CN202030547U - Crystallizer for supersaturated solution of barium chloride - Google Patents
Crystallizer for supersaturated solution of barium chloride Download PDFInfo
- Publication number
- CN202030547U CN202030547U CN2011201230549U CN201120123054U CN202030547U CN 202030547 U CN202030547 U CN 202030547U CN 2011201230549 U CN2011201230549 U CN 2011201230549U CN 201120123054 U CN201120123054 U CN 201120123054U CN 202030547 U CN202030547 U CN 202030547U
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- CN
- China
- Prior art keywords
- separate chamber
- separation chamber
- main
- crystallizer
- pipeline
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- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
The utility model relates to a crystallizer for supersaturated solution of barium chloride, which is characterized by comprising a main separation chamber, a secondary separation chamber, an axial flow circulating pump, vacuum equipment, a feed opening and a discharge opening, wherein the upper end of the main separation chamber is connected with the upper end of the secondary separation chamber through a pipeline; the bottom of the secondary separation chamber is connected with the axial flow circulating pump through a pipeline; the axial flow circulating pump is connected with the main separation chamber through a pipeline; the main separation chamber and the secondary separation chamber are respectively connected with the vacuum equipment through pipelines; the feed opening is arranged at the lower end of the secondary separation chamber; and the discharge opening is arranged at the lower end of the main separation chamber. The crystallizer comprises the main separation chamber and the secondary separation chamber, so as to prolong the detention time of solution in the crystallizer and the crystallization time, increase the granularity of crystal grains, and reduce the environmental pollution. The main separation chamber of the crystallizer can separate large crystallized particles from mixed solution in time and discharge the large crystallized particles and the mixed solution to prevent pipeline blockage, which is beyond the reach of a conventional circulating cooling crystallizer.
Description
Technical field
The utility model relates to a kind of bariumchloride supersaturated solution crystallizer, belongs to the chemical industry equipment field.
Background technology
Present existing bariumchloride supersaturated solution decrease temperature crystalline device all is a separate chamber, all can not make too big separate chamber on the cost of manufacture of slave unit and the manufacture difficulty, this has just limited the crystallization time of solution in equipment must be very short, and will make bariumchloride crystallization fully separate out like this, the bariumchloride crystal grain that crystallization is simultaneously separated out is all very little, this has caused difficulty just for next operation-drying course, and the bariumchloride crystal that particle is little forms dust easily and flies away in air, cause environmental pollution.
The utility model content
According to the deficiencies in the prior art, technical problem to be solved in the utility model is: a kind of bariumchloride supersaturated solution crystallizer is provided, form by main separate chamber and time two separate chambers, separate chamber, increased the time that solution stops in equipment, increase crystallization time, increase the crystal grain granularity, reduce environmental pollution.
The technical scheme that its technical problem that solves the utility model adopts is: a kind of bariumchloride supersaturated solution crystallizer is provided, it is characterized in that comprising: main separate chamber, inferior separate chamber, the axial flow recycle pump, vacuum apparatus, opening for feed and discharge port, upper end, main separate chamber is by pipe connection time upper end, separate chamber, bottom, inferior separate chamber connects the axial flow recycle pump with crossing pipeline, the axial flow recycle pump connects main separate chamber by pipeline, main separate chamber is connected vacuum apparatus by pipeline respectively with time separate chamber, lower end, inferior separate chamber is provided with opening for feed, and lower end, main separate chamber is provided with discharge port.
Be separately installed with visor in described main separate chamber and time separate chamber.
During use, the bariumchloride supersaturated solution enters time separate chamber by opening for feed, separate in inferior separate chamber, inferior separate chamber connects vacuum apparatus, steam after the separation is taken away by vacuum, bariumchloride supersaturated solution and crystallization then are delivered to main separate chamber by pipeline by the axial flow recycle pump, main separate chamber connects vacuum apparatus equally, separate in main separate chamber that bariumchloride supersaturated solution and bariumchloride xln are discharged by the discharge port that is arranged on lower end, main separate chamber completely, enter the whizzer in the next operation, separate incomplete bariumchloride supersaturated solution and get back to time separate chamber with the pipeline that upper end, inferior separate chamber is connected by main separate chamber, circulate once more, when emitting material, again by opening for feed from raw feed, inlet amount is complementary with the blowing amount, and the control of blowing amount and inlet amount is then observed by the visor that is arranged in main separate chamber and time separate chamber.
The beneficial effects of the utility model are: be made up of main separate chamber and time two separate chambers, separate chamber, increased the time that solution stops in equipment, increase crystallization time, increase the crystal grain granularity, reduce environmental pollution; The main separate chamber of this equipment can make the crystalline macrobead in time separate with mixing solutions and discharge, and prevents to block pipeline, and this is to spread the decrease temperature crystalline device not accomplish; This equipment has also increased the area of vacuum-evaporation, makes solution just can drop to the temperature of requirement in the short period of time, has also saved vapor-liquid separating device simultaneously, has reduced the cost of manufacture of equipment.
