CN201593993U - Trace gas flowmeter for testing permeability of low-permeability rock - Google Patents

Trace gas flowmeter for testing permeability of low-permeability rock Download PDF

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CN201593993U
CN201593993U CN2010200467497U CN201020046749U CN201593993U CN 201593993 U CN201593993 U CN 201593993U CN 2010200467497 U CN2010200467497 U CN 2010200467497U CN 201020046749 U CN201020046749 U CN 201020046749U CN 201593993 U CN201593993 U CN 201593993U
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林光荣
高春宁
刘学刚
刘秋兰
韩翼云
杜朝峰
高微
罗丽荣
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Petrochina Co Ltd
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Abstract

A trace gas flowmeter for testing the permeability of low-permeability rock is applied to testing the gas permeability of stratum rock. The device mainly comprises an intercepting pipe, a communicating pipe, an air inlet pipe and a U-shaped transparent pipe, wherein one end of the U-shaped transparent pipe is connected with the communicating pipe, and the U-shaped transparent pipe is communicated with the communicating pipe. The other end of the communicating pipe is fixed with a cut-off pipe. The middle part of the communicating pipe is connected with an air inlet pipe which is communicated with the communicating pipe. The effect is as follows: the instantaneous gas flow of the rock sample of the low-permeability reservoir can be tested. And the testing requirement of the rock sample of the low-permeability reservoir is met. By the trial of the micro gas flowmeter, the environmental, system and human errors are reduced, the measurement result is accurate, the repeatability is good, and the working efficiency is improved.

Description

测试低渗岩石渗透率的微量气体流量计 Trace Gas Flow Meter for Testing Low Permeability Rock Permeability

技术领域technical field

本实用新型涉及石油勘探开发技术,特别涉及在实验室内进行地层岩石气体渗透率测试的装置,是一种计量气体通过岩石瞬时流量的流量计量装置。The utility model relates to petroleum exploration and development technology, in particular to a device for testing the gas permeability of formation rocks in a laboratory, which is a flow metering device for measuring the instantaneous flow of gas passing through rocks.

背景技术Background technique

在测试岩石气体渗透率时,需要计量通过岩样的气体流量。微量气体流量计在低渗岩石样品的气体渗透率测试中尤为重要,微量气体流量计影响气体渗透率测试结果,对于低渗样品能否测量出气体渗透率起到了决定性作用。目前,皂膜流量计是国内外测试岩石气体渗透率使用的经典气体测量装置,能通过气体推动泡膜在不同管径的流速,换算成单位时间的流量。皂膜流量计的缺点是:(1)材料准备多,不同渗透率岩石样品需更换不同管径的流量管;(2)测试程序复杂;(3)样品测试劳动强度大。When testing rock gas permeability, it is necessary to measure the gas flow through the rock sample. Trace gas flowmeters are particularly important in the gas permeability test of low-permeability rock samples. Trace gas flowmeters affect the gas permeability test results and play a decisive role in measuring the gas permeability of low-permeability samples. At present, the soap film flowmeter is a classic gas measuring device used at home and abroad to test the gas permeability of rocks. It can push the flow rate of the bubble film in different pipe diameters through the gas and convert it into the flow rate per unit time. The disadvantages of the soap film flowmeter are: (1) There are many materials to prepare, and flow tubes with different diameters need to be replaced for rock samples with different permeability; (2) The test procedure is complicated; (3) The sample test is labor-intensive.

使用质量流量计同样能测试岩石气体渗透率。质量流量计测流量计自动化程度高,但仍有其不足:(1)外部环境影响测量结果,如在电压稳定的情况下才能获得准确的测量结果;(2)电子原件的稳定性对流量测量精度影响较大,尤其是在低流量测试中。(3)目前市场销售的质量流量计最小测量精度是10ml/min。测试低渗岩石样品对流量计的精度要求在1ml/min以下,质量流量计不能满足低渗岩石样品的测试要求。Rock gas permeability can also be tested using a mass flow meter. The mass flow meter has a high degree of automation, but it still has its shortcomings: (1) The external environment affects the measurement results, such as the accurate measurement results can only be obtained when the voltage is stable; (2) The stability of the electronic components has a great influence on the flow measurement. Accuracy has a big impact, especially in low flow tests. (3) The minimum measurement accuracy of mass flowmeters currently on the market is 10ml/min. When testing low-permeability rock samples, the accuracy of the flowmeter is required to be below 1ml/min, and the mass flowmeter cannot meet the test requirements for low-permeability rock samples.

