CN1960648A

CN1960648A - Tobacco compositions

Info

Publication number: CN1960648A
Application number: CN 200480040041
Authority: CN
Inventors: 詹姆斯·A·斯特里克兰; 弗兰克·S·阿奇利; 詹姆斯·M·罗斯曼; 阿曼德·J·德斯马雷斯; 斯科特·A·威廉斯; 托德·J·米勒; 彻恩·W·约翰逊
Original assignee: US Smokeless Tobacco Co LLC
Current assignee: US Smokeless Tobacco Co LLC
Priority date: 2003-11-07
Filing date: 2004-11-05
Publication date: 2007-05-09
Also published as: ZA200604406B

Abstract

The invention features tobacco compositions and methods of their use and manufacture. Compositions of the invention may be based on a variety of technologies. Technologies include films, tabs, shaped parts, gels, consumable units, insoluble matrices, and hollow shapes. In addition to tobacco, compositions may also contain flavors, colors, and other additives as described herein. Compositions may also be orally disintegrable. Exemplary compositions and methods of their manufacture are described herein.

Description

Tobacco compositions

Invention field

The present invention relates to tobacco product (tobacco products) field.

The invention summary

The present invention is characterised in that tobacco compositions and their use and preparation method.Composition of the present invention can be based on kinds of processes.Described technology comprise film, tablet (tab), profiled member, gel, can the unit of consumption (consumable units), insoluble matrix (insoluble matrices) and hollow shape.Except that tobacco, said composition also can comprise as spices described herein, colorant (colors) and other additives.Described composition also can be mouthful disintegration (orally disintegrable).Exemplary composition and their preparation method have been described here.

For example, any composition as described herein can comprise spices or odor masking agent (flavormasking agent).Exemplary spices comprises Radix Glycyrrhizae, kudzu, hydrangea, day raw white skin lily magnolia leaf (Japanese white bark magnolia leaf), yellow chamomile, fenugreek, cloves, menthol, cornmint, Chinese anise, Chinese cassia tree, vanilla (herb), Chinese ilex (winter green), cherry, berry, apple, peach, Dramboui, bourbon's wine (bourbon), Drambuie (scotch), whiskey, spearmint, peppermint (peppermint), lavender, cardamom, celery, the card lamb's-quarters, nutmeg, santal, bergamot, geranium wilfordii (geranium), honey smart (honey essace), attar of rose, vanilla, lemon oil, orange oil, cassia bark, crowndaisy chrysanthemum, cognac wine, jasmine, add and take the pattern tree, Salvia japonica, fennel, allspice (piment), ginger, anise, coriandrum, coffee or from any kind peppermint oil of Mentha.

Any composition of the present invention can comprise that also sweetener is (as sucrose; sucralose; dioxygen _ thiazine kalium; Aspartame; asccharin; cyclohexyl-n-sulfonate; lactose; sucrose; glucose; fructose; D-sorbite and mannitol); surfactant; plasticizer is (as glycerine; propane diols; polyethylene glycol; D-sorbite/mannitol; acetylizad monoglyceride; glyceryl triacetate and 1, the 3-butanediol); filler is (as starch; microcrystalline cellulose; wood pulp; soluble fibre; calcium carbonate; Dicalcium Phosphate; calcium sulfate and clay); lubricant (as stearic acid and stearate) or wax are (as lecithin; glycerin monostearate and propylene glycolmonostearate); anticorrisive agent (as methylparoban and potassium sorbate) and/or stabilizing agent are (as ascorbic acid; citric acid list sterol ester; BHT and BHA).

Any composition described herein can further comprise as unglazed or glossiness coating (coating).Described coating preferably includes colorant, spices, sweetener or odor masking agent.Described coating also can comprise with composition in different spices, colorant or the disintegration rates of form agent (format).Described coating also can comprise tobacco.

Any composition described herein can further comprise as the printed patterns for sign (logo).Printed patterns can comprise colorant, tobacco, spices, sweetener or odor masking agent.The surface of any composition described herein also can comprise embossing pattern (pattern in relief).

The tobacco that is contained in any composition can be powder, particle, fragment or can feel dissolving in mouth.

Any composition described herein can further comprise thin slice, as comprises tobacco or multiple spices or colorant.

Any composition of the present invention may be molded to the shape that is suitable for applying in mouth.Composition of the present invention can further provide tobacco satisfaction (tobacco satisfaction), in during 10-30 minute.

Feature of the present invention also is to be put in the method that obtains the tobacco satisfaction in the mouth by at least a portion with any composition described herein.

Feature of the present invention also is to prepare method for compositions as described herein.In these methods any can further comprise coating is applied on the composition, for example by spraying, brushing, roller coat, scraping blade curtain coating, seam be coated with, squeezing and coating or hot melt deposition.Any method also can be included in printed patterns on the composition, as by offset printing, aniline printing, intaglio printing, ink-jet, laser or serigraphy.In addition, the described method of preparation composition also comprises spices described herein, colorant, odor masking agent or any other composition is joined in described form agent or the composition.

Compile (the compilation of ingredients) as composition in composition that provides here or composition is provided " form agent ", for example is carrier or reagent.

