The utility model content
In order to address the above problem, the purpose of this utility model be to provide energy consumption low, be suitable for suitability for industrialized production, especially for the magnetic agitation reactor of palmitoyl chloride preparation.
The technical solution of the utility model is:
A kind of magnetic agitation reactor comprises pedestal, motor, permanent magnet and ceramic reactor,
Described magnetic agitation reactor also comprises stirring frame and back shaft, and the stirring frame is enclosed within and is arranged in the ceramic reactor on the back shaft;
Described permanent magnet is the magnetic framework, is made up of top frame, underframe, left frame and right frame, and permanent magnet can be center 360 degree rotations with the rotating shaft on the motor by driven by motor;
Described ceramic reactor is the sealed shell of tank that is provided with feeding mouth and discharging opening, and the discharging opening place is provided with valve; Permanent magnet is set in the ceramic reactor outside, between permanent magnet and the ceramic reactor, all leave magnetic field space between ceramic reactor and the stirring frame;
Preferably, described stirring frame is fixed on the back shaft by locating part, and the magnet of answering that stirs frame can be center 360 degree rotations with the back shaft.
Preferably, described stirring frame is fixed on the back shaft by locating part, and back shaft is fixed in the ceramic reactor by the tripod that is arranged on the ceramic reactor inside bottom wall, and stirring frame can be center 360 degree rotations with the back shaft.
Preferably, the left frame of described permanent magnet and right frame are magnetic.
Preferably, described magnetic agitation reactor is the vertical response still, and the top of back shaft is connected with the roof inboard of ceramic reactor, and the bottom of back shaft is passed two crossbeams stirring frame and linked to each other with tripod on being arranged on the ceramic reactor inside bottom wall.
Preferably, described magnetic agitation reactor is the horizontal reacting still, and an end of back shaft is by driven by motor, and links to each other with left bracing frame on the pedestal; The other end of back shaft runs through permanent magnet, ceramic reactor, stirring frame successively and links to each other with right bracing frame on the pedestal.
Permanent magnet of the present utility model not only is confined to the square frame body, also can adapt with ceramic reactor, the framework of other shapes; In order to make the stirring in the ceramic reactor more even, the ceramic reactor internal pressure is excessive when preventing high rotating speed, the bumping of the liquid that reacts, and can also put in ceramic reactor can the auxiliary son of free movable stirring.
The utility model comprises motor, permanent magnet and ceramic reactor, because permanent magnet is a framework, preferably two of framework side frames are magnetic, thereby when the large-scale reaction vessel of needs, also only needs the driven by motor framework to rotate, so energy consumption is less relatively; Because in the course of reaction, permanent magnet can be center 360 degree rotations with the rotating shaft on the motor by driven by motor, the stirring frame that drives in the ceramic reactor is center 360 degree rotations with the back shaft, and mechanical oscillation are little, rotating excitation field is stable, and reaction liquid mixes; Because ceramic reactor is a sealed shell of tank, can not suck air in the course of reaction, the situation of reaction liquid bumping also can not occur, has guaranteed the quality of course of reaction when preventing bumping, and environmentally friendly, especially is suitable for suitability for industrialized production.
The specific embodiment
Below in conjunction with accompanying drawing the specific embodiment of the present utility model is described in further detail.
Implementation column 1
A kind of vertical magnetic agitation reactor, comprise pedestal 9, motor 5, permanent magnet 3, ceramic reactor 2, stir frame 1 and back shaft 4, from inside to outside, be followed successively by and stir frame, ceramic reactor, permanent magnet, the stirring frame is enclosed within and is arranged in the ceramic reactor on the back shaft;
Described permanent magnet is the magnetic framework, is made up of top frame 32, underframe 34, left frame 33 and right frame 31, and permanent magnet can be center 360 degree rotations with the rotating shaft on the motor 51 by driven by motor; Wherein, the left frame of permanent magnet and right frame are magnetic.
Described ceramic reactor is the sealed shell of tank that is provided with feeding mouth 201 and discharging opening 202, and the discharging opening place is provided with valve 43; Permanent magnet is set in the ceramic reactor outside, between permanent magnet and the ceramic reactor, all leave magnetic field space 8 between ceramic reactor and the stirring frame;
Described stirring frame answers the magnet 13 and the right side to answer magnet 11 to form by head piece 12, cross member 14, a left side, by locating part 6, head piece and cross member is fixed on the back shaft, and it can be center 360 degree rotations with the back shaft that the left side on the stirring frame answers the magnet and the right side to answer magnet.
The top 41 of described back shaft is connected with roof 22 inboards of ceramic reactor, and the bottom 42 of back shaft is passed successively and stirred two crossbeams of frame, the diapire 24 of ceramic reactor, the underframe of permanent magnet and link to each other with pedestal 9.