Description of drawings
Fig. 1 is the utility model structural representation;
1 is main separate chamber among the figure; 2 is time separate chamber; 3 is the axial flow recycle pump; 4 is vacuum apparatus; 5 is opening for feed; 6 is discharge port; 7 is visor.
Embodiment
Below in conjunction with accompanying drawing embodiment of the present utility model is described further:
As described in Figure 1, the utility model comprises: main separate chamber 1, inferior separate chamber 2, axial flow recycle pump 3, vacuum apparatus 4 and opening for feed 5,1 upper end, main separate chamber is by pipe connection time 2 upper ends, separate chamber, 2 bottoms, inferior separate chamber connect axial flow recycle pump 3 with crossing pipeline, axial flow recycle pump 3 connects main separate chamber 1 by pipeline, main separate chamber 1 is connected vacuum apparatus 4 by pipeline respectively with time separate chamber 2, and 2 lower ends, inferior separate chamber are provided with opening for feed 5, and lower end, main separate chamber is provided with discharge port 6.
Be separately installed with visor 7 in main separate chamber 1 and time separate chamber 2.
During use, the bariumchloride supersaturated solution enters time separate chamber 2 by opening for feed 5, separate in inferior separate chamber 2, inferior separate chamber 2 connects vacuum apparatus 4, steam after the separation is taken away by vacuum, bariumchloride supersaturated solution and crystallization then are delivered to main separate chamber 1 by pipeline by axial flow recycle pump 3, the main separate chamber 1 same vacuum apparatus 4 that connects, separate bariumchloride supersaturated solution and of discharge port 6 discharges of bariumchloride xln completely by being arranged on 1 lower end, main separate chamber in main separate chamber 1, enter the whizzer in the next operation, separate incomplete bariumchloride supersaturated solution and get back to time separate chamber 2 with the pipeline that 2 upper ends, inferior separate chamber are connected by main separate chamber 1, circulate once more, when emitting material, again by opening for feed 5 charging again, inlet amount is complementary with the blowing amount, and the control of blowing amount and inlet amount is then observed by the visor 7 that is arranged in main separate chamber 1 and time separate chamber 2.
The utility model is made up of main separate chamber 1 and time 2 two separate chambers, separate chamber, has increased the time that solution stops in equipment, increases crystallization time, increases the crystal grain granularity, reduces environmental pollution.
Claims (2)
1. bariumchloride supersaturated solution crystallizer, it is characterized in that comprising: main separate chamber (1), inferior separate chamber (2), axial flow recycle pump (3), vacuum apparatus (4), opening for feed (5) and discharge port (6), upper end, main separate chamber (1) is by pipe connection time upper end, separate chamber (2), bottom, inferior separate chamber (2) connects axial flow recycle pump (3) with crossing pipeline, axial flow recycle pump (3) connects main separate chamber (1) by pipeline, main separate chamber (1) is connected vacuum apparatus (4) by pipeline respectively with time separate chamber (2), lower end, inferior separate chamber (2) is provided with opening for feed (5), and lower end, main separate chamber is provided with discharge port (6).
2. bariumchloride supersaturated solution crystallizer according to claim 1 is characterized in that being separately installed with visor (7) in described main separate chamber (1) and time separate chamber (2).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2011201230549U CN202030547U (en) | 2011-04-22 | 2011-04-22 | Crystallizer for supersaturated solution of barium chloride |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2011201230549U CN202030547U (en) | 2011-04-22 | 2011-04-22 | Crystallizer for supersaturated solution of barium chloride |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN202030547U true CN202030547U (en) | 2011-11-09 |
Family
ID=44892854
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2011201230549U Expired - Fee Related CN202030547U (en) | 2011-04-22 | 2011-04-22 | Crystallizer for supersaturated solution of barium chloride |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN202030547U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102745730A (en) * | 2011-04-22 | 2012-10-24 | 山东众诚钡盐股份有限公司 | Barium chloride supersaturated solution crystallizer |
-
2011
- 2011-04-22 CN CN2011201230549U patent/CN202030547U/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102745730A (en) * | 2011-04-22 | 2012-10-24 | 山东众诚钡盐股份有限公司 | Barium chloride supersaturated solution crystallizer |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| PP01 | Preservation of patent right |
Effective date of registration: 20130702 Granted publication date: 20111109 |
|
| RINS | Preservation of patent right or utility model and its discharge | ||
| PD01 | Discharge of preservation of patent |
Date of cancellation: 20130702 Granted publication date: 20111109 |
|
| PP01 | Preservation of patent right |
Effective date of registration: 20131223 Granted publication date: 20111109 |
|
| RINS | Preservation of patent right or utility model and its discharge | ||
| PD01 | Discharge of preservation of patent |
Date of cancellation: 20140623 Granted publication date: 20111109 |
|
| PP01 | Preservation of patent right |
Effective date of registration: 20140626 Granted publication date: 20111109 |
|
| RINS | Preservation of patent right or utility model and its discharge | ||
| PD01 | Discharge of preservation of patent |
Date of cancellation: 20150102 Granted publication date: 20111109 |
|
| RINS | Preservation of patent right or utility model and its discharge | ||
| C17 | Cessation of patent right | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20111109 Termination date: 20140422 |