CN1973664A - Process of producing edible cellulose tablet with red bayberry residue - Google Patents
Process of producing edible cellulose tablet with red bayberry residue Download PDFInfo
- Publication number
- CN1973664A CN1973664A CNA2006101553784A CN200610155378A CN1973664A CN 1973664 A CN1973664 A CN 1973664A CN A2006101553784 A CNA2006101553784 A CN A2006101553784A CN 200610155378 A CN200610155378 A CN 200610155378A CN 1973664 A CN1973664 A CN 1973664A
- Authority
- CN
- China
- Prior art keywords
- cellulose
- myrica ruba
- ruba marc
- filter residue
- red bayberry
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 229920002678 cellulose Polymers 0.000 title claims abstract description 29
- 239000001913 cellulose Substances 0.000 title claims abstract description 29
- 244000132436 Myrica rubra Species 0.000 title claims abstract description 18
- 238000000034 method Methods 0.000 title claims abstract description 14
- 238000001291 vacuum drying Methods 0.000 claims abstract description 5
- 241000219433 Myrica Species 0.000 claims description 30
- 241000709400 Ruba Species 0.000 claims description 30
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 20
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 16
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 16
- 238000001914 filtration Methods 0.000 claims description 12
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims description 10
- 239000002893 slag Substances 0.000 claims description 8
- 238000003756 stirring Methods 0.000 claims description 8
- 238000004061 bleaching Methods 0.000 claims description 4
- 230000003292 diminished effect Effects 0.000 claims description 4
- 238000010828 elution Methods 0.000 claims description 4
- 150000002632 lipids Chemical class 0.000 claims description 4
- 238000010298 pulverizing process Methods 0.000 claims description 4
- 238000007605 air drying Methods 0.000 claims description 3
- 238000004519 manufacturing process Methods 0.000 abstract description 3
- 235000013305 food Nutrition 0.000 description 3
- 238000011161 development Methods 0.000 description 2
- 238000012545 processing Methods 0.000 description 2
- 235000007270 Gaultheria hispida Nutrition 0.000 description 1
- 235000009134 Myrica cerifera Nutrition 0.000 description 1
- 244000269152 Myrica pensylvanica Species 0.000 description 1
- 235000012851 Myrica pensylvanica Nutrition 0.000 description 1
- 235000003283 Pachira macrocarpa Nutrition 0.000 description 1
- 240000001085 Trapa natans Species 0.000 description 1
- 235000014364 Trapa natans Nutrition 0.000 description 1
- 238000013459 approach Methods 0.000 description 1
- 235000013361 beverage Nutrition 0.000 description 1
- 235000015895 biscuits Nutrition 0.000 description 1
- 235000008429 bread Nutrition 0.000 description 1
- 235000012970 cakes Nutrition 0.000 description 1
- 238000001354 calcination Methods 0.000 description 1
- 239000002775 capsule Substances 0.000 description 1
- 150000001720 carbohydrates Chemical class 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 239000002778 food additive Substances 0.000 description 1
- 235000013373 food additive Nutrition 0.000 description 1
- 235000011389 fruit/vegetable juice Nutrition 0.000 description 1
- 235000013402 health food Nutrition 0.000 description 1
- 229910001385 heavy metal Inorganic materials 0.000 description 1
- 238000002386 leaching Methods 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 235000009165 saligot Nutrition 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
Landscapes
- Jellies, Jams, And Syrups (AREA)
- General Preparation And Processing Of Foods (AREA)
- Polysaccharides And Polysaccharide Derivatives (AREA)
Abstract
The present invention relates to process of producing edible cellulose tablet with red bayberry residue. The production process includes the steps of stoving red bayberry residue, crushing, acidifying, decolorizing, defatting, vacuum drying and crushing. The present invention can utilize the red bayberry resource fully and eliminate pollution caused by red bayberry residue.
Description
Technical field
The present invention relates to a kind of method of utilizing producing edible cellulose tablet with red bayberry residue, is to belong to edible cellulose to extract production field.
