CN201445957U - Combination stirring vessel - Google Patents

Combination stirring vessel Download PDF

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Publication number
CN201445957U
CN201445957U CN2009200474303U CN200920047430U CN201445957U CN 201445957 U CN201445957 U CN 201445957U CN 2009200474303 U CN2009200474303 U CN 2009200474303U CN 200920047430 U CN200920047430 U CN 200920047430U CN 201445957 U CN201445957 U CN 201445957U
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China
Prior art keywords
stirred tank
agitator
blade
baffle plate
ratio
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Expired - Fee Related
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CN2009200474303U
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Chinese (zh)
Inventor
杨国强
陈义刚
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MERYA'S LECITHIN Co Ltd
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MERYA'S LECITHIN Co Ltd
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Abstract

The utility model discloses a combination type stirring vessel, comprising a stirrer and a reactor vessel of a baffle, wherein two layers of stirrers are longitudinally arranged along the stirring axle of the stirrer and the upper layer is a paddle agitator and the lower layer is a disc turbine type agitator. The combination stirring vessel combines the paddle agitator with the disc turbine type agitator to solve the problem that the single agitator does not quickly make the fluid achieve turbulent condition and the paddle agitator makes the upper fluid horizontally surge up and stir up, thus the high-viscosity fluid quickly reaches turbulent condition and the disc turbine type agitator can generate strong shear force for the fluid action, thus the dispersion effect of the material can be optimal. The combination stirring vessel is especially suitable for the technology for extracting yolk lecithin from yolk powder using the solvent method, thus the powdery yolk lecithin is produced at high production efficiency and large production yield and the combination type stirring vessel is also suitable for other solvent extraction technology of the other substance.

