CN201186882Y - Drying or absorbing tower for preparing sulfuric acid - Google Patents

Drying or absorbing tower for preparing sulfuric acid Download PDF

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Publication number
CN201186882Y
CN201186882Y CNU2007200656389U CN200720065638U CN201186882Y CN 201186882 Y CN201186882 Y CN 201186882Y CN U2007200656389 U CNU2007200656389 U CN U2007200656389U CN 200720065638 U CN200720065638 U CN 200720065638U CN 201186882 Y CN201186882 Y CN 201186882Y
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CN
China
Prior art keywords
acid
drying
tower body
absorption tower
tower
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Expired - Fee Related
Application number
CNU2007200656389U
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Chinese (zh)
Inventor
王一丁
陈南洋
袁爱武
舒春桃
孙南峰
吴桂荣
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CINF Engineering Corp Ltd
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Changsha Design Institute of Nonferrous Metallurgy
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Priority to CNU2007200656389U priority Critical patent/CN201186882Y/en
Application granted granted Critical
Publication of CN201186882Y publication Critical patent/CN201186882Y/en
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Expired - Fee Related legal-status Critical Current

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Abstract

The utility model discloses a drying or absorbing tower for the sulfuric acid preparation, which is mainly used for drying SO2-containg fume and absorbing SO3-containg fume during the sulfuric acid preparation process. An acid return passage is formed on one side of the drying tower body or the absorbing tower body and communicates with a concentrated acid circulation tank via a transition section, and the drying tower body or the absorbing tower body and the concentrated acid circulation tank are arranged on a same base, connected into a whole, and located on a same plane, thereby saving the construction and production operation cost, and reducing the manufacture cost of the production device.