实用新型内容Utility model content

本实用新型的目的是:提供一种测试低渗岩石渗透率的微量气体流量计,利用不同流量的气体进入微量气体流量计,会使U形透明管两端内液体产生一定的水位差,利用U形透明管两端水位差,换算得出气体瞬时流量。解决低渗储层岩石样品常规气体渗透率测试中存在的测量精度低、工作效率低的问题,满足低渗储层岩石样品测试需要,降低劳动强度,提高工作效率。The purpose of the utility model is to provide a trace gas flowmeter for testing the permeability of low-permeable rocks. When gases with different flow rates enter the trace gas flowmeter, a certain water level difference will be generated in the liquid at both ends of the U-shaped transparent tube. The water level difference at both ends of the U-shaped transparent tube is converted to obtain the instantaneous flow rate of the gas. Solve the problems of low measurement accuracy and low work efficiency in the conventional gas permeability test of low-permeability reservoir rock samples, meet the needs of low-permeability reservoir rock sample testing, reduce labor intensity, and improve work efficiency.

本实用新型采用的技术方案是:测试低渗岩石渗透率的微量气体流量计,主要由截流管、联通管、进气管和U形透明管组成,其特征在于:在U形透明管的一端连接有联通管,U形透明管与联通管联通。在联通管的另一端内固定有截流管。在联通管的中部连接有进气管,进气管与联通管联通。当测试过程中的微量气体通过进气管进入联通管,气体通过截流管时受到一定阻力,会使联通管内产生一定的压力,并使U形透明管两端的液面发生变化。而根据一定压力值对应一定流量的原理,不同的压力对应不同的流量,观察U形透明管两端液面变化情况。微量气体流量计通过标定后,能测定不同的压力下岩石样品气体渗透率、流量、水位读数的函数关系式,求得不同水位读数对应不同流量。The technical solution adopted by the utility model is: a trace gas flowmeter for testing low-permeability rock permeability, which is mainly composed of a shut-off pipe, a communication pipe, an air intake pipe and a U-shaped transparent pipe, and is characterized in that: one end of the U-shaped transparent pipe is connected to There is a Unicom pipe, and the U-shaped transparent pipe is connected with the Unicom pipe. A shut-off tube is fixed in the other end of the communication tube. An air intake pipe is connected to the middle part of the communication pipe, and the air intake pipe communicates with the communication pipe. When the trace gas in the test process enters the connecting pipe through the intake pipe, the gas is subjected to certain resistance when passing through the intercepting pipe, which will generate a certain pressure in the connecting pipe and cause the liquid level at both ends of the U-shaped transparent pipe to change. According to the principle that a certain pressure value corresponds to a certain flow rate, and different pressures correspond to different flow rates, observe the change of the liquid level at both ends of the U-shaped transparent tube. After the micro gas flowmeter is calibrated, it can measure the functional relational expression of gas permeability, flow rate and water level reading of rock samples under different pressures, and obtain different flow rates corresponding to different water level readings.

U形透明管的直径在4~8毫米之间;U形透明管的高度在750~950毫米之间。U形透明管两端有刻度。The diameter of the U-shaped transparent tube is between 4 and 8 millimeters; the height of the U-shaped transparent tube is between 750 and 950 millimeters. There are scales at both ends of the U-shaped transparent tube.

通过改变截流管的直径,来控制微量气体流量大小。截流管的内径在0.02~0.1毫米之间。By changing the diameter of the cut-off tube, the flow of trace gas can be controlled. The inner diameter of the shut-off tube is between 0.02 and 0.1 mm.

本实用新型的有益效果:本实用新型测试低渗岩石渗透率的微量气体流量计,能测试低渗储层岩石样品气体瞬时流量。满足低渗储层岩石样品测试需要。通过微量气体流量计的试用,降低了环境、系统和人为误差,测量结果准确,重复性好,降低了测试劳动强度,提高工作效率。Beneficial effects of the utility model: the utility model is a trace gas flowmeter for testing the permeability of low-permeability rocks, which can test the gas instantaneous flow rate of low-permeability reservoir rock samples. Meet the testing needs of low-permeability reservoir rock samples. Through the trial of the micro gas flowmeter, the environment, system and human errors are reduced, the measurement results are accurate, the repeatability is good, the labor intensity of the test is reduced, and the work efficiency is improved.

附图说明Description of drawings

图1是本实用新型测试低渗岩石渗透率的微量气体流量计结构剖面示意图。Figure 1 is a schematic cross-sectional view of the structure of a trace gas flowmeter for testing the permeability of low-permeability rocks according to the present invention.