Description

A kind of combined type stirred tank
Technical field
The utility model belongs to technical field of chemical engineering, is specifically related to a kind of stirred tank.
Background technology
Mechanical stirring kettle is to implement mixing of materials to promote one of important form of heat transfer, mass transfer.The mechanism of mechanical stirring kettle comprises agitator structure and baffle arrangement.In order to improve the performance that mixes,, need optimize targetedly the structure of baffle plate and agitator to different technology to material.
Phosphatide is the main composition composition of animal cell membrane system, therefore be to form one of most important basic substance of life, proportion is higher than other system in nerve and internal organ system, and for example: the ratio of phosphatide is high in the seed of brain, liver, yolk, plant etc.Because phosphatide is a kind of bioactivator, it has unique physical and chemical properties and nutritive value, so phosphatide food, health products, medicine and feedstuff industry worldwide is more and more to be extensive use of.People's edible phospholipid can play and reduce higher blood fat, improves fatty liver symptom, brain tonic and intelligence development and physiological function such as delay senility.
Phosphatide is the general name of the phosphorous lipoid of a class, is made up of mixing such as lecithin (phosphatid ylcholine), cephalin (phosphatidyl-ethanolamine), lipositol (phosphatidylinositols), serinephosphatide (phosphatidylserine), sphingomyelins.Wherein, lecithin (phosphatid ylcholine) is that wherein tool is bioactive a kind of.Lecithin can extract from soybean lecithin and yolk and yolk powder, be called soybean lecithin and egg yolk lecithin, comprehensive and deep processing along with egg product, yolk powder has become the broad range of food raw material, contains 50% the neutral fat of having an appointment, 10% phosphatide and about 40% livetin in the yolk powder of food grade.With the yolk powder is that raw material extracts egg yolk lecithin, and conventional method is exactly a solvent method, and yolk powder and the dispersity of egg yolk lecithin wherein in solvent have directly influenced de-oiling effect, extraction yield and product appearance.Therefore press for the stirred autoclave of a kind of low energy consumption, high-effect, high pass mass-energy power.
Summary of the invention
A technical problem to be solved in the utility model is that the structure to baffle plate and agitator is optimized, provide a kind of solvent method that is applicable to from yolk powder, to extract the combined type stirred tank of egg yolk lecithin, this stirred tank has low power consuming, high-effect, high pass mass-energy power, can guarantee that material has higher dispersive property in the middle of solvent
For solving the problems of the technologies described above, technical scheme to be solved in the utility model is as follows:
A kind of combined type stirred tank comprises the reactor that is equipped with agitator and baffle plate, and the shaft of described agitator is vertically arranged with two-layer agitator, and wherein, the upper strata is a dasher, and lower floor is a disc turbine formula agitator.
Wherein, the blade of described dasher is a hinging type.
Wherein, the blade of described disc turbine formula agitator is an arrow leaf formula.
Wherein, described baffle number is 4, radially is provided with along reactor, is evenly distributed on the reactor inwall, is in the stirring region substantially.
The optimal technical scheme of combinations thereof formula stirred tank is: stirred tank is the stainless steel stirred tank of 500~5000 liters of volumes, and the stirred tank ratio of height to diameter is 1: 1.2~0.8, and the ratio of stirred tank internal diameter and stirrer diameter is 2~6: 1; The space internal diameter that baffle plate surrounds in reactor is 0.8~0.9: 1 with reactor internal diameter ratio, single height of baffle plate is 0.6~1: 1 with the ratio of kettle height, the thickness of single baffle plate is 2~5mm, and the spacing between described baffle plate and the inner wall of kettle is 0~0.008 with reactor internal diameter ratio: 1. the diameter of shaft is 40~80mm; The wheel hub of dasher is provided with 2 blades, blade vertical with shaft and with the angle of horizontal plane be 30 °~90 °, vane thickness is 1~5mm, width of blade is 60~120mm; The wheel hub of disc turbine formula agitator is provided with 6 groups of blades, and every group is that 30 °~90 ° blade is formed (being arrow leaf formula) by 2 angles, and vane thickness is 1~5mm, and width of blade is 60~120mm.
A more preferred scheme of combinations thereof formula stirred tank is: stirred tank is the stainless steel stirred tank of 1500~2500 liters of volumes, and the stirred tank ratio of height to diameter is 1: 1, and the ratio of stirred tank internal diameter and stirrer diameter is 3~5: 1; The space internal diameter that baffle plate surrounds in reactor is 0.85~0.86: 1 with reactor internal diameter ratio, single height of baffle plate is 0.8~0.9: 1 with the ratio of kettle height, the thickness of single baffle plate is 3~4mm, and the spacing between described baffle plate and the inner wall of kettle is 0~0.005: 1 with reactor internal diameter ratio; The diameter of shaft is 50~70mm; The wheel hub of dasher is provided with 2 blades, blade vertical with shaft and with the angle of horizontal plane be 45 °~60 °, vane thickness is 3~4mm, width of blade is 80~100mm; The wheel hub of disc turbine formula agitator is provided with 6 groups of blades, and every group is that 45 °~60 ° blade is formed by 2 angles, and vane thickness is 3~4mm, and width of blade is 80~100mm.
