CN201697875U - Aerosol sample tank for infrared analysis - Google Patents

Aerosol sample tank for infrared analysis Download PDF

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Publication number
CN201697875U
CN201697875U CN 201020240757 CN201020240757U CN201697875U CN 201697875 U CN201697875 U CN 201697875U CN 201020240757 CN201020240757 CN 201020240757 CN 201020240757 U CN201020240757 U CN 201020240757U CN 201697875 U CN201697875 U CN 201697875U
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CN
China
Prior art keywords
infrared
sample
top cover
sealing
cavity
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
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CN 201020240757
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Chinese (zh)
Inventor
王玄玉
诸雪征
安刚
冯宗伟
余世魁
白海涛
宋黎
孙逊
王金生
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Antichemical Command Engineering College P L A
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Antichemical Command Engineering College P L A
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Priority to CN 201020240757 priority Critical patent/CN201697875U/en
Application granted granted Critical
Publication of CN201697875U publication Critical patent/CN201697875U/en
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Abstract

The utility model relates to an aerosol sample tank for infrared analysis, which comprises a sample cavity, flat plates, a top cover, three through holes, three sealing plugs, a lead hole, a fan and two annular pressing plates. The top edge of the sampling cavity with a U-shaped groove structure is turned outwards; the flat plates with circular holes at the centers are arranged at two ends of the sample cavity; the top cover is connected with the top edge of the sample cavity, and a flexible sealing washer is arranged at the connecting position of the top cover with the top edge; the through holes are equidistantly processed along the longitudinal axis on the top cover, the heights of the sealing plugs in the shapes of circular tables are slightly larger than the thickness of the top cover, and the median diameters of the sealing plugs are equal to the diameters of the through holes; the lead hole is arranged on one of the sealing plugs; the fan is fixed at the center of the bottom of the top cover, a lead of the fan is led out from the lead hole of the sealing plug; and the annular pressing plate can be fixed at the positions corresponding to the circular holes at two ends of the sample tank and are used for fixing circular infrared glass or infrared film materials which are larger in diameters onto the outer sides of the positions of the circular holes at two ends of the sample tank. The aerosol sample tank has the advantages of large capacity, long optical distance, convenient sample adding, convenient cleaning and replacement of infrared window sheets, fine sealing performance and the like.

