CN201250112Y - Novel ultrasonic hydrolysis device - Google Patents
Novel ultrasonic hydrolysis device Download PDFInfo
- Publication number
- CN201250112Y CN201250112Y CNU2008200079526U CN200820007952U CN201250112Y CN 201250112 Y CN201250112 Y CN 201250112Y CN U2008200079526 U CNU2008200079526 U CN U2008200079526U CN 200820007952 U CN200820007952 U CN 200820007952U CN 201250112 Y CN201250112 Y CN 201250112Y
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- hydrolysis
- ultrasonic wave
- tower
- intensified
- utility
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Abstract
The utility model relates to a novel hydrolysis device, which consists of a hydrolysis tower, a ultrasonic strengthening device and a catalyst load stuffing layer. Through the cooperation effect of the ultrasonic wave and special active catalyst that is loaded on the stuffing layer, the hydrolysis process of the grease is strengthened, thereby improving the hydrolysis rate of the grease and the reaction speed.
Description
Technical field
The utility model belongs to the utilisation technology of ultrasonic wave at chemical field, is a kind of hydrolysis device that utilizes ultrasonic wave to carry out the reaction of grease enhanced hydrolysis.
Background technology
Present domestic oils industry, the production technique great majority of lipid acid adopt high temperature, the hydrolysis of high pressure adverse current, have advantages such as reliable, stable, that scale is big, but also existence are not enough, and are not high enough as percent hydrolysis, are about 95-97%; Be not suitable for the high fat hydrolysis of degree of unsaturation; High temperature and high pressure causes the energy consumption height, shortcomings such as perishable in the tower, easy polymerization coking.
Summary of the invention
The purpose of this utility model is to overcome the shortcoming of prior art, and a kind of novel ultrasonic wave hydrolysis device is provided.
The utility model hydrolysis device is made of hydrolysis tower, ultrasound-enhanced device and catalyst cupport packing layer.The horn of intensified by ultrasonic wave device and emitting head insert in the hydrolysis tower, are distributed in the main reaction region of hydrolysis tower.Sp act binary composite catalyst with ultrasound-enhanced effect is carried on the filler and is installed on the hydrolysis tower main reaction region.Being characterized as of the utility model ultrasonic wave hydrolysis device increased the intensified by ultrasonic wave device, can adjust the frequency and the power of intensified by ultrasonic wave device according to different greases; Increased the catalyst cupport packing layer, ultrasonic hydrolysis has been had synergy.
The function of the utility model ultrasonic wave hydrolysis device is achieved by the following scheme, and fills with at hydrolysis tower under the situation of oil and water, feeds steam heating.Open ultrasonic generator when temperature reaches 80～180 ℃, the cavatition that produces by ultrasonic wave, and the synergy of packing layer catalyzer can shorten inductive phase of fat hydrolysis, improve percent hydrolysis.
The utility model with the advantage that present hydrolysis device relatively has is:
1, improves the percent hydrolysis of fat hydrolysis reaction, reach more than 98.5%;
2, reduce the temperature and pressure of reaction, cut down the consumption of energy, can be suitable for wider raw material range.
3, reduce polymerization, the coking of material, minimizing equipment parking wash number.
The utility model intensified by ultrasonic wave hydrolysis device will be described in further detail in conjunction with the accompanying drawings.
Fig. 1 is the structural representation of the utility model intensified by ultrasonic wave hydrolysis device.
1-hydrolysis tower; The import of 2-grease; The import of 3-process water; The outlet of 4-lipid acid; The outlet of 5-sugar water; 6-intensified by ultrasonic wave device; 7-support of the catalyst filler.
Fig. 2 is the ultrasonic unit structural representation of the utility model intensified by ultrasonic wave hydrolysis device.
