CN201894867U - Anhydrous hydrofluoric acid rectification tower - Google Patents

Anhydrous hydrofluoric acid rectification tower Download PDF

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Publication number
CN201894867U
CN201894867U CN2010206513874U CN201020651387U CN201894867U CN 201894867 U CN201894867 U CN 201894867U CN 2010206513874 U CN2010206513874 U CN 2010206513874U CN 201020651387 U CN201020651387 U CN 201020651387U CN 201894867 U CN201894867 U CN 201894867U
Authority
CN
China
Prior art keywords
jet cover
hydrofluoric acid
anhydrous hydrofluoric
injection cap
hole
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
CN2010206513874U
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Chinese (zh)
Inventor
曹宗高
杨望军
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
HUNAN NONFERROUS CHENZHOU FLUORDE CHEMICAL CO Ltd
Original Assignee
HUNAN NONFERROUS CHENZHOU FLUORDE CHEMICAL CO Ltd
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Publication date
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Priority to CN2010206513874U priority Critical patent/CN201894867U/en
Application granted granted Critical
Publication of CN201894867U publication Critical patent/CN201894867U/en
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

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Abstract

The utility model discloses an anhydrous hydrofluoric acid rectification tower, which comprises a gas lifting hole, an injection cap, an injection cap top plate, a tower plate, a downcomer, a guide baffle plate, an overflow weir, a tower body, a skylight, support legs, injection holes and guide holes, wherein the injection cap top plate is positioned at the upper end of the injection cap; the lower edge of the injection cap is uniformly connected with 3 to 4 support legs; the injection cap is positioned at a position where a lifting hole of the tower plate is formed; a liquid flow channel is formed between the bottom surface of the injection cap and the tower plate; the injection holes are uniformly distributed on the injection cap; the guide holes are uniformly formed on the injection cap top plate; the skylight is formed between the injection cap and the injection cap top plate; and the injection cap is arranged at a position which corresponds to the gas lifting hole. The anhydrous hydrofluoric acid rectification tower has the advantages of high treatment capacity, high mass transfer efficiency, small pressure drop, high operational flexibility and the like.

Description

A kind of anhydrous hydrofluoric acid rectifying column
Technical field
The utility model relates to a kind of rectifying column, is specially a kind of anhydrous hydrofluoric acid rectifying column.
Background technology
Present rectifying column generally uses structured packing, and when in the distillation process that is used in anhydrous hydrofluoric acid, its defective is: the disposal ability of rectifying column is little, and mass-transfer efficiency is low, and pressure drop is big, and operating flexibility is little.
The utility model content
The technical problem that the utility model solved is to provide a kind of anhydrous hydrofluoric acid rectifying column, to solve the shortcoming in the above-mentioned background technology.
The technical problem that the utility model solved realizes by the following technical solutions:
A kind of anhydrous hydrofluoric acid rectifying column, comprise air rising hole, jet cover, the jet cover top board, column plate, downspout, deflector apron, downflow weir, tower body, the skylight, leg, spray-hole and pilot hole, described jet cover top board is positioned at the upper end of jet cover, described jet cover lower limb evenly is connected with 3-4 leg, described jet cover is in the position of the rise hole of column plate, leave fluid course between the bottom surface of described jet cover and the column plate, be evenly distributed with spray-hole on the described jet cover, evenly have pilot hole on the described jet cover top board, described jet cover is cylindrical or truncated cone-shaped, described jet cover top board be shaped as circle with jet cover coupling, have the skylight between described jet cover and the jet cover top board, horizontal column plate of several layers and supporting with it downspout and downflow weir are installed in the described tower body, have the plurality of rows air rising hole vertical on the described column plate with the liquid phase flow direction, on the position corresponding, jet cover is installed, and every row's jet cover is adopted as the alternate mounting means of arranging straggly of height with air rising hole.
Beneficial effect
It is big to the utlity model has disposal ability, mass-transfer efficiency height, advantage such as pressure drop is little, and operating flexibility is big.
Description of drawings
Fig. 1 is a schematic diagram of the present utility model;
Fig. 2 is the vertical view of jet cover of the present utility model;
Fig. 3 is the front view of jet cover of the present utility model.
The specific embodiment
For technological means, creation characteristic that the utility model is realized, reach purpose and effect is easy to understand, below in conjunction with concrete diagram, further set forth the utility model.
Referring to Fig. 1, Fig. 2, Fig. 3, a kind of schematic diagram of anhydrous hydrofluoric acid rectifying column, a kind of vertical view of jet cover of anhydrous hydrofluoric acid rectifying column, a kind of front view of jet cover of anhydrous hydrofluoric acid rectifying column, a kind of anhydrous hydrofluoric acid rectifying column, comprise air rising hole 1, jet cover 2, jet cover top board 3, column plate 4, downspout 6, deflector apron 7, downflow weir 9, tower body 10, skylight 11, leg 12, spray-hole 13 and pilot hole 14, described jet cover top board 3 is positioned at the upper end of jet cover 2, described jet cover 2 lower limbs evenly are connected with 3-4 leg 12, described jet cover 2 is in the position of the rise hole 1 of column plate 4, leave fluid course between the bottom surface of described jet cover 2 and the column plate 4, be evenly distributed with spray-hole 13 on the described jet cover 2, evenly have pilot hole 14 on the described jet cover top board 3, described jet cover 2 is cylindrical or truncated cone-shaped, described jet cover top board 3 be shaped as circle with jet cover 2 coupling, have skylight 11 between described jet cover 2 and the jet cover top board 3, horizontal column plate 4 of several layers and supporting with it downspout 6 and downflow weir 9 are installed in the described tower body 10, have on every layer of column plate 4 with liquid and flow the vertical plurality of rows air rising hole 1 of 8 directions, on the position corresponding, jet cover 2 is installed, and every row's jet cover 2 is adopted as the alternate mounting means of arranging straggly of height with air rising hole 1.
During operation, liquid phase 8 flows into this layer column plate 4 from the downspout 6 of last layer column plate 4, every row's jet cover 2 of flowing through flows to down on one deck column plate 4 through downspout 6 again, gas phase 5 enters in the jet cover 2 of this layer column plate 4 from the below of column plate 4 by air rising hole 1, in gas phase 5 enters jet cover 2 and when rising, liquid phase 8 enters from the fluid course of the bottom surface of jet cover 2, gas-liquid two-phase carries out violent mixing contact in jet cover 2, liquid phase 8 is broken into the drop that varies in size in a large number by gas phase 5 in contact process, after this gas-liquid mixture is spouting from the pilot hole 14 of the sidewall spray-hole 13 of jet cover 2 and bar shaped skylight 11 and jet cover top board 3, at first beat on described guiding plate washer 7 by the gas-liquid mixture that eject in skylight 11, the gas-liquid mixture that is ejected by the pilot hole on the jet cover top board 3 14 can be stopped because of the fish scale shape of pilot hole 14, in this process, drop continues to be broken, after the mixing, opening direction along deflector apron 7 or fish scale pilot hole 14 is spouting, last gas phase 5 and the drop place, space between jet cover 2 and column plate 4 is through the collision cohesion, drop captures, processes such as jet cover top board 3 captures and gas phase 5 are in the curve baffling rising centrifugation of 2 of jet covers, drop can fall back in the liquid phase 8 on the column plate 4 and flow to down on one deck column plate 4 by downspout 6 subsequently, and gas-liquid two-phase is finished mass transfer in this contact process, processes such as heat transfer.
More than show and described basic principle of the present utility model and principal character and advantage of the present utility model; the technical staff of the industry should understand; the utility model is not restricted to the described embodiments; that describes in the foregoing description and the specification just illustrates principle of the present utility model; under the prerequisite that does not break away from the utility model spirit and scope; the utility model also has various changes and modifications; these changes and improvements all fall in claimed the utility model scope, and the claimed scope of the utility model is defined by appending claims and equivalent thereof.

