CN201495384U - Device of continuously producing nanometer fiber films - Google Patents

Device of continuously producing nanometer fiber films Download PDF

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Publication number
CN201495384U
CN201495384U CN2009201706007U CN200920170600U CN201495384U CN 201495384 U CN201495384 U CN 201495384U CN 2009201706007 U CN2009201706007 U CN 2009201706007U CN 200920170600 U CN200920170600 U CN 200920170600U CN 201495384 U CN201495384 U CN 201495384U
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CN
China
Prior art keywords
roller
nano fibrous
fibrous membrane
roll
continuous production
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
CN2009201706007U
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Chinese (zh)
Inventor
张晓涛
刘阿兴
刘昌炎
张禄荪
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
CHANGZHOU JIULIAN BATTERY MATERIAL Co Ltd
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CHANGZHOU JIULIAN BATTERY MATERIAL Co Ltd
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Priority to CN2009201706007U priority Critical patent/CN201495384U/en
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Publication of CN201495384U publication Critical patent/CN201495384U/en
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  • Nonwoven Fabrics (AREA)

Abstract

The utility model relates to a device of continuously producing nanometer fiber films. By adopting the device, macromolecular solution can be continuously manufactured into nanometer fiber films by using an electrostatic spinning method. The device comprises a direct current high-pressure power supply, a supply system, a spray cap set, a wire receiving system and a wrap-up system, wherein the wire receiving system is a cylinder with diameter of 400 to 600 mm and length of 800 to 1500 mm and is connected with a speed adjustment motor, the wrap-up system is composed of two portions, one portion is a film-tearing and guide roller 2 close to a wire receiving roller 1 and is the cylinder with diameter of 100 to 200 mm, the surface of the one portion is covered by a layer of rubber, the length is matched with the roller 1, and the distance between 2 and 1 is adjusted by a pneumatic element installed on 2. The other portion is a wrap-up roller 3, and the distance between 3 and 2 is adjusted by the pneumatic element installed on 3. The roller 2 is adjoining to the roller 1, and the speed of 2 and 1 lines is the same but the direction is oppositely rotated because of friction between two rollers. The roller 3 is adjoining to 2, and the speed of 3 and 2 lines is the same but the direction is oppositely rotated due to friction between two rollers.

Description

A kind of device of continuous production nano fibrous membrane
Technical field
The utility model relates to a kind of device of continuous production nano fibrous membrane, adopts this device Polymer Solution can be made nano fibrous membrane continuously with method of electrostatic spinning.
Technical background
Number of patent application be 200480056915 and WO2005073441 in, a kind of continuous electrostatic spinning film forming apparatus has successfully been described.But lack description in these schemes to wrap-up.The utility model provides a kind of device that has the continuous production nano fibrous membrane of film take-up in order to overcome above-mentioned shortcoming.
The content of invention
The objective of the invention is provides a kind of electrostatic spinning film forming apparatus by the utility model, a kind ofly can produce the nano fibrous membrane industrialized unit continuously.This device comprises DC high-voltage power supply, liquid-supplying system, jet head sets, meets a system, the rolling system.DC high-voltage power supply is that a voltage adjustable range is the high pressure generator of 0-35000 volt; Liquid-supplying system is made up of the sebific duct of peristaltic pump and organic solvent-resistant; Jet head sets 4 is made up of some syringe needles; To meet a system and be a diameter be that 400-600mm is long is the cylinder of 800-1500mm, is referred to as to connect roll dies 1 and links to each other with a buncher; The rolling system is made up of two parts: the first is taken off the film guide roller 2 of holding concurrently near what connect roll dies 1, and roller 2 is diameters for the 100-200mm surface is surrounded by the cylinder of one deck rubber, length with connect the roll dies coupling, 2 and 1 distance can be by the pneumatic element adjusting that is contained on 2; Another part is that the distance of wind-up roll 3,3 and 2 is regulated by the pneumatic element that is contained on 3.
Description of drawings
The cross-sectional view that has schematically shown apparatus of the present invention in the accompanying drawing.Figure acceptance of the bid 1 is for connecing roll dies; 2 are wind-up roll for taking off hold concurrently guide roller 3 of film; 4 is jet head sets.
The specific embodiment
The continuous production nano fibrous membrane industrialized unit that adopts the utility model to provide prepares nano fibrous membrane with suitable Polymer Solution.Its process is also to claim electrospinning liquid to be sent to jet head sets 4 Polymer Solution with solution feed pump, is flowed out by shower nozzle again.When shower nozzle and connect between the roll dies 1 when forming high electric field, electrospinning liquid forms Taylor's cone on the shower nozzle top.Because effect of electric field, liquid flow split becomes some threads, flows to connect roll dies.The solvent evaporates macromolecular solid changes into fiber simultaneously, is connecing film forming on the roll dies.Control connects the roll dies rotating speed, makes the film of acceptance reach the thickness that needs.Film is peeled off from connecing roll dies, walked around guide roller 2 and reach wind-up roll 3.Simultaneously with roller 2 near connecing roll dies 1 because the friction between two rollers, make 2 identical with 1 linear velocity and direction is rotated on the contrary.Simultaneously also with roller 3 near 2 because the friction between two rollers, make 3 identical with 2 linear velocities and direction is rotated on the contrary, with the film rolling.Roller 2 is constantly peeled off film from roller 1, send roller 3 to, forms continuously to produce.When the film of rolling reaches some, regulate pneumatic element roller 3 and roller 2 are left, change new wind-up roll, continue rolling near roller 2 again.
Example
Kynoar (PVDF) with the 3F company trade mark 904 is the electrospinning material, is solvent with dimethyl formamide (DMF), and acetone is conditioning agent.With DMF and acetone is mixed solvent, and preparation PVDF content is the electrospinning liquid of 8-10%.The film forming apparatus that adopts the utility model to provide is prepared nano fibrous membrane.Electrospinning liquid is delivered to jet head sets 4 with pump, flows out, under electric field action, carry out electrostatic spinning system film through shower nozzle.The high-pressure side of DC high-voltage power supply links to each other with jet head sets 4, and other end ground connection connects roll dies 1 simultaneously and also links to each other with the ground end.Regulate high pressure output at 20000~35000 volts, shower nozzle is about 180mm with connecing the roll dies spacing, and the electrospinning temperature is controlled at 30~40 ℃.Obtain the fiber of diameter, form non-weaving cloth connecing on the roll dies 1, be called nano fibrous membrane at 40~1000nm.Regulate the rotating speed of wind-up roll, can obtain the nano fibrous membrane of 10~100 μ m different-thickness.Film is peeled off from connecing roll dies, walked around guide roller 2 and reach wind-up roll 3.Film is constantly peeled off from connecing on the roll dies, and rolling is on wind-up roll continuously.
Industrial applicibility
The device of the continuous production nano fibrous membrane that the utility model provides is suitable for producing continuously various types of nano fibrous membranes. Can produce continuously thickness from 10-100 μ m, especially produce the following film of 20 μ m, this device overcome general device peel off with rolling on difficulty. Nano fibrous membrane can be used for lithium battery diaphragm, fuel cell barrier film, membrane for water treatment, protective articles etc.

