CN202052349U - Ultrasonic wave and microwave synergy reinforcing circulation device for extracting supindus-saponin - Google Patents
Ultrasonic wave and microwave synergy reinforcing circulation device for extracting supindus-saponin Download PDFInfo
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- CN202052349U CN202052349U CN2011200851496U CN201120085149U CN202052349U CN 202052349 U CN202052349 U CN 202052349U CN 2011200851496 U CN2011200851496 U CN 2011200851496U CN 201120085149 U CN201120085149 U CN 201120085149U CN 202052349 U CN202052349 U CN 202052349U
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Abstract
The utility model discloses an ultrasonic wave and microwave synergy reinforcing circulation device for extracting supindus-saponin. The device is sequentially connected with an ultrasonic wave reinforcing microwave outer circulation extracting system, a microwave decompression outer circulation concentration system, a concentrated solution continuous centrifugal separation system and a spray drying system in series, wherein a plurality of microwave generators and a plurality of ultrasonic wave generators are arranged on the lower half portion of an ultrasonic wave reinforcing microwave outer circulation extracting tank, at least one layer of lifting baskets used for placing soapberry peels are movably arranged in the ultrasonic wave reinforcing...outer circulation extracting tank, and 20-200 meshes of sieving holes are arranged on both the bottom and the cylindrical surface of the lifting baskets made of polytetrafluoroethylene materials. An extracting tank and a concentrating tank of the device adopt a microwave heating structure without a jacket to replace a steam jacket heating structure or a water bath jacket heating structure, so that the jacket structure is saved, equipment manufacture cost is reduced, heating rate is fastened, energy consumption is reduced, and the device is easy to operate and realize industrialization.
Description
Technical field
The utility model relates to a kind of extractive technique of sapindoside, is that a kind of ultrasonic wave and microwave cooperating are strengthened the equipment that sapindoside is extracted in circulation specifically.
Background technology
Sapindoside is the main component of wild deciduous tree sapindaceous plant soapberry pericarp, mainly comprises with the hederagenin being three obedient saponins (I), sequiterpene glucosides class (II), fat oil and the protein of basic framework.It is a kind of natural nonionic surface active agent, and dirt-removing power is strong, and foam is abundant, green non-pollution, and have and antibioticly whiten, tender skin, speckle removing, acne removing, prevent and treat advantage such as skin disease.Sapindoside is a kind of pure natural product, can 100% high-fall separating, and long-term use can not produce and any human body and the harmful residue of environment be can be applicable to the daily use chemicals industry, particularly in washing and the cosmetics.
At present, few about the report of sapindoside extracting method and equipment both at home and abroad, manufacturer of domestic existing a few family all uses jacket type extractor and solvent recovery jar, adopt the mode of steam or water-bath heating, and employing directly feeds intake to extractor, the mode of filtering with filter cloth again after extraction finishes, have equipment processing difficulties, manufacturing cost height, extraction time is long, energy consumption is high, when filtering filter screen easily stop up, the easily sticking wall of material when floccule is easily residual, dry, problem such as product purity is low, recovery rate is low.Though, Chinese patent 200910115096.5 discloses a kind of continuous extraction equipment and production technology of sapindoside, but it still continues to use traditional chuck extractor and concentration tank, adopt the Steam Heating mode, problem such as still have device fabrication cost height, energy consumption height, extraction time is long, recovery rate is low.Under present green low-carbon economy and the efficient fast situation that production in enormous quantities is more and more given prominence to, this traditional mode of production obviously lacks the market competitiveness.
Summary of the invention
The utility model purpose is to overcome above-mentioned the deficiencies in the prior art part, for a kind of manufacturing cost of process specialized designs ultrasonic wave and microwave cooperating low, simple to operate relatively that collection extracts, concentrates, centrifugation, spray-drying and solvent recovery are one strengthened the equipment that sapindoside is extracted in circulation.
