CN201437556U - CNT pickling device of composite electrodeposition - Google Patents
CNT pickling device of composite electrodeposition Download PDFInfo
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- CN201437556U CN201437556U CN200920058653XU CN200920058653U CN201437556U CN 201437556 U CN201437556 U CN 201437556U CN 200920058653X U CN200920058653X U CN 200920058653XU CN 200920058653 U CN200920058653 U CN 200920058653U CN 201437556 U CN201437556 U CN 201437556U
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Abstract
The utility model relates to a CNT pickling device of composite electrodeposition. A stirrer is arranged in a pickling container. The upper end orifice of the pickling container is provided with a sealing plug. A water inlet pipe penetrates through the sealing plug and is communicated with the pickling container. The lower part of the pickling container is communicated with the inlet end of a centrifugal filter through a pipe and the outlet end of the centrifugal filter is communicated with a vacuum bottle through the pipe. The upper end orifice of the vacuum bottle is communicated with one end of a pumping filter through the pipe and the other end of the pumping filter is communicated with an exhaust gas receiver through the pipe. The lower side of the vacuum bottle is communicated with a waste liquid receiver through the pipe. The CNT is evenly dipped by acid liquor in the pickling container and the acid liquor after the pickling and the waste gas generated in the pickling process are respectively collected and stored by the waste liquid receiver and the exhaust gas receiver for the environmental protection and the human body health. The utility model has the advantages of complete and thorough cleaning, simple and convenient operation, safe and credible running and full waste material recycle.
Description
[technical field]
The utility model belongs to the pickler technical field, relates to a kind of pickler of carbon nanotube when being used for composite electrodeposition.
[background technology]
Since Japanese scientist Iijima since finding carbon nanotube (CNTs) in 1991, carbon nanotube has received increasing concern because of its excellent mechanics and optical property, because carbon nanotube has particular structure and good physics and chemical property, become in the preparation matrix material material of tool application prospect.At present; utilize carbon nanotube as wild phase; it is more to adopt composite electrodeposition technique to prepare the research of various metal-base composites; in carbon nanotube composite electrodeposition process; generally must carry out cleanup acid treatment to carbon nanotube; also there is not at present a kind of general pickler; generally carbon nanotube is put into beaker; add various acid solutions again and carry out pickling; after pickling, pour out acid solution again; wash with deionized water or distilled water at last, the weak point of this method is, because the reunion of carbon nanotube; it is even by acid soak that it is difficult for; acid solution after the pickling in the beaker is difficult for removing thoroughly; in addition, the waste gas that is produced in the acid cleaning process directly enters air, is unfavorable for environment protection and HUMAN HEALTH.Therefore, a kind of pickler that is used for carbon nanotubes in composite coating of design just seems and is even more important.
[utility model content]
In order to overcome the above-mentioned shortcoming of prior art, the utility model provide a kind of have cleaning completely, simple to operation, safe and reliable to operation and waste material fully reclaim advantage be used for composite electrodeposition the time carbon nanotube pickler.
The technical scheme that its technical problem that solves the utility model adopts is: a kind of pickler of carbon nanotube when being used for composite electrodeposition, the pickling container is arranged, in the pickling container, agitator is housed, upper port at the pickling container is equipped with sealing plug, water inlet pipe runs through sealing plug and communicates with the pickling container, entrance end in pickling container bottom by conduit and centrifugal filter links, the exit end of centrifugal filter links by conduit and vacuum vessel, the upper port of vacuum vessel links by an end of conduit and suction filtration machine, the other end of suction filtration machine links by conduit and waste gas holder, and bottom one side of vacuum vessel links by conduit and waste liquid holder.
Be provided with several layers organic solvent micropore filtering film in the described centrifugal filter.
Described pickling container is plastic containers.
The beneficial effects of the utility model are: under the effect of agitator, carbon nanotube can be even by acid soak in the pickling container, the waste gas that is produced in acid solution after the pickling and the acid cleaning process is collected storage by waste liquid holder and waste gas holder respectively, helps environment protection and HUMAN HEALTH; Use the organic solvent micropore filtering film in the centrifugal filter to prevent that effectively carbon nanotube from stopping up the micropore of multilayer film, the assurance waste liquid separates smoothly with carbon nanotube, use the suction filtration machine that the pickling container is vacuumized processing, utilizing draught head that acid solution and diluent are extracted out gradually, is neutral up to the pH value; Have cleaning completely, simple to operation, safe and reliable to operation and waste material fully reclaims advantage, is a kind of multipurpose plant that carbon nanotube carries out pickling when being used for composite electrodeposition.
[description of drawings]
Fig. 1 is a structural representation of the present utility model;
Among the figure: 1-water inlet pipe, 2-sealing plug, 3-agitator, 4-pickling container, 5-centrifugal filter, 6-vacuum vessel, 7-suction filtration machine, 8-waste gas holder, 9-waste liquid holder, 10-conduit, 11-organic solvent micropore filtering film.