Claims (7)

1. the utility model relates to a kind of device of continuous production nano fibrous membrane, comprise roll dies and the rolling system of connecing, it is characterized in that the rolling system, be made up of two parts: the first is taken off the film guide roller (2) of holding concurrently near what connect roll dies (1), and another part is wind-up roll (3).
2. the device of continuous production nano fibrous membrane according to claim 1, it is characterized in that taking off the film guide roller (2) of holding concurrently is a diameter for the 100-200mm surface is surrounded by the cylinder of one deck rubber, length with connect roll dies 1 coupling.
3. the device of continuous production nano fibrous membrane according to claim 1 is characterized in that taking off film and holds concurrently and pneumatic element is housed on the guide roller (2), regulates and connect the distance of roll dies (1).
4. the device of continuous production nano fibrous membrane according to claim 1 is characterized in that on the wind-up roll (3) pneumatic element being housed, and regulates the distance with roller (2).
5. the device of continuous production nano fibrous membrane according to claim 1, it is characterized in that connecing roll dies is that a diameter is that 400-600mm length is the cylinder of 800-1500mm, and links to each other with a buncher.
6. the device of continuous production nano fibrous membrane according to claim 1 is characterized in that taking off film and holds concurrently guide roller (2) near connecing roll dies (1), because the friction between two rollers, makes (2) and (1) linear velocity is identical and direction is rotated on the contrary.
7. the device of continuous production nano fibrous membrane according to claim 1 is characterized in that wind-up roll (3) near (2), because the friction between two rollers, makes (3) and (2) linear velocity is identical and direction is rotated on the contrary.
CN2009201706007U 2009-08-10 2009-08-10 Device of continuously producing nanometer fiber films Expired - Lifetime CN201495384U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN2009201706007U CN201495384U (en) 2009-08-10 2009-08-10 Device of continuously producing nanometer fiber films

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN2009201706007U CN201495384U (en) 2009-08-10 2009-08-10 Device of continuously producing nanometer fiber films

Publications (1)

Publication Number Publication Date
CN201495384U true CN201495384U (en) 2010-06-02

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN2009201706007U Expired - Lifetime CN201495384U (en) 2009-08-10 2009-08-10 Device of continuously producing nanometer fiber films

Country Status (1)

Country Link
CN (1) CN201495384U (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103582964A (en) * 2012-05-30 2014-02-12 松下电器产业株式会社 Cell, cell separator, and method for production of cell separator

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103582964A (en) * 2012-05-30 2014-02-12 松下电器产业株式会社 Cell, cell separator, and method for production of cell separator
CN103582964B (en) * 2012-05-30 2017-03-22 松下知识产权经营株式会社 Cell, cell separator, and method for production of cell separator

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Granted publication date: 20100602

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