The purpose of this utility model is to be achieved through the following technical solutions:
A kind of ultrasonic wave and microwave cooperating are strengthened the equipment that sapindoside is extracted in circulation, it is characterized in that: this equipment comprises ultrasonic wave and microwave cooperating reinforcement outer circulating extracting system, microwave decompression outer circulation concentration systems, concentrate continuous centrifugal separation system and the spray drying system of series connection successively, wherein to strengthen the composition and the annexation of outer circulating extracting system and microwave decompression outer circulation concentration systems as follows for ultrasonic wave and microwave cooperating, and following annexation is by conveying pipeline UNICOM:
Described ultrasonic wave and microwave cooperating are strengthened the outer circulating extracting system, comprise: ultrasonic wave and microwave cooperating are strengthened outer circulating extracting jar, microwave generator, supersonic generator, extractor outer circulation pump, high-order solvent tank, high-order extract storage tank, low level extract storage tank, condenser and air compressor, wherein at ultrasonic wave and microwave cooperating reinforcement outer circulating extracting jar Lower Half several microwave generators and supersonic generator are installed; The material liquid outlet of extractor is connected with the inlet of extractor outer circulation pump, extractor outer circulation delivery side of pump is connected with the feed liquid loop head of extractor, the outlet of high-order solvent tank and the outlet parallel connection of high-order extract storage tank are connected with the feed liquid loop head of extractor again; Extractor outer circulation delivery side of pump is connected with the inlet of high-order extract storage tank, and is connected with the feed liquid inlet of concentration tank; The condensing reflux outlet of extractor is connected with the inlet of condenser, the outlet of condenser is connected with the condensing reflux of extractor inlet, the outlet of condenser is connected with the inlet of low level extract storage tank, the outlet of low level extract storage tank is connected with the inlet of extractor outer circulation pump, and the outlet of air compressor is connected with the outlet of extractor feed liquid;
Described microwave decompression outer circulation concentration systems, comprise: microwave decompression outer circulation concentration tank, microwave generator, concentration tank outer circulation pump, solvent recovery jar, surge tank, water ring pump, high-order concentrate storage tank, condenser and magnetic valve, microwave decompression outer circulation concentration tank, two condensers, solvent recovery jar, surge tank, water ring pumps are connected successively, the Lower Half of wherein said microwave decompression outer circulation concentration tank is equipped with microwave generator, and its top is equipped with magnetic valve; The material liquid outlet of described concentration tank is connected with the inlet of concentration tank outer circulation pump, and concentration tank outer circulation delivery side of pump is connected with the feed liquid loop head of concentration tank, and concentration tank outer circulation delivery side of pump is connected with the feed liquid inlet of high-order concentrate storage tank again.
Be movably installed with one deck placement soapberry pericarp hanging basket at least in described ultrasonic wave and the microwave cooperating reinforcement outer circulating extracting jar.
All have 20～200 mesh sieve holes on the bottom of described hanging basket and the face of cylinder.
Described hanging basket is a polytetrafluoroethylmaterial material.
The described microwave generator that is installed in ultrasonic wave and microwave cooperating reinforcement outer circulating extracting jar and microwave decompression outer circulation concentration tank Lower Half respectively is 1～10, and its frequency is 1KW for 2450MHz power.
The utility model is compared with the equipment ratio with prior art has following advantage:
1, the utility model extractor and concentration tank adopt no chuck heating using microwave structure replacement steam or water-bath chuck heating arrangement, have not only saved jacket structuredly, have reduced the device fabrication cost, and have accelerated firing rate, and can cut down the consumption of energy about 20%.
2, adopt the structure of multilayer polytetrafluoroethylarticles basket charging in the utility model extractor, not only can guarantee that extractant can fully be dipped into material, avoid extracting insufficient, and saved the operation of strainer filtering and had easily problem such as obstruction of filter screen.
3, the special equipment of the utility model design, manufacturing cost is low relatively, simple to operate, is easy to industrialization.
Description of drawings
Fig. 1 is that the ultrasonic wave and the microwave cooperating of the utility model equipment strengthened outer circulating extracting system formation schematic diagram;
Fig. 2 is that the microwave decompression outer circulation concentration systems of the utility model equipment constitutes schematic diagram.
