CN1982394A - Production of inorganic mineral colloid binder - Google Patents
Production of inorganic mineral colloid binder Download PDFInfo
- Publication number
- CN1982394A CN1982394A CN 200510048035 CN200510048035A CN1982394A CN 1982394 A CN1982394 A CN 1982394A CN 200510048035 CN200510048035 CN 200510048035 CN 200510048035 A CN200510048035 A CN 200510048035A CN 1982394 A CN1982394 A CN 1982394A
- Authority
- CN
- China
- Prior art keywords
- inorganic mineral
- colloidal adhesive
- weight percentage
- primary election
- stir
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 229910052500 inorganic mineral Inorganic materials 0.000 title claims abstract description 34
- 239000000084 colloidal system Substances 0.000 title claims description 7
- 238000004519 manufacturing process Methods 0.000 title abstract description 3
- 239000011230 binding agent Substances 0.000 title abstract 2
- 239000002002 slurry Substances 0.000 claims abstract description 8
- 238000001914 filtration Methods 0.000 claims abstract description 6
- 230000005484 gravity Effects 0.000 claims abstract description 6
- 239000012535 impurity Substances 0.000 claims abstract description 6
- 239000000853 adhesive Substances 0.000 claims description 20
- 230000001070 adhesive effect Effects 0.000 claims description 20
- 238000006243 chemical reaction Methods 0.000 claims description 10
- 238000003756 stirring Methods 0.000 claims description 9
- 238000005516 engineering process Methods 0.000 claims description 8
- 238000002360 preparation method Methods 0.000 claims description 8
- 230000003068 static effect Effects 0.000 claims description 6
- 238000010009 beating Methods 0.000 claims description 5
- 238000011109 contamination Methods 0.000 claims description 5
- 238000000151 deposition Methods 0.000 claims description 5
- 239000011259 mixed solution Substances 0.000 claims description 5
- 239000008239 natural water Substances 0.000 claims description 5
- 238000000926 separation method Methods 0.000 claims description 5
- SVPXDRXYRYOSEX-UHFFFAOYSA-N bentoquatam Chemical compound O.O=[Si]=O.O=[Al]O[Al]=O SVPXDRXYRYOSEX-UHFFFAOYSA-N 0.000 claims description 4
- 239000004927 clay Substances 0.000 claims description 3
- 239000000126 substance Substances 0.000 abstract description 5
- 239000002537 cosmetic Substances 0.000 abstract description 3
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 abstract 2
- 238000003801 milling Methods 0.000 abstract 2
- 239000012467 final product Substances 0.000 abstract 1
- 239000007788 liquid Substances 0.000 abstract 1
- 238000004537 pulping Methods 0.000 abstract 1
- 229910000029 sodium carbonate Inorganic materials 0.000 abstract 1
- 235000017550 sodium carbonate Nutrition 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
- 239000003795 chemical substances by application Substances 0.000 description 8
- 239000000606 toothpaste Substances 0.000 description 7
- 229940034610 toothpaste Drugs 0.000 description 7
- 229920000881 Modified starch Polymers 0.000 description 5
- 239000004368 Modified starch Substances 0.000 description 5
- 235000019426 modified starch Nutrition 0.000 description 5
- 238000004513 sizing Methods 0.000 description 5
- 239000007787 solid Substances 0.000 description 5
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 4
- 235000013399 edible fruits Nutrition 0.000 description 4
- 239000000463 material Substances 0.000 description 4
- 239000000843 powder Substances 0.000 description 4
- 239000002994 raw material Substances 0.000 description 4
- 239000011734 sodium Substances 0.000 description 4
- 239000004372 Polyvinyl alcohol Substances 0.000 description 3
- 239000010451 perlite Substances 0.000 description 3
- 235000019362 perlite Nutrition 0.000 description 3
- 229920002451 polyvinyl alcohol Polymers 0.000 description 3
- 238000009987 spinning Methods 0.000 description 3
- 239000007844 bleaching agent Substances 0.000 description 2
- 235000009508 confectionery Nutrition 0.000 description 2
- 230000018044 dehydration Effects 0.000 description 2
- 238000006297 dehydration reaction Methods 0.000 description 2
- 239000003599 detergent Substances 0.000 description 2
- 238000001035 drying Methods 0.000 description 2
- 239000003995 emulsifying agent Substances 0.000 description 2
- 239000000835 fiber Substances 0.000 description 2
- 235000011187 glycerol Nutrition 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 229920003023 plastic Polymers 0.000 description 2
- 239000004033 plastic Substances 0.000 description 2
- 230000008719 thickening Effects 0.000 description 2
- 235000013311 vegetables Nutrition 0.000 description 2
- FWVCSXWHVOOTFJ-UHFFFAOYSA-N 1-(2-chloroethylsulfanyl)-2-[2-(2-chloroethylsulfanyl)ethoxy]ethane Chemical compound ClCCSCCOCCSCCCl FWVCSXWHVOOTFJ-UHFFFAOYSA-N 0.000 description 1
- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 description 1