[embodiment]
Below in conjunction with drawings and Examples the utility model is further specified:
Referring to Fig. 1, a kind of pickler of carbon nanotube when being used for composite electrodeposition, pickling container 4 is arranged, this pickling container 4 adopts plastic containers, agitator 3 is housed in pickling container 4, under the effect of agitator 3, carbon nanotube can be even by acid soak in pickling container 4, upper port at pickling container 4 is equipped with sealing plug 2, water inlet pipe 1 runs through sealing plug 2 and communicates with pickling container 4, in pickling container 4, add deionized water or distilled water washes by water inlet pipe 1, link by the entrance end of conduit 10 in pickling container 4 bottoms with centrifugal filter 5, be provided with several layers organic solvent micropore filtering film 11 in this centrifugal filter 5, be provided with the organic solvent micropore filtering film 11 of layer 2-3 among the embodiment, use the organic solvent micropore filtering film 11 in the centrifugal filter 5 to prevent that effectively carbon nanotube from stopping up the micropore of multilayer film, the assurance waste liquid separates smoothly with carbon nanotube; The exit end of centrifugal filter 5 links by conduit 10 and vacuum vessel 6, the upper port of vacuum vessel 6 links by the end of conduit 10 with suction filtration machine 7, using 7 pairs of pickling containers 4 of suction filtration machine to vacuumize processing, utilize draught head that acid solution and diluent are extracted out gradually, is neutral up to the pH value; The other end of suction filtration machine 7 links by conduit 10 and waste gas holder 8; bottom one side of vacuum vessel 6 links by conduit 10 and waste liquid holder 9; the waste gas that is produced in acid solution after the pickling and the acid cleaning process is collected storage by waste liquid holder 9 and waste gas holder 8 respectively, helps environment protection and HUMAN HEALTH.
Claims (2)
1. the pickler of a carbon nanotube when being used for composite electrodeposition, the pickling container is arranged, it is characterized in that: in the pickling container, agitator is housed, upper port at the pickling container is equipped with sealing plug, water inlet pipe runs through sealing plug and communicates with the pickling container, entrance end in pickling container bottom by conduit and centrifugal filter links, the exit end of centrifugal filter links by conduit and vacuum vessel, the upper port of vacuum vessel links by an end of conduit and suction filtration machine, the other end of suction filtration machine links by conduit and waste gas holder, and bottom one side of vacuum vessel links by conduit and waste liquid holder.
2. the pickler of carbon nanotube when being used for composite electrodeposition as claimed in claim 1 is characterized in that: be provided with several layers organic solvent micropore filtering film in the described centrifugal filter.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN200920058653XU CN201437556U (en) | 2009-06-18 | 2009-06-18 | CNT pickling device of composite electrodeposition |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN200920058653XU CN201437556U (en) | 2009-06-18 | 2009-06-18 | CNT pickling device of composite electrodeposition |
Publications (1)
Publication Number | Publication Date |
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CN201437556U true CN201437556U (en) | 2010-04-14 |
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Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
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CN200920058653XU Expired - Fee Related CN201437556U (en) | 2009-06-18 | 2009-06-18 | CNT pickling device of composite electrodeposition |
Country Status (1)
Country | Link |
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CN (1) | CN201437556U (en) |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101591795B (en) * | 2009-06-18 | 2011-06-29 | 广东韶配动力机械有限公司 | Pickling unit for carbon nanotubes in composite coating and using method thereof |
CN103435038A (en) * | 2013-08-16 | 2013-12-11 | 西安工程大学 | Separation device and separation method of activated carbon and pickling solution in preparation of activated carbon from sludge |
CN117646268A (en) * | 2024-01-26 | 2024-03-05 | 江苏台祥自动化科技有限公司 | Electroplating equipment |
-
2009
- 2009-06-18 CN CN200920058653XU patent/CN201437556U/en not_active Expired - Fee Related
Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101591795B (en) * | 2009-06-18 | 2011-06-29 | 广东韶配动力机械有限公司 | Pickling unit for carbon nanotubes in composite coating and using method thereof |
CN103435038A (en) * | 2013-08-16 | 2013-12-11 | 西安工程大学 | Separation device and separation method of activated carbon and pickling solution in preparation of activated carbon from sludge |
CN103435038B (en) * | 2013-08-16 | 2015-06-24 | 西安工程大学 | Separation device and separation method of activated carbon and pickling solution in preparation of activated carbon from sludge |
CN117646268A (en) * | 2024-01-26 | 2024-03-05 | 江苏台祥自动化科技有限公司 | Electroplating equipment |
CN117646268B (en) * | 2024-01-26 | 2024-04-16 | 江苏台祥自动化科技有限公司 | Electroplating equipment |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20100414 Termination date: 20150618 |
|
EXPY | Termination of patent right or utility model |