Among the figure: 1 ultrasonic wave and microwave cooperating are strengthened the outer circulating extracting jar, 1-1 extractor material liquid outlet, 1-2 extractor feed liquid loop head, the outlet of 1-3 extractor condensing reflux, 1-4 extractor condensing reflux inlet, 2 extractor outer circulation pumps, 2-1 extractor outer circulation pump discharge, 2-2 extractor outer circulation pump intake, 3 high-order solvent tanks, the high-order solvent tank outlet of 3-1,4 high-order extract storage tanks, the high-order extract storage tank outlet of 4-1, the high-order extract storage tank inlet of 4-2,5 low level extract storage tanks, the outlet of 5-1 low level extract storage tank, 5-2 low level extract storage tank inlet, 6 condensers, the 6-1 condensator outlet, the 6-2 condenser inlet, 7 air compressors, the outlet of 7-1 air compressor, 8 microwave generator A, 9 microwave temperature controller A, 10 supersonic generators, 11 hanging baskets, 12 microwaves decompression outer circulation concentration tank, 12-1 concentration tank material liquid outlet, 12-2 concentration tank feed liquid loop head, 12-3 concentration tank feed liquid inlet, 13 concentration tank outer circulation pumps, 13-1 concentration tank outer circulation pump discharge, 13-2 concentration tank outer circulation pump intake, 14 microwave generator B, 15 microwave temperature controller B, 16 solvent recovery jars, 17 surge tanks, 18 water ring pumps, 19 high-order concentrate storage tanks, the high-order concentrate storage tank of 19-1 feed liquid inlet, 20 condenser A, 21 condenser B, 22 magnetic valves
The specific embodiment
By following embodiment and accompanying drawing thereof the utility model is described in further detail, but embodiment of the present utility model is not limited thereto.
Embodiment 1
The utility model is used to realize that ultrasonic wave and microwave cooperating strengthen circulation and extract the equipment of sapindoside method and strengthen outer circulating extracting system, microwave decompression outer circulation concentration systems, concentrate continuous centrifugal separation system and spray drying system etc. by ultrasonic wave and microwave cooperating and form, and they are by conveying pipeline UNICOM successively.
The formation of described ultrasonic wave and microwave cooperating reinforcement outer circulating extracting system comprises as shown in Figure 1: ultrasonic wave and microwave cooperating reinforcement outer circulating extracting jar 1, extractor outer circulation pump 2, high-order solvent tank 3, high-order extract storage tank 4, low level extract storage tank 5, condenser 6, air compressor 7 and conveying pipeline.Described ultrasonic wave and microwave cooperating are strengthened outer circulating extracting jar 1 Lower Half uniformly-spaced annular 1～10 microwave generator A8 of installation and 1～5 supersonic generator 10, it is that microwave generator A8 and 1 frequency of 1KW is the supersonic generator 10 of 3KW for 28KHz power for 2450MHz power that present embodiment is installed 10 frequencies, and microwave generator A8 links to each other with microwave temperature controller 9 again.Following annexation is by conveying pipeline UNICOM, and described extractor material liquid outlet 1-1 is connected with extractor outer circulation pump intake 2-2, and extractor outer circulation pump discharge 2-1 is connected with extractor feed liquid loop head 1-2; High-order solvent tank outlet 3-1 and high-order extract storage tank outlet 4-1 parallel connection are connected with extractor feed liquid loop head 1-2 again; Extractor outer circulation pump discharge 2-1 is connected with high-order extract storage tank inlet 4-2, and is connected with concentration tank feed liquid inlet 12-3; Extractor condensing reflux outlet 1-3 is connected with condenser inlet 6-2, condensator outlet 6-1 is connected with extractor condensing reflux inlet 1-4, condensator outlet 6-1 is connected low level extract storage tank outlet 5-1 and extractor outer circulation pump intake 2-2 UNICOM with low level extract storage tank inlet 5-2; Air compressor outlet 7-1 is connected with extractor material liquid outlet 1-1.
The formation of described microwave decompression outer circulation concentration systems comprises as shown in Figure 2: microwave decompression outer circulation concentration tank 12, concentration tank outer circulation pump 13, microwave generator B14, microwave temperature controller B15, solvent recovery jar 16, surge tank 17, water ring pump 18, high-order concentrate storage tank 19, condenser 20, condenser 21, magnetic valve 22 and conveying pipeline; Microwave decompression outer circulation concentration tank 12, condenser A20, condenser B21, solvent recovery jar 16, surge tank 17, water ring pump 18 are connected successively by conveying pipeline.Described microwave decompression outer circulation concentrates 12 tops magnetic valve 22 is installed, Lower Half uniformly-spaced annular is installed 1～10 microwave generator B14, it is the microwave generator B14 of 1KW for 2450MHz power that present embodiment is installed 10 frequencies, and microwave generator B14 links to each other with microwave temperature controller 15 again; Concentration tank material liquid outlet 12-1 is connected with concentration tank outer circulation pump intake 13-2, and concentration tank outer circulation pump discharge 13-1 is connected with concentration tank feed liquid loop head 12-2, and concentration tank outer circulation pump discharge 13-1 is connected with high-order concentrate storage tank feed liquid inlet 19-1 again.