Alleged in this specification " internal diameter ", " directly " etc. are all diameter.
When using single disc turbine formula agitator, stirring system is to the stirring of high viscosity fluid the time, because the incipient viscosity ratio of fluid is bigger, after agitator often occurring and starting a period of time, just near the direction that stirs along with agitator of the fluid the agitator is done circumference and is flowed, what stirred tank was interior is in relative static conditions from agitator fluid far away, particularly liquid level; When using single paddle agitator, though can adopt hinged joint slurry formula impeller, axial flow that also can convection cell has a kind of effect, because this agitator speed is generally not high, and makes the convection circulation of fluid relatively poor.
For the suspension operation of solid matter at liquid material; the purpose of agitator is to make being evenly distributed of solid; thereby chemical processes such as dissolving are finished in the requirement by technology; under the turning effort of agitator; make solid particle obtain certain movement velocity; be suspended in the liquid phase to overcome its extreme sinking speed; the principal element of decision solid particle suspension degree in liquid material is the turbulent extent of liquid; it is flow rate of fluid; for the liquid in the still; same when using single disc turbine formula agitator; what only have that circumference flows is to be difficult to accomplish higher stirring rank; also be difficult to obtain bigger shearing force, thereby be difficult to obtain higher efficient and yield.After adopting combined type agitator of the present invention, owing to given full play to the advantage of paddle agitator and disc turbine formula agitator, reach the fluid that makes away from agitator and seethed stirring up and down, make high stickiness fluid reach turbulence state very soon, and the very strong shearing force of convection cell effect, make the material dispersed effect reach best, manifest characteristics aspect higher saving energy consumption, easy operation, efficient.
Beneficial effect: combined type stirred tank of the present utility model is used in combination dasher and disc turbine formula agitator, can not make fluid reach the problem of turbulence state very soon to solve single agitator, paddle agitator can make the fluid on top seethe stirring up and down, make the high viscosity fluid reach turbulence state very soon, disc turbine formula agitator can produce the very strong shearing force of convection cell effect, makes the material dispersed effect reach best.Combined type stirred tank of the present utility model is specially adapted to utilize solvent method to extract the technology of egg yolk lecithin from yolk powder, the production efficiency height, the production yield is big, can produce the egg yolk lecithin (technology in the past can only be produced the egg yolk lecithin of paste) of powdery, combined type stirred tank of the present invention also is applicable to the solvent extraction technology of other materials simultaneously.
Description of drawings
Fig. 1 is a combination stirring-type reactor schematic diagram of the present utility model.
Fig. 2 is the baffle plate vertical view.
Fig. 3 is the front view of disc turbine formula agitator in the utility model.
Fig. 4 is the vertical view of disc turbine formula agitator in the utility model.
Fig. 5 is that the A of the blade-section of disc turbine formula agitator in the utility model is to view.
The specific embodiment:
According to following embodiment, can understand the utility model better.
Embodiment 1:
As shown in Figure 1, the combined type stirred tank is the stainless steel stirred tank of 2000 liters of volumes, comprise the reactor 1 that is equipped with agitator and baffle plate 2, agitator is rotatable under the effect of variable-frequency motor 3, the shaft of described agitator is vertically arranged with two-layer agitator, wherein, the upper strata is a dasher 4, and lower floor is a disc turbine formula agitator 5.
The stirred tank ratio of height to diameter is 1: 1, and the ratio of stirred tank internal diameter and stirrer diameter is 3.5.The diameter of shaft is 65mm.The blade of dasher 4 is a hinging type, is arranged with 2 blades on the wheel hub, blade vertical with shaft and with the angle of horizontal plane be 45 °, vane thickness is 4mm, width of blade is 100mm; The blade of disc turbine formula agitator 5 is an arrow leaf formula, wheel hub is provided with 6 groups of blades (Fig. 3~4), every group is that 60 ° blade is formed (Fig. 5) by 2 angles, vane thickness is 4mm, width of blade is 100mm, the blade direction of rotation is opposite with the leaf angle bearing of trend, is to flow to the arrow tail by arrow to guarantee flow direction.Because blade is slightly curved, its section is parabolic, thereby two strands of oblique circular flows are up and down axially arranged, and is low in energy consumption, and has higher shearing force.
Baffle number is 4, radially is provided with along reactor, and evenly vertical distribution is in the stirring region substantially at the reactor inwall, and promptly baffle plate is divided reactor equally and is the quartering, as shown in Figure 2.The space internal diameter that baffle plate surrounds in reactor is 0.85: 1 with reactor internal diameter ratio, single height of baffle plate is 0.85: 1 with the ratio of kettle height, the thickness of single baffle plate is 4mm, and the spacing between described baffle plate and the inner wall of kettle is 0.003: 1 with reactor internal diameter ratio.