- NIXOWILDQLNWCW-UHFFFAOYSA-N 2-Propenoic acid Natural products OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 description 1
- 229920000742 Cotton Polymers 0.000 description 1
- FKNQFGJONOIPTF-UHFFFAOYSA-N Sodium cation Chemical compound [Na+] FKNQFGJONOIPTF-UHFFFAOYSA-N 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 230000000975 bioactive effect Effects 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- 239000003112 inhibitor Substances 0.000 description 1
- 238000001746 injection moulding Methods 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- -1 papermaking Substances 0.000 description 1
- 230000000704 physical effect Effects 0.000 description 1
- 231100000614 poison Toxicity 0.000 description 1
- 230000007096 poisonous effect Effects 0.000 description 1
- 229910001415 sodium ion Inorganic materials 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 239000004753 textile Substances 0.000 description 1
Landscapes
- Adhesives Or Adhesive Processes (AREA)
- Cosmetics (AREA)
- Paper (AREA)
Abstract
Production of binding agent is carried out by primary ore milling, mixed pulping for inorganic mineral 20-40% and water 60-80wt%, agitating to obtain mixed liquid, removing impurities by gravity ore milling method, filtering, concentrating above 100 meshes, adding Na2CO3 into concentrated slurry, agitating, chemically reacting, determining pH value=7.5+-0.5, and laying aside for 12hrs to obtain the final product. It is cheap and has excellent skin-caring and hair-caring functions, and it can be used for chemical paste and cosmetics.
Description
Technical field
The invention belongs to tackiness agent preparation technology field, particularly a kind of preparation technology of inorganic mineral colloidal adhesive.
Background technology
In the daily chemical industry field, toothpaste in the past, makeup tackiness agent can only play carrier function, and the dirt of can not dispelling, bleach, clean the teeth, even the perlite in the Chinese toothpaste also only is an additive, and perlite also will mix with other tackiness agent and could finally become colloid.From the physicals angle, perlite is a kind of high temperature expansible lagging material, and the content's index of Pb, As, Hg poisonous and harmful element may have problems, and therefore, its raw material thing as toothpaste remains further to be studied.
Summary of the invention
The object of the present invention is to provide a kind of alternative grain for industrial uses, reduce product cost, improve corresponding quality product, can replace toothpaste, the existing carrier of makeup in the daily chemical industry field, can be used as the preparation technology of the inorganic mineral colloidal adhesive of spinning sizing agent in the textile industry field.
Technical solution of the present invention can realize according to following mode:
The preparation technology of inorganic mineral colloidal adhesive is characterized in, carries out successively as follows:
1) primary election: get inorganic mineral, removal of contamination carries out primary election;
2) making beating: get weight percentage and be 20～40% inorganic mineral and weight percentage and be 60～80% natural water and carry out mixed pulp, stir, till complete miscibility;
3) selected: with step 2) mixed solution of gained removes impurity, filtration with gravity separation method, and fineness is more than 100 orders;
4) chemical reaction: add Na in the slurries after selected
2CO
3And stir, treat that fully pH value 7.5 ± 0.5 is measured in the reaction back, static depositing 12 hours made colloid.
As a kind of preferred version, inorganic mineral of the present invention can be clay or wilkinite.
Alternative or the alternative a large amount of grain for industrial uses (as compartmentalized box for holding assorted fruits and candies, fruit tray, the cutlery box of spinning sizing agent, papermaking, plastics) of part of inorganic mineral colloidal adhesive involved in the present invention.Average 3000 yuan/ton of industrial modified starch, inorganic mineral colloidal adhesive involved in the present invention, its comprehensive cost of manufacture is 1000 yuan/ton, and it has reduced raw-material cost, and the grain that saves can solve 1～2,000 ten thousand people's problem of food and clothing.In the detergents and cosmetic field, the function that toothpaste, the present used carrier of makeup also do not possess the dirt of dispelling, bleach, clean the teeth, inorganic mineral colloidal adhesive involved in the present invention has been filled up this blank, and contains a large amount of surface active molecules, and good skin care, hair care function are arranged.The content of harmful elements such as Pb, As, Hg is lower than several times to tens times of national standards in the above-mentioned tackiness agent, and therefore, this inorganic mineral colloidal adhesive should belong to green material.