Described thickening temperature concentrates vacuum by magnetic valve 22 controls that are installed in microwave decompression outer circulation concentration tank 12 tops by the microwave temperature controller B15 control that links to each other with microwave generator B14.
Described ultrasonic wave and microwave cooperating are strengthened can movable install the hanging basket 11 of the polytetrafluoroethylmaterial material making of one deck band sieve aperture at least in the outer circulating extracting jar, have 20～200 mesh sieve holes on the bottom of hanging basket and the face of cylinder.Present embodiment hanging basket 11 is three layers, and sieve aperture is 100 orders.Of the present utility modelly be used to realize ultrasonic wave and microwave cooperating to strengthen circulation to extract the key step and the process conditions thereof of sapindoside method as follows:
Step 1: the outer circulating extracting under ultrasonic wave and microwave cooperating are strengthened
(1) be that 50 purpose soapberry pericarps are put into hanging basket 11 with fineness;
(2) hanging basket 11 is put into ultrasonic wave and microwave cooperating and strengthened outer circulating extracting jar 1, and throw in ultrasonic wave and microwave cooperating are strengthened outer circulating extracting jar 1 by weight percentage by high-order solvent tank 3 that soapberry pericarp and ethanol water solid-to-liquid ratio are 1: 5, the percent by volume that wherein contains ethanol in the ethanol water is 50%;
(3) open and to be positioned at ultrasonic wave and microwave cooperating to strengthen microwave generator A8 and 1 frequency of 10 of outer circulating extracting jar Lower Halves be the supersonic generator 10 of 3KW for 28KHz power, material is outer circulating extracting under ultrasonic wave and microwave cooperating invigoration effect, extract temperature and be controlled at 65 ℃, extraction time is 120 minutes, extract the extract that finishes the back acquisition and inject high-order extract storage tank 4 by extractor outer circulation pump 2, be the compressed air of 0.5Mpa to ultrasonic wave and microwave cooperating reinforcement outer circulating extracting jar 1 feeding pressure then, the extract that has in the soapberry pericarp in ultrasonic wave and the microwave cooperating reinforcement outer circulating extracting jar 1 is compressed air and blows to low level extract storage tank 5, the feeding time is 60 minutes, and the extract in high-order extract storage tank 4 and the low level extract storage tank 5 is injected microwave decompression outer circulation concentration tank 12; The outer circulation of extract realizes as follows: extract is to be flowed out by extractor material liquid outlet 1-1 under explosion-proof type extractor outer circulation pump 2 effect of 5KW at power, through conveying pipeline, by extractor feed liquid loop head 1-2, turn back to ultrasonic wave and microwave cooperating and strengthen in the outer circulating extracting jar 1, realize the outer circulation of extract.The said extracted temperature is by the microwave temperature controller A9 control that links to each other with microwave generator A8.
Step 2: microwave decompression outer circulation concentrates
(1) opening 10 frequencies simultaneously is the microwave generator B14 of 1KW and the water ring pump 18 that power is 0.5～5KW for 2450MHz power, extract outer circulation under the microwave depressurization concentrates, thickening temperature is 65 ℃, concentrated vacuum is 0.07MPa, concentration time is 60 minutes, then concentrate is injected high-order concentrate storage tank 19;
(2) outer circulation of feed liquids realizes as follows in described (1) microwave decompression outer circulation concentration tank 12: feed liquid is to be flowed out by concentration tank material liquid outlet 12-1 under concentration tank outer circulation pump 13 effects of 5KW at power, deliver to concentration tank feed liquid loop head 12-2 through conveying pipeline, return in the microwave decompression outer circulation concentration tank 12, realize the outer circulation of feed liquid.
Step 3: the concentrate continuous centrifugal separates and spray-drying
Concentrate in the high-order concentrate storage tank 19 is the GQ105 tube centrifuge through model, is that the spray drying device of ZPG-25 is dried to the sapindoside finished product through model again after the 8000r/min centrifugation, and gained sapindoside finished product purity is 61.62%.
Embodiment 2
Present embodiment ultrasonic wave and microwave cooperating are strengthened the equipment that sapindoside is extracted in circulation, and except for the following differences, other are with embodiment 1:
(1) two-layer hanging basket 11, the bottom and the face of cylinder have 200 mesh sieve holes;
(2) the uniformly-spaced annular number that microwave generator A8 is installed of described ultrasonic wave and microwave cooperating reinforcement outer circulating extracting jar 1 Lower Half is 5, the microwave decompression outer circulation concentration tank 12 Lower Halves uniformly-spaced number of annular installation microwave generator B14 also are 5, and it is 1KW that their frequency is 2450MHz power;
(3) explosion-proof type extractor outer circulation pump 2 power are 2KW;
(4) water ring pump 18 power are 2KW.