Claims (7)

1. a combined type stirred tank comprises the reactor that is equipped with agitator and baffle plate, it is characterized in that the shaft of described agitator is vertically arranged with two-layer agitator, and wherein, the upper strata is a dasher, and lower floor is a disc turbine formula agitator.
2. combined type stirred tank according to claim 1, the blade that it is characterized in that described dasher is a hinging type.
3. combined type stirred tank according to claim 1, the blade that it is characterized in that described disc turbine formula agitator are arrow leaf formula.
4. combined type stirred tank according to claim 1 is characterized in that described baffle number is 4, radially is provided with along reactor, is evenly distributed on the reactor inwall, is in the stirring region substantially.
5. according to any described combined type stirred tank in the claim 1~4, it is characterized in that, stirred tank is the stainless steel stirred tank of 500~5000 liters of volumes, and the stirred tank ratio of height to diameter is 1: 1.2~0.8, and the ratio of stirred tank internal diameter and stirrer diameter is 2~6: 1; The space internal diameter that baffle plate surrounds in reactor is 0.8~0.9: 1 with reactor internal diameter ratio, single height of baffle plate is 0.6~1: 1 with the ratio of kettle height, the thickness of single baffle plate is 2~5mm, and the spacing between described baffle plate and the inner wall of kettle is 0~0.008: 1 with reactor internal diameter ratio.
6. combined type stirred tank according to claim 5, the diameter that it is characterized in that shaft is 40~80mm; The wheel hub of dasher is provided with 2 blades, blade vertical with shaft and with the angle of horizontal plane be 30 °~90 °, vane thickness is 1~5mm, width of blade is 60~120mm; The wheel hub of disc turbine formula agitator is provided with 6 groups of blades, and every group is that 30 °~90 ° blade is formed by 2 angles, and vane thickness is 1~5mm, and width of blade is 60~120mm.
7. combined type stirred tank according to claim 6 is characterized in that stirred tank is the stainless steel stirred tank of 1500~2500 liters of volumes, and the stirred tank ratio of height to diameter is 1: 1, and the ratio of stirred tank internal diameter and stirrer diameter is 3~5: 1; The space internal diameter that baffle plate surrounds in reactor is 0.85~0.86: 1 with reactor internal diameter ratio, single height of baffle plate is 0.8~0.9: 1 with the ratio of kettle height, the thickness of single baffle plate is 3~4mm, and the spacing between described baffle plate and the inner wall of kettle is 0~0.005: 1 with reactor internal diameter ratio; The diameter of shaft is 50~70mm; The wheel hub of dasher is provided with 2 blades, blade vertical with shaft and with the angle of horizontal plane be 45 °~60 °, vane thickness is 3~4mm, width of blade is 80~100mm; The wheel hub of disc turbine formula agitator is provided with 6 groups of blades, and every group is that 45 °~60 ° blade is formed by 2 angles, and vane thickness is 3~4mm, and width of blade is 80~100mm.
CN2009200474303U 2009-07-16 2009-07-16 Combination stirring vessel Expired - Fee Related CN201445957U (en)

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102532504A (en) * 2011-12-16 2012-07-04 化学工业第二设计院宁波工程有限公司 Synthetic reaction kettle suitable for preparation of carbon dioxide-epoxypropane copolymer
CN102861546A (en) * 2012-09-25 2013-01-09 科迈化工股份有限公司 Stirring apparatus used in DM (dibenzothiazyl disulfide) synthesizing process
CN106947687A (en) * 2017-05-06 2017-07-14 赤峰中元晟华生物燃气项目建设有限责任公司 A kind of big-and-middle-sized marsh-gas fermentation tank
CN109467136A (en) * 2018-12-26 2019-03-15 华友新能源科技(衢州)有限公司 A kind of preparation method for the ternary nickel cobalt manganese anode material presoma changing microcrystal grain accumulation mode

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102532504A (en) * 2011-12-16 2012-07-04 化学工业第二设计院宁波工程有限公司 Synthetic reaction kettle suitable for preparation of carbon dioxide-epoxypropane copolymer
CN102861546A (en) * 2012-09-25 2013-01-09 科迈化工股份有限公司 Stirring apparatus used in DM (dibenzothiazyl disulfide) synthesizing process
CN106947687A (en) * 2017-05-06 2017-07-14 赤峰中元晟华生物燃气项目建设有限责任公司 A kind of big-and-middle-sized marsh-gas fermentation tank
CN109467136A (en) * 2018-12-26 2019-03-15 华友新能源科技(衢州)有限公司 A kind of preparation method for the ternary nickel cobalt manganese anode material presoma changing microcrystal grain accumulation mode
CN109467136B (en) * 2018-12-26 2021-04-13 华友新能源科技(衢州)有限公司 Preparation method of ternary nickel-cobalt-manganese positive electrode material precursor for changing microcrystalline particle accumulation mode

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GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20100505

Termination date: 20160716

CF01 Termination of patent right due to non-payment of annual fee