Description

Drying or absorption tower in the sulfuric acid preparation
Technical field:
The utility model relates to and is used to contain SO in a kind of sulphuric acid process 2The drying of flue gas and SO 3The tower groove of the absorption of flue gas refers to a kind of drying or absorption tower of tower groove one especially.
Background technology:
In the sulphuric acid process, contain SO 2The drying of flue gas and SO 3The absorption of flue gas is two important steps that do not link up mutually.Because these two steps all are to use the vitriol oil as absorption agent, dry, equipment that absorption is adopted all is again the acid resistance filler tower of the spray vitriol oil, the drying of moisture content and SO in the flue gas 3To be absorbed in the Principle of Process of being carried out in the packing tower identical.Therefore in engineering design, drying tower in the sulphuric acid process almost completely identical with the structure on absorption tower (generally being selected demister difference) increases the versatility of device fabrication and spare parts as far as possible, so that production management and reduction production run cost.
In sulphuric acid process, drying tower, absorption tower are matching used with its concentrated acid circulation groove.In actual gas washing in SA production engineering design, the drying of traditional structure, absorption tower and its supporting concentrated acid circulation groove are separate configuration.Generally, dry, absorption tower is arranged on the civil engineering platform, the concentrated acid circulation groove be arranged on tower body under (or below, positive front), the concentrated acid cooler configuration is by the concentrated acid circulation groove.This distributing style on the whole, layout structure is reasonable, engineering application experience maturation is the distributing style that generally adopts in the gas washing in SA production design.But this distributing style has following disappearance:
1, owing to dry, absorption tower are arranged on the civil engineering platform, and the spacing of tower body has certain requirement, and tower body weight is big, and therefore required civil engineering platform floor space is big, and the span of support post is bigger.Need the column and the supporting traverse of preparation larger sectional area in the civil Engineering Design, high to the supporting capacity requirement of civil engineering foundation, make that the civil engineering costs cost is higher.
2, owing to top dry, that the absorption tower is arranged on the concentrated acid circulation groove, and concentrated acid circulation groove upper space makes that apart from certain requirement (needing to consider the installation, maintenance hoisting height of sour pump) is arranged the lift of recycle acid lifting is bigger.Need the cyclic acid pump that allocating power is big, lift is high, so the buying expenses of equipment and running cost are all higher.
3, since the concentrated acid circulation groove dry, that the absorption tower matches with it for controlling up and down, the concentrated acid water cooler need dispose in addition with selecting, collaborates for preventing the acid tube road, also need on the sour export pipeline on drying, absorption tower an acid seal device be set.Make between the tower groove vitriol oil circulating line complex circuit and to come and go distance long.Caused the pipeline cost of manufacture higher, the construction and installation workload too much is unfavorable for production management in the leak point on the way than big and pipeline.
The utility model content:
Technical problem to be solved in the utility model is: the deficiency at existing in dry in the above-mentioned prior art, absorption tower and its concentrated acid circulation groove mode arranged apart, a kind of dry tower body is provided, absorb tower body and cell body connect into an integral body and be located at grade sulfuric acid in preparing drying or absorption tower.
In order to solve the problems of the technologies described above, the technical scheme that the utility model adopted is: drying or absorption tower in a kind of sulfuric acid preparation, it comprises dry tower body or absorbs tower body, concentrated acid circulation cell body, this drying tower body or absorption tower body and concentrated acid circulation cell body are all cylindrical shell, the liner tile masonry, this drying tower body or absorb that tower body is provided with successively from bottom to up that inlet mouth, filler support brick arch, advance acid and acid separating device, acid inlet, demister, air outlet, filler supports on the brick arch and advances to be filled with the porcelain ring filler between acid and acid separating device; The cell body of this concentrated acid circulation cell body is provided with recycle acid pumping hole, overflow port, reaches the acid discharge mouth; Be characterized in: described dry tower body or absorb tower body one side and have back sour paths, and being communicated with concentrated acid circulation cell body by transition section, and should the drying tower body or absorption tower body and concentrated acid circulation cell body be seated on the same base.
For reducing the opening stress of dry cylindrical shell or absorber tower cylinder and concentrated acid circulation groove cylindrical shell connection, this transition section adopts half waist shape, and is made by the Steel Sheel of half waist shape, is provided with liner tile in the Steel Sheel.
Because it is different in dry tower body or the absorption tower body with the intravital gaseous tension of concentrated acid circulation groove, the air flue that needs consideration to utilize the liquid level of recycle acid to seal between the tower groove prevents to collaborate, so offer two semi-circular through hole in going back to sour paths and transition section joint on the liner tile of transition section bottom.Both guarantee the area of time sour paths, reduced the height liquid seal of required acid solution again, thereby reduced the height of concentrated acid circulation cell body.
