CN201037134Y - Tubular reactor with static mixing element and biological diesel oil continuous reactor - Google Patents

Tubular reactor with static mixing element and biological diesel oil continuous reactor Download PDF

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Publication number
CN201037134Y
CN201037134Y CNU200720089873XU CN200720089873U CN201037134Y CN 201037134 Y CN201037134 Y CN 201037134Y CN U200720089873X U CNU200720089873X U CN U200720089873XU CN 200720089873 U CN200720089873 U CN 200720089873U CN 201037134 Y CN201037134 Y CN 201037134Y
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China
Prior art keywords
static mixing
mixing element
reactor
tubular reactor
heating unit
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Expired - Fee Related
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CNU200720089873XU
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Chinese (zh)
Inventor
马晓建
李洪亮
陈俊英
韩秀丽
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BIOCHEMISTRY ENGINEERING CENTER ZHENGZHOU UNIV
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BIOCHEMISTRY ENGINEERING CENTER ZHENGZHOU UNIV
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Priority to CNU200720089873XU priority Critical patent/CN201037134Y/en
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    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P30/00Technologies relating to oil refining and petrochemical industry
    • Y02P30/20Technologies relating to oil refining and petrochemical industry using bio-feedstock

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Abstract

The utility model relates to a tubular reactor with static hybrid elements consisting of static hybrid elements arranged in the middle of a tube body and heating elements arranged outside the tube body. The heating elements are sleeve pipes which are arranged outside the tube body and work as a heating medium or resistance wires of an out-sleeved ceramic ring of a ceramic tube. The static hybrid elements are Kenics static hybrid elements or GK static hybrid elements. A biodiesel successive reaction device comprises a first-order reactor and a second-order reactor which are connected in series, wherein, the second-order reactor is connected with a separator; the front of the first-order reactor is connected with the tubular reactor with static hybrid elements which consists of static hybrid elements arranged in the middle of a tube body and heating elements arranged outside the tube body. The utility model manufactures biodiesel and has the advantages of simple equipment, low investment, low energy consumption and good effect.

Description

The tubular reactor and the biofuel continuous reaction apparatus of band static mixing element
Technical field
The utility model belongs to production of biodiesel device technique field, particularly a kind of tubular reactor and biofuel continuous reaction apparatus that has static mixing element.
Background technology
Along with continuous progress in science and technology, human more and more higher to the degree of dependence of the energy, cause the petrochemical industry resource to peter out.Biofuel can be used as the substitute of traditional petrifaction diesel, and combustionproperty is suitable, and sulfur-bearing, oxygen level are high and have biodegradability, can significantly reduce environmental pollution, have excellent environmental-protecting performance.Thereby, wide application prospect is arranged as a kind of novel renewable energy.
Existing biofuel reaction unit mostly is intermittently stirring-type greatly, and mixed effect is good inadequately, and energy consumption is very high.CN1740273A adopts coil pipe type reactor to realize continuous production, but before alcohol and grease enter tubular reactor, is preheating to the low-temperature values that sets by a cryogenic thermostat preheater earlier.Alcohol and grease feed in the tubular reactor that is heated by a high temperature constant temperature process furnace after mixing tank mixes again, are elevated to required high temperature values.This method need adopt special well heater and mixing tank to carry out the heating of alcohol oil, mix, and has increased facility investment.CN1743416A adopts two sections tubular reactors, all was added with interchanger and carries out heat exchange to improve temperature before two sections tubular reactors.This method need adopt special interchanger to carry out heat exchange.
The utility model content
The utility model purpose is to provide a kind of tubular reactor and biofuel continuous reaction apparatus of the band static mixing element that heating edge is reacted while mixing.
For reaching above-mentioned purpose, the utility model adopts following technical scheme: the tubular reactor of band static mixing element constitutes by being located at body intermediary static mixing element and being located at the outer heating unit of body.
Heating unit is to be located at the sleeve pipe that body is outer, supply heating medium to pass through.
Heating unit be located at that body is outer, the resistance wire of outer cotton up to ring or porcelain tube.
Static mixing element is Kenics static mixing element or GK static mixing element.
The biofuel continuous reaction apparatus, comprise mutual placed in-line A reactor and second reactor, second reactor connects separator, the tubular reactor of tape splicing static mixing element before the A reactor, the tubular reactor of band static mixing element constitutes by being located at body intermediary static mixing element and being located at the outer heating unit of body.
Heating unit is to be located at the sleeve pipe that body is outer, supply heating medium to pass through.
Heating unit be located at that body is outer, the resistance wire of outer cotton up to ring or porcelain tube.
Static mixing element is Kenics static mixing element or GK static mixing element.
In the utility model, tubular reactor constitutes by being located at body intermediary static mixing element and being located at the outer heating unit of body, can be single hose or telescoping, can or be welded to connect by flange between each section, it is spiral that profile can be coil pipe type, oval coil tube type, Long Circle.Static mixing element is known for those skilled in the art, be a series of structural similitudies of in body, placing, by certain regularly arranged stationary element, when fluid flows through, rely on the fluid self kinetic energy, realize constantly cutting, be out of shape, be shifted and converge, can realize the fluidic thorough mixing, energy consumption is low, compact construction, manufacturing is easy for installation, floor space is little, running cost is low.Static mixing element can be Kenics static cell, GK static cell.Heating unit is to be located at the body sleeve pipe outer, that pass through for heating medium or the resistance wire of outer cotton up to ring or porcelain tube.This tubular reactor can make raw materials such as grease and low first alcohol while mixing heating edge react, mix, the level of response height, can realize the segmentation gradient-heated, also can realize not having gradient-heated.
The biofuel continuous reaction apparatus is composed in series by the tubular reactor that has static mixing element and A reactor, second reactor and separator, thermal source can be steam, warm air, stack gas, fused salt, thermal oil or; A reactor, second reactor and separator are conventional equipment, and equipment is simple, invest for a short time, and energy consumption is low.Be applicable to and utilize grease, pure production biofuel and harmonic biodiesel.When being used for harmonic biodiesel, only adopt tubular reactor to get final product.The utility model manufacturing is simple, and special heating, mixing device need be provided, and is suitable for industrial-scale production.
Description of drawings
Fig. 1 is a biofuel continuous reaction apparatus structural representation.Wherein, horizontal arrow is the material movement direction, and perpendicular arrow is steam or wet goods flow direction.
Embodiment
Embodiment 1, biofuel continuous reaction apparatus, comprise mutual placed in-line A reactor 3 and second reactor 4, second reactor 4 connects separator 5, the tubular reactor of tape splicing static mixing element before the A reactor 3, the tubular reactor of band static mixing element is coil pipe type, constitutes by being located at body 6 intermediary static mixing elements 2 and being located at body 6 outer heating units 1.Static mixing element 2 is a simple helix shape static mixing element; Heating unit 1 is the interlayer sleeve pipe of band heating medium passage, heating medium in the sleeve pipe is a steam, material in heat passes to by tube wall in the pipe makes the material heating, the alcohols vaporization, carry out esterification, in reaction process, material cuts, converges through static mixing element, and the fluidic less turbulence strengthens, it is fierce to mix, and promotes two alternate quality, heat transmission greatly.After the tubular reactor reaction, enter maintenance for some time continuation reaction in A reactor 3, the second reactor 4 successively, reacted material is sent into separator 5 and is carried out the separation of biofuel.Separator 5 tops go out biofuel, and the bottom goes out raw glycerine.
In embodiment 2, the present embodiment, the tubular reactor of band static mixing element is oval coil tube type, and static mixing element 2 is the Kenics static mixing element, and the heating medium in the sleeve pipe is a thermal oil.Other are with embodiment 1.
In embodiment 3, the present embodiment, tubular reactor is a sector boss round screw thread tubular reactor, and static mixing element 2 is the GK static mixing element.Heating medium in the sleeve pipe is a fused salt.Other are with embodiment 1.
In embodiment 4, the present embodiment, heating unit 1 is the resistance wire of cotton up to ring or porcelain tube.Other are with embodiment 1.

