Dalmatian chrysanthemum cycling extraction device
Technical field
The utility model belongs to effective ingredient abstraction technique field in the plant, relates to the device of the cycling extraction of a kind of Dalmatian chrysanthemum plant.
Background technology
In the prior art, adopt mode intermittently to carry out, promptly in single jar, extract the extraction of Dalmatian chrysanthemum plant, extraction equipment includes an extractor, feed tube is installed above jar, below drain pipe is installed, on feed tube and drain pipe, stop valve is installed.When extracting work, earlier raw material is packed in the extractor, extractant to be put into, raw material forms extract soak certain hour in solvent after, and extract is put into by drain pipe, is transported in the enrichment process to concentrate, and recycles solvent; Raw material carries out the secondary immersion through putting into novel solvent after once immersion extracts again, and the extract that secondary soaks is put into by drain pipe, is transported in the enrichment process to concentrate, and recycles solvent; Also will put into novel solvent through the raw material of reextraction and carry out three immersions, the extract of three immersions is put into by drain pipe, is transported in the enrichment process to concentrate, and recycles solvent, and raw material is regarded the residue discharge after soaking through three times.In the prior art, often use a plurality of extractors to be connected in parallel and produce, to improve product yield.
In the prior art, during producing, the extraction of Dalmatian chrysanthemum raw material has following shortcoming:
1, in three extraction processes, the extract that at every turn soaks out all will carry out concentration, could reclaim and use solvent, and it is longer to reclaim the used time of solvent, causes the production cycle to increase, and energy consumption increases, and during workload increased, production efficiency descended.
2, three extraction gained extract effective component contents differ bigger, have influenced follow-up concentration technology, cause the crude extract quality after concentrating to differ bigger, influence the subsequent product quality of stability.
The utility model content
For solving in the prior art, to the extraction of Dalmatian chrysanthemum plant material effective ingredient the time, the solvent recovery number of times of existence is too much, it is longer to reclaim elapsed time, the crude extract quality differs bigger problem, and the utility model provides a kind of Dalmatian chrysanthemum cycling extraction device, and its technical scheme is as follows:
Dalmatian chrysanthemum cycling extraction device, comprise four extractors, be A jar, B jar, C jar and D jar, feed tube and drain pipe all are installed on each extractor, stop valve all is installed on feed tube and the drain pipe, the feed tube on the extractor all is communicated with the solvent inlet pipe, drain pipe on the extractor all goes out pipe with solvent and is communicated with, solvent inlet pipe and solvent go out Guan Shangjun to be had by main valve, and solvent inlet pipe and solvent go out also to be communicated with the solvent circulation pipe between the pipe, and stop valve and high-pressure pump are arranged on the solvent circulation pipe.
Adopt technique scheme, the duty by stop valve in the control device and high-pressure pump can realize that extractant circulates between four extractors.
During this device busy: can realize three kinds of different extraction processes, first kind is: the new raw material in jar separates through directly putting into separation circuit behind the single extraction of solvent; Second kind is: the raw material through behind the single extraction, carry out reextraction with novel solvent, and extraction fluid is put into next extractor, and the new raw material in the jar is extracted first, and extract is put into separation circuit and is separated afterwards; The third is: through the raw material of twice extraction, putting into novel solvent again carries out in extraction for the third time, the gained extract is put into next extractor the raw material that jar had extracted is once carried out the extraction second time, the gained extract is put into next jar again the new raw material of jar is extracted first, and extract is put into separation circuit and separated afterwards.
Because in traditional batch production, in three extraction processes, same solvent can only soak primary material, and each extract all will concentrate, and reclaims and uses solvent; After adopting technical solutions of the utility model, same solvent can be to carrying out three times immersion to raw materials for production in different jars, and three times immersion back solvent just concentrates recycling, therefore, solvent concentrates the number of times that reclaims and significantly reduces, and has shortened the production cycle, has reduced production cost and has known.
In the technical program, solvent is in the cycling extraction process, all to raw material carried out first, secondary and three times extraction, the effective component content that extracts in the solvent is more approaching, extract operation when concentrated is more unified, help concentrating to be operated under the unified technical standard carrying out, the crude extract quality index that concentrates the back gained is more approaching, helps improving the quality of products in the subsequent production.
Below in conjunction with the drawings and specific embodiments the utility model is described in further detail:
Description of drawings
Fig. 1 is a structure diagram of the present utility model.
The specific embodiment
Embodiment one: subcritical continuous extraction Dalmatian chrysanthemum device as shown in Figure 1, comprise four extractors, it is the A jar, the B jar, C jar and D jar, feed tube (1) and drain pipe (2) all are installed on each extractor, on feed tube (1) and the drain pipe (2) stop valve (3) is installed all, feed tube on the extractor (1) all is communicated with solvent inlet pipe (4), drain pipe on the extractor (2) all goes out pipe (5) with solvent and is communicated with, solvent inlet pipe (4) and solvent go out on the pipe (5) all to be had by main valve (6), it is characterized in that: solvent inlet pipe (4) and solvent go out between the pipe (5) also to be communicated with solvent circulation pipe (8), and circulating valve (9) and high-pressure pump (7) are housed on the solvent circulation pipe (8).