Technical background
At present, along with the expansion of red bayberry cultivated area, output increases sharply, and can not adapt to the development that red bayberry produces based on the commodity basis of eating raw.For this reason, deep process technology of red bayberry and product have obtained very fast development, as products such as red bayberry inspissated juice, Waxberry beverage and red bayberry fermented wine, well do not utilize approach but really produced a large amount of processing waste pomaces thereupon, let alone contaminated environment.
Summary of the invention
The objective of the invention is to work out a kind of method of producing edible cellulose tablet with red bayberry residue.
The present invention will solve is the utilization of myrica ruba marc discarded object in the red bayberry deep-processing process and prevents problem of environment pollution caused.
The method that myrica ruba marc is produced edible cellulose may further comprise the steps successively:
A. with myrica ruba marc oven dry or air-dry to water content between 5%-10%, pulverized the 20-40 mesh sieve.
B. the myrica ruba marc of pulverizing is immersed in volumn concentration in the hydrochloric acid of 0.0002%-0.0005%, stirring at room 1 hour-3 hours is stayed slag after the filtration.
C. with filter residue by weight 1: 10-1: 20 drop in the water, regulate pH1.5-2.5 with hydrochloric acid, and temperature is controlled at 80 ℃-90 ℃, stirs 2-4 hour.Slag is stayed in filtration.
D. filter residue with 60 ℃-70 ℃ hot-water soak after, water is washed till neutrality with filter residue.Use 4%-6%H
2O
2Decolouring, bleaching temperature is 60 ℃-70 ℃, 2 hours-3 hours action time.Use the filter residue behind the 95% ethanol elution look at last, flush away lipid.Filtration under diminished pressure reclaims ethanol, and the vacuum drying filter residue obtains the myrica ruba marc cellulose that water content is 4%-8%.
E. with the levigate 100-200 mesh sieve of crossing of dried myrica ruba marc cellulose, promptly get the edible cellulose powder.
F. utilize tablet press machine that cellulose powder is pressed into tablet, the every heavily about 0.3-0.6g of cellulose.
The present invention utilizes discarded myrica ruba marc resource production edible cellulose tablet to have characteristics such as cost is low, content of cellulose height.General cellulosic yield is between 25%-50%, according to the difference of red bayberry kind difference to some extent.The cellulose powder that obtains also can be used for food such as cake, bread, biscuit, and the anticaking agent that can the make food again wet goods food that is used to suckle is broad-spectrum food additives, can also directly be bundled into capsule and make health food and sell.
The specific embodiment
The present invention is further illustrated below in conjunction with embodiment:
Embodiment one
The method of the described producing edible cellulose tablet with red bayberry residue of present embodiment may further comprise the steps successively:
A. throatroot kind myrica ruba marc 500 is restrained oven dry or the air-dry water content that arrives between 5%-10%, pulverized the 20-40 mesh sieve.
B. the myrica ruba marc of pulverizing is immersed in volumn concentration in the hydrochloric acid of 0.0002%-0.0005%, stirring at room 1 hour-3 hours is stayed slag after the filtration.
C. with filter residue by weight 1: 10-1: 20 drop in the water, regulate pH1.5-2.5 with hydrochloric acid, and temperature is controlled at 80 ℃-90 ℃, stirs 2-4 hour.Slag is stayed in filtration.
D. filter residue with 60 ℃-70 ℃ hot-water soak after, water is washed till neutrality with filter residue.Use 4%-6%H
2O
2Decolouring, bleaching temperature is 60 ℃-70 ℃, 2 hours-3 hours action time.Use the filter residue behind the 95% ethanol elution look at last, flush away lipid.Filtration under diminished pressure reclaims ethanol, and the vacuum drying filter residue obtains the myrica ruba marc cellulose that water content is 4%-8%.
E. with the levigate 100-200 mesh sieve of crossing of dried myrica ruba marc cellulose, promptly get edible cellulose powder 250g.
F. utilize tablet press machine that cellulose powder is pressed into the tablet of 0.95-1.20*0.55-0.65*0.2-0.25cm, the every heavily about 0.3-0.6g of cellulose.
The bake out temperature of myrica ruba marc is 40 ℃-60 ℃.
The also available natural air drying of the oven dry of myrica ruba marc replaces.