For preventing that the intravital filler fragment in dry tower body or absorption tower from causing erosion to the pump housing to the drift about local diluted acid that forms at sour face of the damage of the pump housing and the intravital make up water of concentrated acid circulation groove, in concentrated acid circulation cell body, be provided with sour partition wall between the concentrated acid recycle pump of transition section and recycle acid pumping hole below.Thereby can be with filler fragment retaining in the wall bottom, and allow float and have the acid solution of water face to flow to circulation cell body inwall one side is circuitous along sour partition wall, so that the fully mutual tumble mixed of water liquid level and acid solution face, form the high concentrated acid solution of concentration stabilize, thereby the qualified concentrated sulfuric acid solution of assurance output circulates and produces qualified finished acid.This high concentrated acid solution enters in the concentrated acid circulation cell body through the vertical mixing acid of sour partition wall passageway breach.
Above-mentioned base is welded into one-piece construction by base plate and section steel beam, to be born drying by base integral body or to absorb tower body and concentrated acid circulation groove body weight.And should the drying tower body or absorb tower body and concentrated acid circulation cell body directly is seated on the ground foundation of civil work table top that is complementary with its shape by base.
The utility model compared with prior art has following advantage:
1, because tower body and cell body connect into an integral body, and directly is located on the ground on the foundation of civil work table top, cancelled civil engineering tower platform by a unsplit bedplate.Foundation of civil work simple shape, whole stressed area the ground pressure to foundation of civil work greatly are little relatively, thereby have saved a large amount of civil engineering costs.
2, since tower body and cell body be located at grade, so owing to the tower platform has been cancelled in drying, the absorption tower of tower groove one in configuration, make the concentrated acid water cooler can be placed on the vacant lot between two towers (dry with absorption tower or drying and two absorption towers), with tower, groove is parallel controls, form floor space with respect to tower, groove separate configuration is much smaller, meets the spirit that national requirements is saved the area.
3, because tower body and cell body are located at grade, so the lifting lift of recycle acid reduces greatly, only needs allocating power less, the cyclic acid pump that lift is lower.The all corresponding reduction of equipment purchase expense and production run expense.
4, because tower body and cell body have connected into an integral body, saved go back to acid tube road of recycle acid, cancelled pipeline acid seal device.Because the concentrated acid water cooler is arranged side by side with tower body, make that the recycle acid route of pipe line is very compact and succinct between tower and the groove again between Liang Ta.Compare with traditional tower groove form arranged apart, its recycle acid pipe-line contraction in length is about 60%, has both significantly reduced pipeline fabrication and installation cost, has significantly reduced the leak point on the acid tube road again, is more conducive to production management and maintenance and repair.
5, because tower body and cell body have connected into an integral body, a part of recycle acid amount has also just been stored in the bottom of tower body, thereby design round-robin physical dimension reduces relatively, has so both reduced floor space, make and recycle acid pipeline compactness reduced the device fabrication cost again.
Description of drawings:
Fig. 1 is a structure cut-away view of the present utility model.
Fig. 2 is the vertical view of base of the present utility model.
Fig. 3 is the side-view of base of the present utility model.
Fig. 4 is the synoptic diagram of transition section of the present utility model.
Fig. 5 is the cut-away view of Fig. 1 along the A-A line.
Embodiment:
Referring to Fig. 1, the utility model is drying or the absorption tower in the sulfuric acid preparation, and it comprises: dry tower body or absorption tower body 1, concentrated acid circulation cell body 2, this drying tower body or absorption tower body 1 and concentrated acid circulation cell body 2 are all steel cylinders, liner tile masonry 3.This drying tower body or absorption tower body 1, from bottom to up, be provided with successively that inlet mouth 11, filler support brick arch 12, advance acid and acid separating device 13, acid inlet 14, demister 15, air outlet 16, filler supports on the brick arch 12 and advances acid and 13 of acid separating devices are filled with porcelain ring filler 17, this drying tower body or absorption tower body 1 have back sour paths 4 in a side in addition, and are communicated with concentrated acid circulation cell body 2 by transition section 5.The cell body of this concentrated acid circulation cell body 2 is provided with recycle acid pumping hole 21, overflow port 22, reaches acid discharge mouth 23, is provided with sour partition wall 24 in this concentrated acid circulation cell body 2 between the concentrated acid recycle pump (not shown) of transition section 5 and recycle acid pumping hole 21 belows.The both sides of this acid partition wall 24 respectively with concentrated acid circulation cell body in the brick structures 3 established join, wherein, a side top of joint has mixing acid passageway breach 241, the opposite side bottom has maintenance acid discharge mouth 242, as shown in Figure 5.
Referring to Fig. 2 and shown in Figure 3, this drying tower body or absorption tower body 1 and concentrated acid circulation cell body 2 are seated on the same base 6, and this base 6 is welded into one-piece construction by base plate 61 and section steel beam 62.
The transition section 5 that is provided with between this drying tower body or absorption tower body 1 and the concentrated acid circulation cell body 2 is the sour paths between tower body and the cell body.As shown in Figure 4, transition section 5 is half waist shape, is made by half waist shape Steel Sheel 51, is provided with liner tile 52.The length of transition section is generally 600-800mm.Offer two semi-circular through hole 53 in returning sour paths 4 with transition section 5 joints on the liner brick wall of this transition section bottom.

