tank 5 on cover.The internal diameter of drying tower 6 is 15mm, and wall thickness is 3mm, drying tower bottom gate lath spacing 4mm, and every screen bar width is 1.5mm, and screen bar height is 5mm, and drier is a silica gel.Adsorption tower 7 height are 300mm, and the tower internal diameter is 15mm, in the adsorption tower 7 desulfurizing agent is housed.Concentration of hydrogen sulfide analytical instrument 11 is CGA2610-H 2The online hydrogen sulfide analyzer of S.Dress 20%NaOH solution in the vent gas treatment jar 12.
Gas cylinder 1 has two, and one of them gas cylinder 1 is equipped with hydrogen sulfide standard gas, and a gas cylinder 1 is equipped with accompanying gas with crude oil; Be in series with a pressure-reducing valve 2, a needle valve 3 and a spinner flowmeter 4 respectively in the outlet of two gas cylinders 1; The other end of spinner flowmeter 4 connects the inlet of gas blending tank 5 respectively by pipeline; Gas blending tank 5 is connected with a pressure-measuring device 8, a temperature measuring set 9 and a safety valve 10 by pipeline, on the outlet line of gas blending tank 5, be in series with a drying tower 6 and an adsorption tower 7, the outlet of adsorption tower 7 has pipeline to connect the inlet of concentration of hydrogen sulfide analytical instrument 11, and the outlet of concentration of hydrogen sulfide analytical instrument 11 connects a vent gas treatment jar 12 by pipeline.The outlet of safety valve 10 connects on the same vent gas treatment jar 12 by pipeline.

Claims (3)

1. a crude oil storage tank mouth associated gas hydrogen sulfide adsorbs analogue means, mainly form by gas cylinder (1), pressure-reducing valve (2), needle valve (3), spinner flowmeter (4), gas blending tank (5), drying tower (6), adsorption tower (7), pressure-measuring device (8), temperature measuring set (9), safety valve (10), concentration of hydrogen sulfide analytical instrument (11) and vent gas treatment jar (12), it is characterized in that: described gas cylinder (1) has two, one of them gas cylinder (1) is equipped with hydrogen sulfide standard gas, and a gas cylinder (1) is equipped with accompanying gas with crude oil; Outlet at two gas cylinders (1) is in series with pressure-reducing valve (2), needle valve (3) and spinner flowmeter (4) respectively; The other end of spinner flowmeter (4) connects the inlet of gas blending tank (5) respectively by pipeline; Gas blending tank (5) is connected with pressure-measuring device (8), temperature measuring set (9) and safety valve (10) by pipeline, on the outlet line of gas blending tank (5), be in series with drying tower (6) and adsorption tower (7), the outlet of adsorption tower (7) has pipeline to connect the inlet of concentration of hydrogen sulfide analytical instrument (11), and the outlet of concentration of hydrogen sulfide analytical instrument (11) connects vent gas treatment jar (12) by pipeline; The outlet of safety valve (10) connects vent gas treatment jar (12) by pipeline.
2. crude oil storage tank mouth associated gas hydrogen sulfide absorption analogue means according to claim 1, it is characterized in that: adsorption tower is equipped with desulfurizing agent in (7).
3. crude oil storage tank mouth associated gas hydrogen sulfide according to claim 1 absorption analogue means, it is characterized in that: the gas blending tank is provided with flow-stopping plate in (5), the gas feed of gas blending tank (5) and outlet all be arranged on gas blending tank (5) on cover.
CN2011200988588U 2011-04-07 2011-04-07 Associated gas hydrogen sulfide adsorption analog device for crude oil storage tank opening Expired - Lifetime CN202061516U (en)

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CN2011200988588U CN202061516U (en) 2011-04-07 2011-04-07 Associated gas hydrogen sulfide adsorption analog device for crude oil storage tank opening

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Application Number Priority Date Filing Date Title
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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104330349A (en) * 2014-10-17 2015-02-04 江阴利鑫环保科技有限公司 Hydrogen induced crack (HIC) test device
CN104897844A (en) * 2014-03-07 2015-09-09 中国石油化工股份有限公司 Crude oil produced hydrogen sulfide on-line monitoring experimental device
CN107655866A (en) * 2017-08-11 2018-02-02 新地能源工程技术有限公司 A kind of desulfurizing agent evaluating apparatus and method
CN113090867A (en) * 2020-01-09 2021-07-09 中国石油天然气股份有限公司 Crude oil conveying pipeline pipe cleaning and gas stripping simulation equipment and method

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104897844A (en) * 2014-03-07 2015-09-09 中国石油化工股份有限公司 Crude oil produced hydrogen sulfide on-line monitoring experimental device
CN104330349A (en) * 2014-10-17 2015-02-04 江阴利鑫环保科技有限公司 Hydrogen induced crack (HIC) test device
CN107655866A (en) * 2017-08-11 2018-02-02 新地能源工程技术有限公司 A kind of desulfurizing agent evaluating apparatus and method
CN113090867A (en) * 2020-01-09 2021-07-09 中国石油天然气股份有限公司 Crude oil conveying pipeline pipe cleaning and gas stripping simulation equipment and method

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Granted publication date: 20111207

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