A kind of hydrolysis kettle
Technical field
The utility model belongs to technical field of chemical, particularly a kind of hydrolysis kettle with gas-filtering device.
Background technology
Furfural is a kind of sparkling and crystal-clear transparency liquid of light yellow or amber no mechanical impurity, and as important organic chemical industry's product, it is widely used in fields such as synthetic resin, petroleum refining, fuel, medicine and light industry.Furfural adopts the plant fiber material preparation of being rich in pentosan to produce, as raw materials such as corncob, cotton seed hulls, oil tea shell, sunflower pericarp, bagasse and rice husks.At present, traditional furfural production technology is as follows substantially: acid, hydrolysis are pulverized, mixed to plant fiber material, and the furfural gas that hydrolysis produces becomes furfural stoste after condensation, furfural stoste again through distillation, neutralization, after refining the furfural finished product.Owing to contain the solid impurity of furfural dregs class in the furfural gas that hydrolysis produces, enter subsequent processing again after these solid impurities need being removed.The solid impurity of furfural gas is to connect the cyclone dust removal scummer to remove behind hydrolysis kettle at present, also need to increase cleaner, and power consumption is big, it is low that impurity is removed rate, below 80%, increase the distillation load and the cleaning frequency (per 20 days 1 time) of subsequent processing like this, increased the production cost of furfural greatly.
The utility model content
The purpose of this utility model provides a kind of simple in structure, impurity and removes the high hydrolysis kettle of rate.
For achieving the above object, the technical solution of the utility model is: a kind of hydrolysis kettle, comprise the still mouth on kettle, kettle top and the kettle cover on the still mouth, and described still oral-lateral wall is provided with aldehyde gas discharge pipe, is provided with the filter that is tightly connected with aldehyde gas discharge pipe in the still mouth.
Described filter comprises the tubular filter skeleton, filters skeleton one end/side and sets out gas port, and the place, gas outlet outwards is provided with escape pipe; Filter on the skeleton and offer aldehyde gas passage, aldehyde gas passage is coated with one deck screen pack outward at least.
The escape pipe of described filter is nested in the aldehyde gas discharge pipe.
Gas outlet opposite end/side is provided with the lifting part on the described filtration skeleton, and the lifting part comprises and is connected in the connecting rod that links to each other between two blocks of side plates filtering on the skeleton and the side plate.
Aldehyde gas discharge pipe opposite side is provided with filter mounting in the described still mouth, and the lifting part is overlapped on the filter mounting.
Described filtration skeleton is circular or square linear tube.
Described filtration skeleton is circular or square ring pipe.
Described aldehyde gas passage is a strip, is distributed on to filter on the skeleton sidewall.
Described screen pack is coated on and filters on the skeleton sidewall, and screen pack is three layers, and the mesh diameter ecto-entad of three layer filtration net reduces gradually.
Compared with prior art, the utlity model has following beneficial effect:
1, the utility model is installed filter in the still mouth, and is simple in structure, and impurity is removed rate up to 95%, and power consumption is few, and is durable in use, saves aldehyde gas production cost, and alleviated the live load of the refining workshop section of furfural production greatly, reduced the equipment cleaning frequency.
2, filter is arranged between aldehyde gas discharge pipe and the filter mounting, installs, dismounting is easy, flexible operation; The escape pipe of filter is nested in the aldehyde gas discharge pipe, realizes being tightly connected, and prevents that gas from leaking, and improves furfural gas discharge efficiency.
3, on the filtration skeleton, coat screen pack,, prevent that furfural dregs dirt from entering aldehyde feed channel, good filtration effect in order to filtering furfural dregs dirt; The mesh diameter ecto-entad of three layer filtration net reduces gradually, and furfural gas is filtered layer by layer, improves impurity and removes rate.
4, be provided with the lifting part filtering on the skeleton, be convenient to the carrying of filter, mounting box is deposited.
Description of drawings
Fig. 1 is a structural representation of the present utility model;
Fig. 2 is the structural representation of the utility model middle filtrator embodiment 1;
Fig. 3 is the A-A cutaway view of Fig. 2;
Fig. 4 is the structural representation of the utility model middle filtrator embodiment 2.