Embodiment two: the method for the described producing edible cellulose tablet with red bayberry residue of present embodiment may further comprise the steps successively:
A. water chestnut kind myrica ruba marc 500 is restrained oven dry or the air-dry water content that arrives between 5%-10%, pulverized the 20-40 mesh sieve.
B. the myrica ruba marc of pulverizing is immersed in volumn concentration in the hydrochloric acid of 0.0002%-0.0005%, stirring at room 1 hour-3 hours is stayed slag after the filtration.
C. with filter residue by weight 1: 10-1: 20 drop in the water, regulate pH1.5-2.5 with hydrochloric acid, and temperature is controlled at 80 ℃-90 ℃, stirs 2-4 hour.Slag is stayed in filtration.
D. filter residue with 60 ℃-70 ℃ hot-water soak after, water is washed till neutrality with filter residue.Use 4%-6%H
2O
2Decolouring, bleaching temperature is 60 ℃-70 ℃, 2 hours-3 hours action time.Use the filter residue behind the 95% ethanol elution look at last, flush away lipid.Filtration under diminished pressure reclaims ethanol, and the vacuum drying filter residue obtains the myrica ruba marc cellulose that water content is 4%-8%.
E. with the levigate 100-200 mesh sieve of crossing of dried myrica ruba marc cellulose, promptly get edible cellulose powder 220g.
F. utilize tablet press machine that cellulose powder is pressed into the tablet of 0.95-1.20*0.55-0.65*0.2-0.25cm, the every heavily about 0.3-0.6g of cellulose.
The bake out temperature of myrica ruba marc is 40 ℃-60 ℃.
The also available natural air drying of the oven dry of myrica ruba marc replaces.
Every index of the myrica ruba marc edible cellulose that obtains among above-mentioned two embodiment is as follows:
The measurement result of myrica ruba marc cellulose powder
| The edible cellulose standard | The myrica ruba marc cellulose | |
| Crude fibre % carbohydrate % heavy metal ppm loss on drying % pH calcination loss % water-soluble substances % | - 97％-102.0％ ≤10 ≤5 5-7 ≤0.05 ≤0.16 | 50％-55％ 97％-99％ 3-5 3-5 6-7 0.02-0.04 0.09-0.15 |
Main innovate point of the present invention is leaching process but not concrete parameter; can carry out parameter adjustment as the case may be in actual applications; as long as can realize that described purpose all should be within protection scope of the present invention, and definitely not limit concrete parameter values of the present invention.
Claims (3)
1. the method for a producing edible cellulose tablet with red bayberry residue, its feature may further comprise the steps successively:
A. with myrica ruba marc oven dry or air-dry to water content between 5%-10%, pulverized the 20-40 mesh sieve;
B. the myrica ruba marc of pulverizing is immersed in volumn concentration in the hydrochloric acid of 0.0002%-0.0005%, stirring at room 1 hour-3 hours is stayed slag after the filtration;
C. with filter residue by weight 1: 10-1: 20 drop in the water, regulate pH1.5-2.5 with hydrochloric acid, and temperature is controlled at 80 ℃-90 ℃, stirs 2-4 hour.Slag is stayed in filtration;
D. filter residue with 60 ℃-70 ℃ hot-water soak after, water is washed till neutrality with filter residue.Use 4%-6%H
2O
2Decolouring, bleaching temperature is 60 ℃-70 ℃, 2 hours-3 hours action time.Use the filter residue behind the 95% ethanol elution look at last, flush away lipid.Filtration under diminished pressure reclaims ethanol, and the vacuum drying filter residue obtains the myrica ruba marc cellulose that water content is 4%-8%;
E. with the levigate 100-200 mesh sieve of crossing of dried myrica ruba marc cellulose, promptly get the edible cellulose powder.
F. utilize tablet press machine that cellulose powder is pressed into tablet, the every heavily about 0.3-0.6g of cellulose.
2. according to claims 1 described method of utilizing myrica ruba marc to produce edible cellulose, the bake out temperature that it is characterized in that myrica ruba marc is 40 ℃-60 ℃.