A-emitting head; B-horn; C-horn cooling chamber; D-joint flange; E-horn heat-eliminating medium inlet; F-horn heat-eliminating medium outlet; G-cooling chamber joint flange; H-transverter cooling chamber; I-transverter heat-eliminating medium inlet; J-transverter heat-eliminating medium outlet; K-transverter.
See figures.1.and.2, the utility model intensified by ultrasonic wave hydrolysis device is that intensified by ultrasonic wave device 6 is embedded in the main reaction region of hydrolysis tower 1, by the ultrasound-enhanced active catalyzer that has in the main reaction region filling carrier 7 the fat hydrolysis process is strengthened simultaneously.
The utility model intensified by ultrasonic wave hydrolysis device example, it is the glyceride stock that the grease import 2 at hydrolysis tower 1 adds, and adds process waters in process water import 3, opens the intensified by ultrasonic wave device when detecting hydrolysis tower 3 hydrolysis area temperature and reach 80～180 ℃.By detecting, the acid number of lipid acid outlet 4 is: 177.6～178.2mgKOH/g, promptly the fat hydrolysis rate reaches 98.6～99.0%.
Claims (2)
1, a kind of novel hydrolysis device is made of hydrolysis tower, intensified by ultrasonic wave device and catalyst cupport packing layer, it is characterized in that: the horn of described ultrasonic transducer is inserted hydrolysis tower inside; The catalyst cupport packing layer is installed in the hydrolysis tower main reaction region; Can regulate horn quantity in the tower according to processing power.
2, ultrasonic wave hydrolysis device according to claim 1 is characterized in that adopting the binary composite catalyst of the sp act with ultrasound-enhanced effect, and is carried on the filler.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNU2008200079526U CN201250112Y (en) | 2007-12-05 | 2008-04-28 | Novel ultrasonic hydrolysis device |
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN200720199912 | 2007-12-05 | ||
| CN200720199912.1 | 2007-12-05 | ||
| CNU2008200079526U CN201250112Y (en) | 2007-12-05 | 2008-04-28 | Novel ultrasonic hydrolysis device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN201250112Y true CN201250112Y (en) | 2009-06-03 |
Family
ID=40745783
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CNU2008200079526U Expired - Fee Related CN201250112Y (en) | 2007-12-05 | 2008-04-28 | Novel ultrasonic hydrolysis device |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN201250112Y (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103253730A (en) * | 2013-05-16 | 2013-08-21 | 清华大学 | Ultrasonic-wave-intensified hydrolytic treatment method for kitchen wastes |
| CN105330020A (en) * | 2015-11-06 | 2016-02-17 | 东莞市环境科学研究所 | Synchronous biochemical advanced oxidation liquid waste treatment method and device |
| CN114699883A (en) * | 2022-04-22 | 2022-07-05 | 浙江大学 | Catalyst-synergistic external field-enhanced carbon dioxide low-energy-consumption desorption system and method |
-
2008
- 2008-04-28 CN CNU2008200079526U patent/CN201250112Y/en not_active Expired - Fee Related
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103253730A (en) * | 2013-05-16 | 2013-08-21 | 清华大学 | Ultrasonic-wave-intensified hydrolytic treatment method for kitchen wastes |
| CN103253730B (en) * | 2013-05-16 | 2015-09-30 | 清华大学 | A kind of changing food waste intensified by ultrasonic wave hydrolysis process for treating |
| CN105330020A (en) * | 2015-11-06 | 2016-02-17 | 东莞市环境科学研究所 | Synchronous biochemical advanced oxidation liquid waste treatment method and device |
| CN114699883A (en) * | 2022-04-22 | 2022-07-05 | 浙江大学 | Catalyst-synergistic external field-enhanced carbon dioxide low-energy-consumption desorption system and method |
| CN114699883B (en) * | 2022-04-22 | 2023-06-13 | 浙江大学 | Catalyst-assisted outfield-enhanced carbon dioxide low-energy desorption system and method |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| C17 | Cessation of patent right | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20090603 Termination date: 20140428 |