Description

Infrared analysis aerosol sample cell
[technical field]
The utility model relates to the aerosol sample cell that a kind of infrared analysis is used, and belongs to instrumental analysis and optical detective technology field.
[background technology]
Infrared analysis occupies critical role in modern analysis, detection technique, wherein infrared spectrometer is the most frequently used, most representative instrument.Infrared spectrometer mainly carries out infrared compressing tablet analysis, and the object of analysis mainly is a solid sample.Infrared spectrometer also can carry out the liquid film analysis, and thickness of liquid film is less than 1 millimeter, and sample size is very limited.Some infrared spectrometer has the function of analytical gas sample, but the majority of gas sample cell is the cost height not only, analyzable sample size is few, and can only analyze the pure gas sample, can't satisfy the needs of the aerosol sample infrared detection of being made up of pressed powder or superfine powder.Therefore, utilizing infrared spectrometer to analyze aerocolloidal infrared characteristic is a technical barrier that exists for a long time.
[utility model content]
The purpose of this utility model is to provide a kind of infrared analysis aerosol sample cell, to solve problems of the prior art.
The utility model is a kind of infrared analysis aerosol sample cell, that this sample cell has is reinforced, stir, sealing, multiple function and characteristics such as volume is big, infrared optical length such as saturating infrared, particularly electronic continuous stirring function can guarantee that aerosol dispersion is even, stable, as shown in Figure 1 and Figure 2.This sample cell has utilized the useful space of infrared spectrograph sample chamber to greatest extent, structurally easy, practical, need not secondary installing, fixing, but globality directly put into the sample chamber of infrared spectrometer and can analyze the infrared characteristic of aerosol sample, as shown in Figure 3.
A kind of infrared analysis aerosol sample cell specifically comprises:
One sample cavity is taked the U type groove structure, and top is turned up; The sample cavity two ends have the flat board of circular hole for central authorities;
One top cover is connected with the top of sample cavity, and the junction of the two is provided with the flexible sealing packing ring; Top cover upper edge longitudinal axis equidistantly is processed with three through holes;
Three sealing-plugs are truncated cone-shaped, highly are slightly larger than top cover thickness, and median diameter equals the diameter of through hole; One of them sealing-plug is provided with wire guide;
One fan is fixed in the bottom center position of top cover, and the lead of fan is drawn by the wire guide of sealing-plug;
Two annular pressing plates, can be fixed in the position of sample cavity two ends circular hole correspondence, be used for some circular infrared glass or infrared membraneous material of slightly larger in diameter is fixed on the outside of circular hole position, sample cell two ends, thereby play infrared and the double action sealed sample pond.
Wherein, described sealing-plug is rubber or vegetable cork.
Wherein, the endoporus of described annular pressing plate is processed into the inclined-plane, and its minimum diameter of bore is identical with the Circularhole diameter at sample cavity two ends; This inclined-plane can be for the circular infrared glass or the infrared membraneous material that fix different-diameter.
Wherein, the endoporus of described annular pressing plate is processed into the one-level stepped ramp type, and its minimum diameter of bore is identical with the Circularhole diameter at sample cavity two ends; This step can be for fixing circular infrared glass or infrared membraneous material.
The utlity model has that processing cost is low, useful volume is big, infrared optical length, easy for operation, need not advantages such as secondary installing, but globality is directly put into the sample chamber of infrared spectrometer and can be analyzed the infrared characteristic of aerosol sample, thereby efficiently solves the difficult problem of aerosol sample Infrared spectroscopy.
[description of drawings]
Fig. 1 is a stereographic map of the present utility model
Fig. 2 is installation of the present utility model and cut-away view
Fig. 3 is installed on whole structure figure behind the infrared spectrometer for the utility model
Figure 4 shows that one of structural representation of annular pressing plate
Figure 5 shows that annular pressing plate structural representation two
Number in the figure is described as follows:
1 top cover, 2 sample cavities
3 annular pressing plates, 4 sealing-plugs
5 wire guides, 6 fans
7 through holes, 8 circular holes
9 infrared spectrometers
[embodiment]
Below in conjunction with accompanying drawing, the technical solution of the utility model is described further.
As shown in Figure 1, 2, a kind of infrared analysis aerosol sample cell specifically comprises:
One sample cavity 2 is taked the U type groove structure, and top is turned up and is provided with some screws; The sample cavity two ends are provided with screw for the flat board that central authorities have circular hole 8 around the circular hole 8;
One top cover 1 can be processed by thicker organic glass, by being located at the threaded hole of periphery, is connected with the top of sample cavity 2, and the junction of the two is provided with the flexible sealing packing ring; Top cover upper edge longitudinal axis equidistantly is processed with three through holes 7; Intermediate throughholes is used to draw fan leads, and two side through hole are used to add sample;
Three sealing-plugs 4 are truncated cone-shaped, highly are slightly larger than top cover thickness, and median diameter equals the diameter of through hole; One of them sealing-plug is provided with wire guide 5; Sealing-plug can be made by rubber or vegetable cork;
One fan 6 is fixed in the bottom center position of top cover, and the lead of fan is drawn by the wire guide 5 of sealing-plug 4;
Two annular pressing plates 3 have the threaded hole of equal number on the circular hole 8 corresponding positions on this annular pressing plate and the sample cavity end face, can be fixed on the end face of sample cavity, as shown in Figure 1 and Figure 2 with screw.As shown in Figure 4, the endoporus of this annular pressing plate is processed as the inclined-plane, its minimum diameter of bore is identical with the Circularhole diameter of sample cavity end face, this inclined-plane can be for the circular infrared glass or the infrared membraneous material that fix different-diameter, so that circular infrared glass or infrared membraneous material are fixed on the outside of circular hole position, sample cell two ends, thereby play infrared and the double action sealed sample pond.
Wherein, as shown in Figure 5, the endoporus of described annular pressing plate 3 also can be processed into the one-level stepped ramp type, and its minimum diameter of bore is identical with the Circularhole diameter at sample cavity two ends; This step can be for fixing circular infrared glass or infrared membraneous material.
Concrete operating process is as follows: as shown in Figure 2, at first take off sample cell top cover 1, sample cavity 2 is cleaned up and dry.The infrared window of choosing is affixed on the circular hole 8 of sample cavity end face, annular pressing plate 3 is installed constitutes sealing, saturating infrared optical window.Afterwards the sample cell integral body of above-mentioned state is put into the infrared background spectrum of sample chamber test of infrared spectrometer 9.After testing background, the top cover that will have miniature electric fan 6 and packing washer is fixed on the sample cavity, connects fan leads and intermediate seal plug.Take off the sealing-plug of both sides, add the powder sample of specified amount, then with sealing-plug sealed sample pond once again.Fig. 1 is ready aerosol sample cell, and Fig. 3 is the whole structure figure that this sample cell and infrared spectrometer 9 are combined as a whole.At last, the circuit of connecting fan leads stirs, the infrared spectrum of collected specimens behind the stable gasoloid to be formed.Remove and disassemble sample cell after the off-test in reverse order and clean, change an operation such as infrared window.