图中,1.截流管,2.联通管,3.进气管,4.U形透明管。In the figure, 1. shut-off pipe, 2. Unicom pipe, 3. intake pipe, 4. U-shaped transparent pipe.

具体实施方式Detailed ways

实施例1:以一个测试低渗岩石渗透率的微量气体流量计为例,对本实用新型作进一步详细说明。Embodiment 1: Taking a trace gas flowmeter for testing low-permeability rock permeability as an example, the utility model is further described in detail.

参阅图1。本实用新型测试低渗岩石渗透率的微量气体流量计,主要由截流管1、联通管2、进气管3和U形透明管4组成,其特征在于:在U形透明管4的一端连接有联通管2,U形透明管4与联通管2联通。在联通管2的另一端内固定有一个截流管1。截流管1的直径为0.05毫米。在联通管2的中部连接有进气管3,进气管3与联通管2联通。See Figure 1. The utility model is a trace gas flowmeter for testing the permeability of low-permeable rocks. Unicom pipe 2, U-shaped transparent pipe 4 and Unicom pipe 2 Unicom. A cut-off pipe 1 is fixed in the other end of the communication pipe 2 . The diameter of the shut-off tube 1 is 0.05 mm. An air intake pipe 3 is connected to the middle part of the communication pipe 2, and the air intake pipe 3 communicates with the communication pipe 2.

U形透明管4的直径为5毫米;U形透明管4的高度为800毫米,U形透明管4两端分别有800mm液柱高度的刻度。The diameter of the U-shaped transparent tube 4 is 5 mm; the height of the U-shaped transparent tube 4 is 800 mm, and the two ends of the U-shaped transparent tube 4 have a scale of 800 mm liquid column height respectively.

微量气体流量计在低渗渗样品气体渗透率测试中尤为重要,它不仅影响气体渗透率结果的精度,而且对于低渗和特低渗的样品能否测量出来起到了决定性因素,从下面公式可以看出,除了气体流量,其余影响气体渗透率的参数都可以用法定计量器具测得。微量气体流量计的研制,弥补了皂膜流量计、质量流量计不能适应最小流量的缺陷。测试低渗岩石渗透率的微量气体流量计最小流量可达到0.00375ml/s。Trace gas flowmeter is particularly important in the gas permeability test of low-permeability samples. It not only affects the accuracy of gas permeability results, but also plays a decisive factor in whether low-permeability and ultra-low-permeability samples can be measured. From the following formula, we can It can be seen that, except for the gas flow rate, other parameters affecting the gas permeability can be measured with legal measuring instruments. The development of micro gas flowmeter makes up for the defect that soap film flowmeter and mass flowmeter cannot adapt to the minimum flow rate. The minimum flow rate of the trace gas flowmeter for testing the permeability of low-permeability rocks can reach 0.00375ml/s.

Ka=(2×Qo×Pa×μ×L)/A×(P1 2-P2 2)K a = (2×Q o ×P a ×μ×L)/A×(P 1 2 -P 2 2 )

Ka-空气渗透率,mD; Ka - air permeability, mD;

Qo-气体流量,ml/sQ o - gas flow rate, ml/s

Pa-大气压力,MPa;P a - atmospheric pressure, MPa;

μ-气体粘度,mPa.s;μ-gas viscosity, mPa.s;

L-样品长度,cm;L-sample length, cm;

A-样品端面积,cm2A-sample end area, cm 2 ;

P1、P2---分别为入口和出口的绝对压力(修约到两位小数),MPa;P 1 , P 2 --- Absolute pressure at the inlet and outlet respectively (rounded to two decimal places), MPa;

将实验获得的气体接入测试低渗岩石渗透率的微量气体流量计的进气管3入口处;气体进入流量计,气体从截流管1中心孔流出。由于截流管1的作用,气体通过的同时会产生一定的压力,这样在U形透明管4上产生一定的水位差,通过标准仪器的标定,一定的水位差对应一定的流量。当压力稳定时,通过样品的气体流量也是稳定的,这样就能测出气体通过样品的流量。The gas obtained in the experiment is connected to the inlet of the inlet pipe 3 of the micro gas flowmeter for testing the permeability of the low-permeability rock; Due to the effect of the shut-off tube 1, a certain pressure will be generated when the gas passes through, so that a certain water level difference will be generated on the U-shaped transparent tube 4. Through the calibration of the standard instrument, a certain water level difference corresponds to a certain flow rate. When the pressure is stable, the flow of gas through the sample is also stable, so that the flow of gas through the sample can be measured.