The specific embodiment
Embodiment 1
Hydrolysis kettle as shown in Figure 1, it comprises the still mouth 7 on kettle 6, kettle 6 tops and the kettle cover 8 on the still mouth 7, is provided with aldehyde gas discharge pipe 10 on still mouth 7 sidewalls, aldehyde gas discharge pipe 10 opposite sides are provided with filter mounting 9 in the still mouth 7, play a supporting role.Be provided with filter 1 between aldehyde gas discharge pipe 10 and filter mounting 9, filter 1 is tightly connected with aldehyde gas discharge pipe 10, makes furfural gas discharge kettle 6 by filter 1 through aldehyde gas discharge pipe 10.
Filter as shown in Figures 2 and 3, it comprises tubular filter skeleton 11, filtering skeleton 11 is circular linear tube, and sealed at both ends, sets out gas port 16 at filtration skeleton 11 1 ends, 16 places outwards are provided with escape pipe 12 in the gas outlet, the internal diameter of the external diameter of escape pipe 12 and aldehyde gas discharge pipe 10 adapts, and escape pipe 12 is nested in the aldehyde gas discharge pipe 10, realizes being tightly connected, prevent that gas from leaking, improve furfural gas discharge efficiency.Aldehyde gas passage 14, the six place's aldehyde gas passages 14 that offer six director's strips on filtration skeleton 11 circumferential wall are distributed on and filter on skeleton 11 circumferential wall, as the filtration channel of furfural gas; Simultaneously, filtering coating three layer filtration net 15 on skeleton 11 circumferential wall,, prevent that furfural dregs dirt from entering the aldehyde feed channel in order to filtering furfural dregs dirt.The mesh diameter ecto-entad of three layer filtration net 15 reduces gradually, and furfural gas is filtered layer by layer, improves impurity and removes rate.Be provided with lifting part 13 in the opposite end of filtering escape pipe 12 on the skeleton 11 or gas outlet 16, lifting part 13 comprises and is connected in the connecting rod 18 that links to each other between two blocks of side plates 17 filtering on the skeleton 11 and the side plate 17.The outside of above-mentioned side plate 17 is wedge shape wide at the top and narrow at the bottom, and is downward more fixing firm more when side plate 17 and filter mounting 9 are joined.For side plate 17 and filter mounting 9 are matched, filter mounting 9 is set to the shape that the wedge shape with side plate 17 adapts.
Specifically, the mesh diameter of three layer filtration net 15 is respectively 14-18mm, 6-10mm and 1-3mm.
Use of the present utility model is: 1, open kettle cover 8, in kettle 6, fill plant fiber material, as corncob, hook the front and back ends of filter 1 respectively with two U-shaped hooks, escape pipe 12 1 ends of filter 1 are fallen and aim at, insert in the aldehyde gas discharge pipe 10, put down the other end then gently, contact with filter mounting 9, promptly finish the installation of filter 1 up to lifting part 13.2, close kettle cover 8, the operation that is hydrolyzed, furfural gas is discharged through aldehyde gas discharge pipe 10 by filter 1 during the hydrolysis.3, after hydrolysis finishes, utilize the U-shaped hook to hook the front and back ends of filter 1, earlier lifting part 13 1 ends are lifted slightly, and move, can take off filter 1 to the back upper place.4, clean the filter 1 that takes off, the furfural dregs dirt on screen pack 15 surfaces is removed totally, in order to using next time.
Embodiment 2
As shown in Figure 1 and Figure 4, the difference of itself and embodiment 1 is: the filtration skeleton 11 of filter 1 be shaped as circular loop pipe, a side of loop pipe sets out gas port 16,16 places, gas outlet are provided with escape pipe 12; Filter skeleton 11 opposite sides and be provided with lifting part 13.Offer rectangular circular-arc aldehyde gas passage 14 on filtration skeleton 11 ring-type circumferential wall, aldehyde gas passage 14 is distributed on and filters on skeleton 11 circumferential wall, is filtering skeleton 11 outer walls coating three layer filtration net 15 simultaneously.
Be not limited to the foregoing description: screen pack 15 shapes of the present utility model also can adapt with aldehyde gas passage 14, and screen pack 15 only is coated on aldehyde gas passage 14, to save the screen pack material; Filter skeleton 11 and also can be other shapes beyond circular, as square, rhombus or regular polygon etc.