Embodiment 3
Present embodiment ultrasonic wave and microwave cooperating are strengthened the equipment that sapindoside is extracted in circulation, and except for the following differences, other are with embodiment 1:
(1) one deck hanging basket 11, and the bottom and the face of cylinder have 20 mesh sieve holes;
(2) the uniformly-spaced annular number that microwave generator A8 is installed of described ultrasonic wave and microwave cooperating reinforcement outer circulating extracting jar 1 Lower Half is 1, the microwave decompression outer circulation concentration tank 12 Lower Halves uniformly-spaced number of annular installation microwave generator B14 also are 1, and it is 1KW that their frequency is 2450MHz power; It is 50KHz that supersonic generator 10 frequencies are installed, and power is 0.5KW;
(3) explosion-proof type extractor outer circulation pump 2 power are 0.5KW;
(4) water ring pump 18 power are 0.5KW.
Claims (5)
1. ultrasonic wave and microwave cooperating are strengthened the equipment that sapindoside is extracted in circulation, it is characterized in that: this equipment comprises ultrasonic wave and microwave cooperating reinforcement outer circulating extracting system, microwave decompression outer circulation concentration systems, concentrate continuous centrifugal separation system and the spray drying system of series connection successively, wherein to strengthen the composition and the annexation of outer circulating extracting system and microwave decompression outer circulation concentration systems as follows for ultrasonic wave and microwave cooperating, and following annexation is by conveying pipeline UNICOM:
Described ultrasonic wave and microwave cooperating are strengthened the outer circulating extracting system, comprise: ultrasonic wave and microwave cooperating are strengthened outer circulating extracting jar, microwave generator, supersonic generator, extractor outer circulation pump, high-order solvent tank, high-order extract storage tank, low level extract storage tank, condenser, air compressor, wherein at ultrasonic wave and microwave cooperating reinforcement outer circulating extracting jar Lower Half several microwave generators and supersonic generator are installed; The material liquid outlet of extractor is connected with the inlet of extractor outer circulation pump, extractor outer circulation delivery side of pump is connected with the feed liquid loop head of extractor, the outlet of high-order solvent tank and the outlet parallel connection of high-order extract storage tank are connected with the feed liquid loop head of extractor again; Extractor outer circulation delivery side of pump is connected with the inlet of high-order extract storage tank, and is connected with the feed liquid inlet of concentration tank; The condensing reflux outlet of extractor is connected with the inlet of condenser, the outlet of condenser is connected with the condensing reflux of extractor inlet, the outlet of condenser is connected with the inlet of low level extract storage tank, the outlet of low level extract storage tank is connected with the inlet of extractor outer circulation pump, and the outlet of air compressor is connected with the outlet of extractor feed liquid;
Described microwave decompression outer circulation concentration systems, comprise: microwave decompression outer circulation concentration tank, microwave generator, concentration tank outer circulation pump, solvent recovery jar, surge tank, water ring pump, high-order concentrate storage tank, condenser, magnetic valve, microwave decompression outer circulation concentration tank, two condensers, solvent recovery jar, surge tank, water ring pumps are connected successively, the Lower Half of wherein said microwave decompression outer circulation concentration tank is equipped with microwave generator, and its top is equipped with magnetic valve; The material liquid outlet of described concentration tank is connected with the inlet of concentration tank outer circulation pump, and concentration tank outer circulation delivery side of pump is connected with the feed liquid loop head of concentration tank, and concentration tank outer circulation delivery side of pump is connected with the feed liquid inlet of high-order concentrate storage tank again.
2. a kind of ultrasonic wave according to claim 1 and microwave cooperating are strengthened the equipment that sapindoside is extracted in circulation, it is characterized in that: be movably installed with one deck placement soapberry pericarp hanging basket at least in described ultrasonic wave and the microwave cooperating reinforcement outer circulating extracting jar.
3. a kind of ultrasonic wave according to claim 2 and microwave cooperating are strengthened the equipment that sapindoside is extracted in circulation, it is characterized in that: all have 20～200 mesh sieve holes on the bottom of described hanging basket and the face of cylinder.