Implementation column 2
A kind of vertical magnetic agitation reactor comprises motor 5, permanent magnet 3, ceramic reactor 2, stirs frame 1 and back shaft 4, from inside to outside, is followed successively by and stirs frame, ceramic reactor, permanent magnet, and the stirring frame is enclosed within and is arranged in the ceramic reactor on the back shaft;
Described permanent magnet is the magnetic framework, is made up of top frame 32, underframe 34, left frame 33 and right frame 31, and permanent magnet can be center 360 degree rotations with the rotating shaft on the motor 51 by driven by motor; Wherein, the left frame of permanent magnet and right frame are magnetic.
Described ceramic reactor is the sealed shell of tank that is provided with feeding mouth 201 and discharging opening 202, and the discharging opening place is provided with valve 43; Permanent magnet is set in the ceramic reactor outside, between permanent magnet and the ceramic reactor, all leave magnetic field space 8 between ceramic reactor and the stirring frame;
Described stirring frame answers the magnet 13 and the right side to answer magnet 11 to form by head piece 12, cross member 14, a left side, stirs frame by locating part 6, and head piece and cross member are fixed on the back shaft; Back shaft is fixed in the ceramic reactor by the tripod 7 that is arranged on the ceramic reactor inside bottom wall, and back shaft passes head piece and cross member, and it can be center 360 degree rotations with the back shaft that the left side on the stirring frame answers the magnet and the right side to answer magnet.
The top 41 of described back shaft is connected with roof 22 inboards of ceramic reactor, and the bottom 42 of back shaft is passed successively and stirred two crossbeams of frame and link to each other with tripod on being arranged on the ceramic reactor inside bottom wall.
The utility model utilizes permanent magnet to realize contactless indirect drive, when the driven by motor permanent magnet rotates, rotation by 360 degree of magnetic on left frame on the permanent magnet and the right frame, utilize the magnetic field effect of stirring in magnetic and the ceramic reactor between the frame, the magnetic line of force passes the left side that the ceramic reactor of isolation drive to stir on the frame and answers the magnet and the right side to answer magnet along the synchronous 360 degree rotations of back shaft, reaction solution reacts under the stirring of stirring frame, stirring in the course of reaction is soft and even, be complete closed in rotary course owing to ceramic reactor simultaneously, thereby can reach leak free course of reaction.
Implementation column 3
A kind of horizontal magnetic agitation reactor, comprise pedestal 9, motor 5, permanent magnet 3, ceramic reactor 2, stir frame 1 and back shaft 4, from inside to outside, be followed successively by and stir frame, ceramic reactor, permanent magnet, back shaft passes permanent magnet, runs through ceramic reactor simultaneously and links to each other with pedestal with the stirring frame;
Described permanent magnet is the magnetic framework, is made up of top frame 31, underframe 33, left frame 32 and right frame 34, and wherein, the top frame of permanent magnet and underframe are magnetic.The top frame of permanent magnet and underframe can be center 360 degree rotations with the back shaft by driven by motor.
Described ceramic reactor is the sealed shell of tank that is provided with feeding mouth 201 and discharging opening 202, and the discharging opening place is provided with valve 43; Permanent magnet is set in the ceramic reactor outside, between permanent magnet and the ceramic reactor, all leave magnetic field space 8 between ceramic reactor and the stirring frame;
Described stirring frame answers magnet 11, the end to answer magnet 13, left frame 12 and correct frame 14 to form by the top, by locating part 6, left frame and correct frame is fixed on the back shaft, and it can be center 360 degree rotations with the back shaft that the top of stirring frame answers the magnet and the end to answer magnet.
One end 41 of described back shaft is by driven by motor, and links to each other with left bracing frame 91 on the pedestal; The right frame that the other end 42 of back shaft runs through right side wall 24, the permanent magnet of the left side wall 22 of left frame, the ceramic reactor of permanent magnet, the left frame that stirs frame, the correct frame that stirs frame, ceramic reactor successively links to each other with right bracing frame 92 on the pedestal.
The utility model utilizes permanent magnet to realize contactless indirect drive, when the driven by motor permanent magnet rotates, rotation by top frame on the permanent magnet and underframe 360 degree, utilize the magnetic field effect of stirring in permanent magnet and the ceramic reactor between the frame, the magnetic line of force passes the top that the ceramic reactor of isolation drive to stir on the frame and answers magnet, the end, answer magnet along the synchronous 360 degree rotations of back shaft, reaction solution reacts under the stirring of stirring frame, stirring in the course of reaction is soft and even, be complete closed in rotary course owing to ceramic reactor simultaneously, thereby can reach leak free course of reaction.
The foregoing description, it is preferred embodiment of the present utility model, be not to be used for limiting the utility model practical range,, all should be included within the utility model claim scope so all equivalences of being done with the described structure of the utility model claim, feature and principle change or modify.