Claims (6)

1, drying tower or the absorption tower in a kind of sulfuric acid preparation, it comprises dry tower body or absorbs tower body (1), concentrated acid circulation cell body (2), this drying tower body or absorption tower body (1) and concentrated acid circulation cell body (2) are all cylindrical shell, liner tile masonry (3), this drying tower body or absorb that tower body (1) is provided with successively from bottom to up that inlet mouth (11), filler support brick arch (12), advance acid and acid separating device (13), acid inlet (14), demister (15), air outlet (16), filler supports brick arch (12) and goes up and advance between sour and acid separating device (13) to be filled with porcelain ring filler (17); The cell body of this concentrated acid circulation cell body (2) is provided with recycle acid pumping hole (21), overflow port (22), reaches acid discharge mouth (23); It is characterized in that: described dry tower body or absorption tower body (1) one side have back sour paths (4), and be communicated with concentrated acid circulation cell body (2) by transition section (5), and should the drying tower body or absorption tower body (1) and concentrated acid circulation cell body (2) be seated on the same base (6).
2, drying or the absorption tower in the sulfuric acid preparation according to claim 1, it is characterized in that: described transition section (5) is half waist shape, is made by half waist shape Steel Sheel (51), is provided with liner tile (52) in this Steel Sheel.
3, drying or the absorption tower in the sulfuric acid preparation according to claim 2, it is characterized in that: the liner tile (52) of described transition section bottom goes up in returning sour paths (4) and offers two semi-circular through hole (53) with transition section (5) joint.
4, drying or the absorption tower in the sulfuric acid preparation according to claim 1 is characterized in that: be provided with sour partition wall (24) in the described concentrated acid circulation cell body (2) between the concentrated acid recycle pump of transition section and recycle acid pumping hole below.
5, drying or the absorption tower in the sulfuric acid preparation according to claim 4, it is characterized in that: the both sides of described sour partition wall (24) respectively with concentrated acid circulation cell body in the brick structures (3) established join, wherein, one side top of joint has mixing acid passageway breach (241), and the opposite side bottom has maintenance acid discharge mouth (242).
6, drying or the absorption tower in the sulfuric acid preparation according to claim 1, it is characterized in that: described base (6) is welded into one-piece construction by base plate (61) and section steel beam (62).
CNU2007200656389U 2007-12-29 2007-12-29 Drying or absorbing tower for preparing sulfuric acid Expired - Fee Related CN201186882Y (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CNU2007200656389U CN201186882Y (en) 2007-12-29 2007-12-29 Drying or absorbing tower for preparing sulfuric acid

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CNU2007200656389U CN201186882Y (en) 2007-12-29 2007-12-29 Drying or absorbing tower for preparing sulfuric acid

Publications (1)

Publication Number Publication Date
CN201186882Y true CN201186882Y (en) 2009-01-28

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103764269A (en) * 2011-09-09 2014-04-30 奥图泰有限公司 Packed tower
CN106365125A (en) * 2016-08-29 2017-02-01 金川集团股份有限公司 Device and method for absorbing free sulfur trioxide in fuming sulfuric acid through concentrated sulfuric acid

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103764269A (en) * 2011-09-09 2014-04-30 奥图泰有限公司 Packed tower
CN103764269B (en) * 2011-09-09 2016-08-17 奥图泰有限公司 Packed tower
CN106365125A (en) * 2016-08-29 2017-02-01 金川集团股份有限公司 Device and method for absorbing free sulfur trioxide in fuming sulfuric acid through concentrated sulfuric acid
CN106365125B (en) * 2016-08-29 2019-08-06 金川集团股份有限公司 A kind of concentrated sulfuric acid absorbs the device and method for the sulfur trioxide that dissociates in oleum

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C14 Grant of patent or utility model
GR01 Patent grant
C56 Change in the name or address of the patentee

Owner name: CHANGSHA ENGINEERING + RESEARCH INSTITUTE LTD. OF

Free format text: FORMER NAME: CHANGSHA DESIGN INST. OF NON-FERROUS METALLURGY

CP01 Change in the name or title of a patent holder

Address after: 410001 No. 199 Jiefang Middle Road, Hunan, Changsha

Patentee after: Changsha Engineering & Research Institute of Nonferrous Metallurgy Co., Ltd.

Address before: 410001 No. 199 Jiefang Middle Road, Hunan, Changsha

Patentee before: Changsha Design Inst. of Non-Ferrous Metallurgy

EE01 Entry into force of recordation of patent licensing contract

Assignee: Hechi Nanfang Non-ferrous Metal Smelting Co., Ltd.

Assignor: Changsha Engineering & Research Institute of Nonferrous Metallurgy Co., Ltd.

Contract record no.: 2011450000089

Denomination of utility model: Drying or absorbing tower for preparing sulfuric acid

Granted publication date: 20090128

License type: Exclusive License

Record date: 20110928

CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20090128

Termination date: 20161229

CF01 Termination of patent right due to non-payment of annual fee