Embodiment
Below in conjunction with embodiment operational path of the present invention is further described.
Embodiment 1:
Be used for detergents and cosmetic, as makeup, the carrier of toothpaste.
The making of inorganic mineral colloidal adhesive (being thickening material, emulsifying agent) is carried out according to following steps:
1) primary election: get the inorganic mineral clay, removal of contamination carries out primary election;
2) making beating: get weight percentage and be 30% inorganic mineral and weight percentage and be 70% natural water and carry out mixed pulp, stirred about 30 minutes, till complete miscibility;
3) selected: with step 2) mixed solution of gained removes impurity, filtration with gravity separation method, and fineness is more than 100 orders;
4) chemical reaction: add Na in the slurries after selected
2CO
3And stir, treat that fully pH value 7.5 is measured in the reaction back, static depositing 12 hours made colloid.
5) preparation in the following manner:
Thickening material: solid content 15%, detailed catalogue are 800, make the main raw material that toothpaste uses.
Emulsifying agent: solid content 10%, detailed catalogue are 1000, make the main raw material that makeup use.
There are a large amount of bioactive molecules, sodium ion in the surface.
Embodiment 2:
Being used for plastics cutlery box, compartmentalized box for holding assorted fruits and candies, fruit tray substitutes the modified starch tackiness agent and makes and pass through the following step successively:
1) primary election: get the inorganic mineral wilkinite, removal of contamination carries out primary election;
2) making beating: get weight percentage and be 30% inorganic mineral and weight percentage and be 70% natural water and carry out mixed pulp, stirred about 30 minutes, till complete miscibility;
3) selected: with step 2) mixed solution of gained removes impurity, filtration with gravity separation method, and fineness is more than 100 orders;
4) chemical reaction: add Na in the slurries after selected
2CO
3And stir, treat that fully pH value 7.5 is measured in the reaction back, static depositing 12 hours made colloid;
5) dehydration, drying: make the inorganic mineral colloidal adhesive become moisture 10% solid;
6) pulverize: the described inorganic mineral colloidal adhesive of step 5 solid siccative is pulverized, its fineness is reached more than 400 orders, be inorganic mineral colloidal adhesive powder;
7) add CO by following part by weight
2Polymkeric substance 20%, vegetable fibre 50%, modified starch 7.5%, inorganic mineral colloidal adhesive powder 22.5% mixes stirring, advances injection moulding machine moulded section.
Inorganic mineral colloidal adhesive powder CO
2Polymkeric substance vegetable fibre modified starch
22.5 20 50 7.5
Embodiment 3:
Being used for spinning sizing agent T/C (65 * 35) 20 * 16 120 * 60 63 " making of the tackiness agent of polyester-cotton blend twill warp sizing (being slurry) is successively through the following step:
1) primary election: get the inorganic mineral wilkinite, removal of contamination carries out primary election;
2) making beating: get weight percentage and be 30% inorganic mineral and weight percentage and be 70% natural water and carry out mixed pulp, stirred about 30 minutes, till complete miscibility;
3) selected: with step 2) mixed solution of gained removes impurity, filtration with gravity separation method, and fineness is more than 100 orders;
4) chemical reaction: add Na in the slurries after selected
2CO
3And stir, treat that fully pH value 7.5 is measured in the reaction back, static depositing 12 hours made colloid;
5) dehydration, drying: make the inorganic mineral colloidal adhesive become moisture 10% solid;
6) superfine grinding reaches 400 orders, becomes inorganic mineral colloidal adhesive powder.
7) be the warp sizing slurry by following weight ratio adding PVA (polyvinyl alcohol), TSF-3 (modified starch), PMA (acrylic acid or the like), inorganic mineral colloidal adhesive, MPN (static inhibitor), glycerine mixing and stirring.