Claims (8)

1. the tubular reactor of band static mixing element is characterized in that, constitutes by being located at body intermediary static mixing element and being located at the outer heating unit of body.
2. the tubular reactor of band static mixing element as claimed in claim 1 is characterized in that, heating unit is to be located at the sleeve pipe that body is outer, supply heating medium to pass through.
3. the tubular reactor of band static mixing element as claimed in claim 1 is characterized in that, heating unit be located at that body is outer, the resistance wire of outer cotton up to ring or porcelain tube.
4. as the tubular reactor of claim 1,2 or 3 described band static mixing elements, it is characterized in that static mixing element is Kenics static mixing element or GK static mixing element.
5. biofuel continuous reaction apparatus, comprise mutual placed in-line A reactor and second reactor, second reactor connects separator, it is characterized in that, the tubular reactor of tape splicing static mixing element before the A reactor, the tubular reactor of band static mixing element constitutes by being located at body intermediary static mixing element and being located at the outer heating unit of body.
6. biofuel continuous reaction apparatus as claimed in claim 5 is characterized in that, heating unit is to be located at the sleeve pipe that body is outer, supply heating medium to pass through.
7. biofuel continuous reaction apparatus as claimed in claim 5 is characterized in that, heating unit be located at that body is outer, the resistance wire of outer cotton up to ring or porcelain tube.
8. as claim 5,6 or 7 described biofuel continuous reaction apparatus, it is characterized in that static mixing element is Kenics static mixing element or GK static mixing element.
CNU200720089873XU 2007-04-02 2007-04-02 Tubular reactor with static mixing element and biological diesel oil continuous reactor Expired - Fee Related CN201037134Y (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CNU200720089873XU CN201037134Y (en) 2007-04-02 2007-04-02 Tubular reactor with static mixing element and biological diesel oil continuous reactor

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CNU200720089873XU CN201037134Y (en) 2007-04-02 2007-04-02 Tubular reactor with static mixing element and biological diesel oil continuous reactor

Publications (1)

Publication Number Publication Date
CN201037134Y true CN201037134Y (en) 2008-03-19

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Family Applications (1)

Application Number Title Priority Date Filing Date
CNU200720089873XU Expired - Fee Related CN201037134Y (en) 2007-04-02 2007-04-02 Tubular reactor with static mixing element and biological diesel oil continuous reactor

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CN (1) CN201037134Y (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101935593A (en) * 2010-09-07 2011-01-05 徐荣江 Method for preparing biodiesel by adopting supercritical methanol continuous process

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101935593A (en) * 2010-09-07 2011-01-05 徐荣江 Method for preparing biodiesel by adopting supercritical methanol continuous process
CN101935593B (en) * 2010-09-07 2012-10-03 徐荣江 Method for preparing biodiesel by adopting supercritical methanol continuous process

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GR01 Patent grant
C17 Cessation of patent right
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20080319

Termination date: 20130402