各种流量计的单位压力下的流量比较Comparison of flow rate per unit pressure of various flowmeters

Figure G2010200467497D00041
Figure G2010200467497D00041

从上表看所研制的微量气体流量计与皂膜流量计相比,精度高、操作简单,不受计时带来的误差影响;与气体质量流量计相比,测试低渗岩石渗透率的微量气体流量计的稳定性好,波动小。It can be seen from the above table that compared with the soap film flowmeter, the micro gas flowmeter developed has high precision, simple operation, and is not affected by the error caused by timing; The gas flowmeter has good stability and small fluctuations.

Claims (3)

1.一种测试低渗岩石渗透率的微量气体流量计,主要由截流管(1)、联通管(2)、进气管(3)和U形透明管(4)组成;其特征在于:在U形透明管(4)的一端连接有联通管(2),U形透明管(4)与联通管(2)联通,在联通管(2)的另一端内固定有截流管(1),在联通管(2)的中部连接有进气管(3),进气管(3)与联通管(2)联通。1. A trace gas flowmeter for testing the permeability of low-permeable rocks, mainly composed of shut-off pipe (1), communication pipe (2), air inlet pipe (3) and U-shaped transparent pipe (4); it is characterized in that: One end of the U-shaped transparent tube (4) is connected with a Unicom tube (2), the U-shaped transparent tube (4) communicates with the Unicom tube (2), and a shut-off tube (1) is fixed in the other end of the Unicom tube (2), An air intake pipe (3) is connected to the middle part of the communication pipe (2), and the air intake pipe (3) communicates with the communication pipe (2). 2.根据权利要求1所述的测试低渗岩石渗透率的微量气体流量计,其特征是:U形透明管(4)的直径在4~8毫米之间;U形透明管(4)的高度在750~950毫米之间,U形透明管(4)两端分别有刻度。2. The micro gas flowmeter for testing low-permeability rock permeability according to claim 1, characterized in that: the diameter of the U-shaped transparent tube (4) is between 4 and 8 millimeters; the diameter of the U-shaped transparent tube (4) The height is between 750-950 millimeters, and the two ends of the U-shaped transparent tube (4) have scales respectively. 3.根据权利要求1所述的测试低渗岩石渗透率的微量气体流量计,其特征是:截流管(1)的内径在0.02~0.1毫米之间。3. The micro-gas flowmeter for testing the permeability of low-permeability rocks according to claim 1, characterized in that: the inner diameter of the shut-off tube (1) is between 0.02-0.1 mm.
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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103575631A (en) * 2013-11-06 2014-02-12 河海大学 Rock permeability testing system and testing method
CN104020096A (en) * 2014-06-20 2014-09-03 青岛理工大学 Device and method for detecting pore pressure by U-shaped pipe hydraulic differential rope method
CN104215282A (en) * 2013-05-30 2014-12-17 中国石油化工股份有限公司 Gas flow measuring device and method for measuring gas flow using same
CN104359819A (en) * 2014-11-10 2015-02-18 中国石油天然气股份有限公司 Low-permeability tight core gas-water relative permeability measurement device and measurement method
CN106596374A (en) * 2016-12-19 2017-04-26 徐州医科大学 Gas permeability detecting device and determination method for tissue engineering porous scaffold

Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104215282A (en) * 2013-05-30 2014-12-17 中国石油化工股份有限公司 Gas flow measuring device and method for measuring gas flow using same
CN104215282B (en) * 2013-05-30 2017-10-27 中国石油化工股份有限公司 Equipment for measuring gas flow rate and the method that measuring gas flow rate is carried out using the device
CN103575631A (en) * 2013-11-06 2014-02-12 河海大学 Rock permeability testing system and testing method
CN103575631B (en) * 2013-11-06 2015-10-07 河海大学 Rock permeability test macro and method of testing
CN104020096A (en) * 2014-06-20 2014-09-03 青岛理工大学 Device and method for detecting pore pressure by U-shaped pipe hydraulic differential rope method
CN104020096B (en) * 2014-06-20 2016-04-27 青岛理工大学 Device and method for detecting pore pressure by U-shaped pipe hydraulic differential rope method
CN104359819A (en) * 2014-11-10 2015-02-18 中国石油天然气股份有限公司 Low-permeability tight core gas-water relative permeability measurement device and measurement method
CN106596374A (en) * 2016-12-19 2017-04-26 徐州医科大学 Gas permeability detecting device and determination method for tissue engineering porous scaffold
CN106596374B (en) * 2016-12-19 2019-01-18 徐州医科大学 A kind of device for checking air permeability and measuring method of tissue engineered porous scaffold

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