Inorganic mineral colloidal adhesive PVA PMA TSF-3 MPN glycerine
100 50 50 60 1 1
Claims (2)
1, the preparation technology of inorganic mineral colloidal adhesive is characterized in that, carries out successively as follows:
1) primary election: get inorganic mineral, removal of contamination carries out primary election;
2) making beating: get weight percentage and be 20～40% inorganic mineral and weight percentage and be 60～80% natural water and carry out mixed pulp, stir, till complete miscibility;
3) selected: with step 2) mixed solution of gained removes impurity, filtration with gravity separation method, and fineness is more than 100 orders;
4) chemical reaction: add Na in the slurries after selected
2CO
3And stir, treat that fully pH value 7.5 ± 0.5 is measured in the reaction back, static depositing 12 hours made colloid.
2, the preparation technology of inorganic mineral colloidal adhesive according to claim 1 is characterized in that: described inorganic mineral is clay or wilkinite.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2005100480353A CN1982394B (en) | 2005-12-16 | 2005-12-16 | Production of inorganic mineral colloid binder |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2005100480353A CN1982394B (en) | 2005-12-16 | 2005-12-16 | Production of inorganic mineral colloid binder |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1982394A true CN1982394A (en) | 2007-06-20 |
| CN1982394B CN1982394B (en) | 2011-04-20 |
Family
ID=38165250
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2005100480353A Expired - Fee Related CN1982394B (en) | 2005-12-16 | 2005-12-16 | Production of inorganic mineral colloid binder |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN1982394B (en) |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103484027A (en) * | 2013-09-02 | 2014-01-01 | 永仁县磊泰矿业有限公司 | Method for producing bonding agent from illite-smectite interstratified clay |
| CN104804669A (en) * | 2015-05-18 | 2015-07-29 | 金凤善 | Corrugated board mineral adhesive as well as preparation method and application thereof |
| CN104891515A (en) * | 2015-05-28 | 2015-09-09 | 赵连福 | Preparation process of microcrystalline rock crystal thixotropic agent |
| CN106012505A (en) * | 2016-04-06 | 2016-10-12 | 赵连福 | Preparation process of sodium-based bentonite textile pulp |
| CN107652916A (en) * | 2017-10-13 | 2018-02-02 | 陈木镇 | A kind of antibacterial corrugated board mineral rubber and preparation method thereof |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1107762C (en) * | 1997-01-29 | 2003-05-07 | 赵连福 | Prodn. process of sodium-base bentonite textile size |
| CN1094144C (en) * | 1999-12-03 | 2002-11-13 | 清华大学 | Process for preparing bentone adhesive for paper |
| CN1145474C (en) * | 2001-08-07 | 2004-04-14 | 中国科学院广州地球化学研究所 | Process for preparing the clay mineral type antimildew, antibactieral and thicking agent for toothpaste |
-
2005
- 2005-12-16 CN CN2005100480353A patent/CN1982394B/en not_active Expired - Fee Related
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103484027A (en) * | 2013-09-02 | 2014-01-01 | 永仁县磊泰矿业有限公司 | Method for producing bonding agent from illite-smectite interstratified clay |
| CN103484027B (en) * | 2013-09-02 | 2014-09-24 | 永仁县磊泰矿业有限公司 | Method for producing bonding agent from illite-smectite interstratified clay |
| CN104804669A (en) * | 2015-05-18 | 2015-07-29 | 金凤善 | Corrugated board mineral adhesive as well as preparation method and application thereof |
| CN104891515A (en) * | 2015-05-28 | 2015-09-09 | 赵连福 | Preparation process of microcrystalline rock crystal thixotropic agent |
| CN106012505A (en) * | 2016-04-06 | 2016-10-12 | 赵连福 | Preparation process of sodium-based bentonite textile pulp |
| CN107652916A (en) * | 2017-10-13 | 2018-02-02 | 陈木镇 | A kind of antibacterial corrugated board mineral rubber and preparation method thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN1982394B (en) | 2011-04-20 |
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Legal Events
| Date | Code | Title | Description |
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| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| ASS | Succession or assignment of patent right |
Owner name: CHAOYANG ZHENGXIN NEW MATERIAL TECHNOLOGY CO., LTD Free format text: FORMER OWNER: ZHAO LIANFU Effective date: 20150624 |
|
| C41 | Transfer of patent application or patent right or utility model | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20150624 Address after: Zhen Nan wa Cun Jianping 122400 Chaoyang City County in Liaoning province of sand Patentee after: Chaoyang Jungshin new Mstar Technology Ltd Address before: 30 floor 110023, Hongqiao Road, Tiexi District, Liaoning, Shenyang, 242 Patentee before: Zhao Lianfu |
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| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20110420 Termination date: 20201216 |
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| CF01 | Termination of patent right due to non-payment of annual fee |