Claims (6)

1. anhydrous hydrofluoric acid rectifying column, comprise air rising hole, jet cover, the jet cover top board, column plate, downspout, deflector apron, downflow weir, tower body, the skylight, leg, spray-hole and pilot hole, it is characterized in that, described jet cover top board is positioned at the upper end of jet cover, described jet cover lower limb evenly is connected with 3-4 leg, described jet cover is in the position of the rise hole of column plate, leave fluid course between the bottom surface of described jet cover and the column plate, be evenly distributed with spray-hole on the described jet cover, evenly have pilot hole on the described jet cover top board, have the skylight between described jet cover and the jet cover top board, on the position corresponding, jet cover is installed with air rising hole.
2. a kind of anhydrous hydrofluoric acid rectifying column according to claim 1 is characterized in that described jet cover is cylindrical or truncated cone-shaped.
3. a kind of anhydrous hydrofluoric acid rectifying column according to claim 1, described jet cover top board be shaped as circle with jet cover coupling.
4. a kind of anhydrous hydrofluoric acid rectifying column according to claim 1 is equipped with horizontal column plate of several layers and supporting with it downspout and downflow weir in the described tower body.
5. a kind of anhydrous hydrofluoric acid rectifying column according to claim 1 has the plurality of rows air rising hole vertical with the liquid phase flow direction on the described column plate.
6. a kind of anhydrous hydrofluoric acid rectifying column according to claim 1, every row's jet cover are adopted as the alternate mounting means of arranging straggly of height.
CN2010206513874U 2010-12-10 2010-12-10 Anhydrous hydrofluoric acid rectification tower Expired - Lifetime CN201894867U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN2010206513874U CN201894867U (en) 2010-12-10 2010-12-10 Anhydrous hydrofluoric acid rectification tower

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN2010206513874U CN201894867U (en) 2010-12-10 2010-12-10 Anhydrous hydrofluoric acid rectification tower

Publications (1)

Publication Number Publication Date
CN201894867U true CN201894867U (en) 2011-07-13

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CN2010206513874U Expired - Lifetime CN201894867U (en) 2010-12-10 2010-12-10 Anhydrous hydrofluoric acid rectification tower

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104524802A (en) * 2014-11-25 2015-04-22 南通苏通分离工程科技有限公司 Multistage baffle cap column plate

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104524802A (en) * 2014-11-25 2015-04-22 南通苏通分离工程科技有限公司 Multistage baffle cap column plate

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C14 Grant of patent or utility model
GR01 Patent grant
CX01 Expiry of patent term
CX01 Expiry of patent term

Granted publication date: 20110713

DD01 Delivery of document by public notice
DD01 Delivery of document by public notice

Addressee: Patent director of Hunan Nonferrous Chenzhou fluorochemical Co.,Ltd.

Document name: Notice of expiration of patent right