Claims (4)

1. infrared analysis aerosol sample cell, it is characterized in that: this sample cell specifically comprises:
One sample cavity is taked the U type groove structure, and top is turned up; The sample cavity two ends have the flat board of circular hole for central authorities;
One top cover is connected with the top of sample cavity, and the junction of the two is provided with the flexible sealing packing ring; Top cover upper edge longitudinal axis equidistantly is processed with three through holes;
Three sealing-plugs are truncated cone-shaped, highly are slightly larger than top cover thickness, and median diameter equals the diameter of through hole; One of them sealing-plug is provided with wire guide;
One fan is fixed in the bottom center position of top cover, and the lead of fan is drawn by the wire guide of sealing-plug;
Two annular pressing plates are fixed in the position of sample cavity two ends circular hole correspondence, are used for circular infrared glass or infrared membraneous material are fixed on the outside of circular hole position, sample cell two ends.
2. infrared analysis aerosol sample cell according to claim 1 is characterized in that: described sealing-plug is rubber or vegetable cork.
3. infrared analysis aerosol sample cell according to claim 1 is characterized in that: the endoporus of described annular pressing plate is processed into the inclined-plane, and its minimum diameter of bore is identical with the Circularhole diameter at sample cavity two ends.
4. infrared analysis aerosol sample cell according to claim 1 is characterized in that: the endoporus of described annular pressing plate is processed into the one-level stepped ramp type, and its minimum diameter of bore is identical with the Circularhole diameter at sample cavity two ends.
CN 201020240757 2010-06-29 2010-06-29 Aerosol sample tank for infrared analysis Expired - Fee Related CN201697875U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN 201020240757 CN201697875U (en) 2010-06-29 2010-06-29 Aerosol sample tank for infrared analysis

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN 201020240757 CN201697875U (en) 2010-06-29 2010-06-29 Aerosol sample tank for infrared analysis

Publications (1)

Publication Number Publication Date
CN201697875U true CN201697875U (en) 2011-01-05

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101881730A (en) * 2010-06-29 2010-11-10 中国人民解放军防化指挥工程学院 Infrared analysis aerosol sample cell
CN104777099A (en) * 2014-01-14 2015-07-15 德尔格安全股份两合公司 Modified measuring cuvette

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101881730A (en) * 2010-06-29 2010-11-10 中国人民解放军防化指挥工程学院 Infrared analysis aerosol sample cell
CN104777099A (en) * 2014-01-14 2015-07-15 德尔格安全股份两合公司 Modified measuring cuvette
GB2523639A (en) * 2014-01-14 2015-09-02 Draeger Safety Ag & Co Kgaa Modified measuring cuvette
US9470621B2 (en) 2014-01-14 2016-10-18 Dräger Safety AG & Co. KGaA Modified measuring cuvette
GB2523639B (en) * 2014-01-14 2017-05-10 Draeger Safety Ag & Co Kgaa Modified measuring cuvette
CN104777099B (en) * 2014-01-14 2018-04-10 德尔格安全股份两合公司 Improved measurement colour comparator

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C14 Grant of patent or utility model
GR01 Patent grant
C17 Cessation of patent right
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20110105

Termination date: 20120629