3. according to the described method of utilizing myrica ruba marc to produce edible cellulose of claims 1, it is characterized in that myrica ruba marc is air-dry and be natural air drying.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN200610155378A CN100589707C (en) | 2006-12-21 | 2006-12-21 | Process of producing edible cellulose tablet with red bayberry residue |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN200610155378A CN100589707C (en) | 2006-12-21 | 2006-12-21 | Process of producing edible cellulose tablet with red bayberry residue |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1973664A true CN1973664A (en) | 2007-06-06 |
| CN100589707C CN100589707C (en) | 2010-02-17 |
Family
ID=38124231
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN200610155378A Expired - Fee Related CN100589707C (en) | 2006-12-21 | 2006-12-21 | Process of producing edible cellulose tablet with red bayberry residue |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN100589707C (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101077182B (en) * | 2007-06-26 | 2011-07-20 | 浙江大学 | Technology for preparing functional dietary fiber through myrica ruba marc enzymolysis |
| CN101744230B (en) * | 2010-01-26 | 2012-05-16 | 浙江扬眉饮品有限公司 | Method for preparing red bayberry dietary fiber powder |
| CN108112665A (en) * | 2016-11-28 | 2018-06-05 | 崇义富百乐发展有限公司 | A kind of production method of red bayberry fiber nut biscuits |
-
2006
- 2006-12-21 CN CN200610155378A patent/CN100589707C/en not_active Expired - Fee Related
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101077182B (en) * | 2007-06-26 | 2011-07-20 | 浙江大学 | Technology for preparing functional dietary fiber through myrica ruba marc enzymolysis |
| CN101744230B (en) * | 2010-01-26 | 2012-05-16 | 浙江扬眉饮品有限公司 | Method for preparing red bayberry dietary fiber powder |
| CN108112665A (en) * | 2016-11-28 | 2018-06-05 | 崇义富百乐发展有限公司 | A kind of production method of red bayberry fiber nut biscuits |
Also Published As
| Publication number | Publication date |
|---|---|
| CN100589707C (en) | 2010-02-17 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| Rouhou et al. | Use of green chemistry methods in the extraction of dietary fibers from cactus rackets (Opuntia ficus indica): Structural and microstructural studies | |
| Kanmani et al. | Extraction and analysis of pectin from citrus peels: augmenting the yield from citrus limon using statistical experimental design | |
| Sabiha-Hanim et al. | Physical properties of hemicellulose films from sugarcane bagasse | |
| Satari et al. | Process optimization for citrus waste biorefinery via simultaneous pectin extraction and pretreatment | |
| CN1923855A (en) | Method of extracting hemicellulose from plant fiber | |
| CN101696245A (en) | Method for preparing octenylsuccinate potato starch ester | |
| CN111560079B (en) | Preparation method of Iota carrageenan glue solution | |
| CN102002875A (en) | Method for preparing microcrystalline cellulose by using carrot pomace | |
| CN1973664A (en) | Process of producing edible cellulose tablet with red bayberry residue | |
| CN101891829A (en) | Acid hydrolysis modified starch and method for preparing same | |
| CN106431068B (en) | A kind of cement retarder and preparation method thereof | |
| CN107058420A (en) | A kind of method that chitin is prepared into chitosan oligosaccharide | |
| CN115058911A (en) | Method for extracting cellulose from cellulose and buckwheat straws | |
| Li et al. | Effect of different processing methods of hawthorn on the properties and emulsification performance of hawthorn pectin | |
| CN103333271A (en) | Method for producing high-quality calcium alginate | |
| CN103435717A (en) | Chitosan oligosaccharide | |
| CN100353867C (en) | Extraction of multifunctional diet fibre from wheat bran | |
| Zhou et al. | Lignin-carbohydrate complexes from coconut (Cocos nucifera) coir: fractionation, structural elucidation, and potential applications | |
| CN104231098A (en) | Method for preparing xylooligosaccharide from bagasse by ethanol/water pretreatment | |
| CN103923225A (en) | Method for preparing citrus pectin | |
| CN1274718C (en) | Production method of sodium carboxy methy starch | |
| CN1098277C (en) | Process for preparing carragheenin | |
| CN1803609A (en) | Method for preparing superfine calcinated talc powder | |
| CN105925640A (en) | Preparation method of yeast beta-glucan | |
| CN109134947A (en) | A kind of degradation plastic layer material of paper plastic bag |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| C17 | Cessation of patent right | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20100217 Termination date: 20131221 |