According to claim 2 or 3 described a kind of ultrasonic waves and microwave cooperating strengthen circulation extract sapindoside equipment, it is characterized in that: described hanging basket is a polytetrafluoroethylmaterial material.
5. a kind of ultrasonic wave according to claim 1 and microwave cooperating are strengthened the equipment that sapindoside is extracted in circulation, it is characterized in that: the described microwave generator that is installed in ultrasonic wave and microwave cooperating reinforcement outer circulating extracting jar and microwave decompression outer circulation concentration tank Lower Half respectively is 1～10, and its frequency is 1KW for 2450MHz power.
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| Application Number | Priority Date | Filing Date | Title |
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| CN2011200851496U CN202052349U (en) | 2011-03-28 | 2011-03-28 | Ultrasonic wave and microwave synergy reinforcing circulation device for extracting supindus-saponin |
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| CN2011200851496U CN202052349U (en) | 2011-03-28 | 2011-03-28 | Ultrasonic wave and microwave synergy reinforcing circulation device for extracting supindus-saponin |
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102225245A (en) * | 2011-03-28 | 2011-10-26 | 张海 | Method and device for circularly extracting soapnut saponin under collaborative strengthening of ultrasonic wave and microwave |
| CN103223262A (en) * | 2013-05-16 | 2013-07-31 | 北京工商大学 | Continuous ultrasonic extraction device production line |
| CN103721438A (en) * | 2013-12-31 | 2014-04-16 | 湖南省百里香天然生物制品开发有限公司 | Microwave extracting device and method for extracting herba elsholtziae |
| CN104014158A (en) * | 2014-06-20 | 2014-09-03 | 王茜南 | Ultrasonic wave and microwave extraction system with reflux devices |
| CN105521619A (en) * | 2014-09-30 | 2016-04-27 | 李肥生 | Coupled device for plant extraction |
| CN107837563A (en) * | 2017-12-20 | 2018-03-27 | 贵州浩诚药业有限公司 | A kind of Chinese medicine ultrasonic wave extraction equipment and system and Chinese medicine supersonic extracting method |
| CN108970169A (en) * | 2015-09-01 | 2018-12-11 | 王小雪 | Manifold type plant component extraction element and process |
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2011
- 2011-03-28 CN CN2011200851496U patent/CN202052349U/en not_active Expired - Lifetime
Cited By (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102225245A (en) * | 2011-03-28 | 2011-10-26 | 张海 | Method and device for circularly extracting soapnut saponin under collaborative strengthening of ultrasonic wave and microwave |
| CN102225245B (en) * | 2011-03-28 | 2013-05-22 | 张海 | Method and device for circularly extracting soapnut saponin under collaborative strengthening of ultrasonic wave and microwave |
| CN103223262A (en) * | 2013-05-16 | 2013-07-31 | 北京工商大学 | Continuous ultrasonic extraction device production line |
| CN103721438A (en) * | 2013-12-31 | 2014-04-16 | 湖南省百里香天然生物制品开发有限公司 | Microwave extracting device and method for extracting herba elsholtziae |
| CN103721438B (en) * | 2013-12-31 | 2014-12-24 | 湖南省百里香天然生物制品开发有限公司 | Microwave extracting device and method for extracting herba elsholtziae |
| CN104014158A (en) * | 2014-06-20 | 2014-09-03 | 王茜南 | Ultrasonic wave and microwave extraction system with reflux devices |
| CN105521619A (en) * | 2014-09-30 | 2016-04-27 | 李肥生 | Coupled device for plant extraction |
| CN105521619B (en) * | 2014-09-30 | 2017-06-06 | 李肥生 | For the coupling device of plant extract |
| CN108970169A (en) * | 2015-09-01 | 2018-12-11 | 王小雪 | Manifold type plant component extraction element and process |
| CN108970169B (en) * | 2015-09-01 | 2023-05-02 | 广州泽力医药科技有限公司 | Coupled plant component extraction device and process method |
| CN107837563A (en) * | 2017-12-20 | 2018-03-27 | 贵州浩诚药业有限公司 | A kind of Chinese medicine ultrasonic wave extraction equipment and system and Chinese medicine supersonic extracting method |
| CN107837563B (en) * | 2017-12-20 | 2020-01-10 | 贵州浩诚药业有限公司 | Traditional Chinese medicine ultrasonic extraction equipment and system and traditional Chinese medicine ultrasonic extraction method |
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