" tobacco " is meant any part among any member of Nicotiana, as leaf, flower, root and stem.The Exemplary types of tobacco comprises that N.rustica and N.tabacum are (as LAB21, LNKY171, TI1406, Basma, Galpao, the Po Like tobacco, Beinhart 1000-1 and Petico), other kinds comprise N.acaulis, N.acuminata, N.acuminata var.multiflona, N.afi icana, N.alata, N.amplexicaulis, N.aretsii, N.attenuata, N.benavidesii, N.benthamiana, N.bigelovii, N.bonariensis, N.cavicola, N.clevelandii, N.cordifolia, N.corymbosa, N.debneyi, N.excelsior, N.forgetiana, N.fragrans, N.glauca, N.glutinosa, N.goodspeedii, N.gossei, N.hybrid, N.ingulba, N.kawakamii, N.knightiana, N.langsdorffii, N.linearis, N.longiflora, N.maritima, N.megalosiphon, N.miersii, N.noctiflora, N.nudicaulis, N.obtusifolia, N.occidentalis, N.occidentalis subsp.hesperis, N.otophora, N.paniculata, N.Pauciflora, N.petunioides, N.plumbaginifolia, N.quadrivalvis, N.raimondii, N.repanda, N.rosulata, N.rosulata subsp.ingulba, N.rotundifolia, N.setchellii, N.simulans, N.solanifolia, N.spegazzinii, N.stocktonii, N.suaveolens, N.sylvestris, N.thyrsiflora, N.tomentosa, N.tomentosiformis, N.trigonophylla, N.umbratica, N.undulata, N.velutina, N.Wigandioides and N.x sanderae.That described tobacco can be is complete, fragment, cut-out, that solidify, aging, fermentation or other processing, as granulation or encapsulated.Tobacco also can be the form agent of finished product, includes but not limited to i.e. (the orally consumed) of mouthful consumption of any tobacco of not firing, as smokeless tobacco.This smokeless tobacco comprises snuff (wet or do), chewing tobacco, loose leaf, capsule cigarette (pouched tobacco) etc., or any form agent that comprises here.This term also comprises the extract of tobacco, and this extract comprises two or more tobacco organoleptic ingredients.

" tobacco satisfaction " in this situation is meant when using smokeless tobacco, component relevant with the tobacco organ sensation that discharges in mouth and the relevant impression of perfume composition that is added.Select to use the adult consumer of smokeless tobacco goods typically to buy the smokeless tobacco goods according to their individual preference, such preference including, but not limited to cutting, the form agent of fragrance, tobacco, be easy to use and pack.

" organ sensation " is meant the comprehensive sensory perception that relates to or help the consumer, and it comprises any combination as fragrance, fragrance, breath, taste, peculiar smell, mouthfeel etc.

" do not fire " and be meant and usually do not burning between the operating period.

From size, be easy to use and the viewpoint of controlled disintegration rate (rate of disintegration), composition described herein is favourable.

Except as otherwise noted, all percentages are percentage by weights.

From following description and claim, other characteristics and advantage are conspicuous.

Detailed Description Of The Invention

The present invention is characterised in that the tobacco compositions that can typical be used for the tobacco satisfaction.

A. tobacco

The tobacco that is used for composition described herein comprises any raw material or form processing agent, as powder, particle or fragment.Preferably, tobacco is of a size of or it is made in mouth can disintegration (as dissolving), with the perception that provides solubility (as, described tobacco does not produce touch feeling in mouth), perhaps easy-to-swallow.Perhaps, described tobacco is of a size of or it is made can provide sense of touch in mouth.Exemplary average-size for example is about 800,500,250,100,80,75,50,25,20,15,10,8,6,5,3,2 or 1 μ m or littler in the 1-1000 mu m range, is preferably less than 80 μ m or littler.But described tobacco also can be the form agent of slurries or flow-gel.But flow-gel is the mixture of form agent, and this form agent is water-soluble and mix with tobacco, and mixes with miscible solvent then to prevent the dissolving fully of described form agent.Such mixture causes described form solvent swell to form the pseudoplastic behavior paste of thickness, and is easy under low pressure that (slight pressure) distributes (dispense) from container (as conduit).Exemplary tobacco is a smokeless tobacco.Other tobaccos are described in U.S. open Nos.2003/0094182 and 2003/0070687, U.S.S.N.60/603 and in the U.S.S.N.__ title of submitting on November 5th, 2004 " Nicotiana composition ", its disclosure is incorporated into to come in by reference.Also can be used for the tobacco of described composition according to the method preparation among the open No.2004/0112394 of U.S., its disclosure is incorporated into to come in by being introduced in.Other suitable tobaccos are known in the art.

Can or spread all over equably in composition the tobacco Random assignment, perhaps focus in its zones of different, for example in central authorities or from the teeth outwards.

The final use that depends on desired characteristic and described composition, typical final tobacco concentration range is the 1%-99% weight of final composition, for example, mostly be 10,15,20,25,30,35,40,45,50,55,60,65,70,75,80,85 or 90% most.In a preferred embodiment, described composition comprises about 25% tobacco.

B. composition

Normally, composition of the present invention is intended for mouthful use or consumption.Can use any suitable compatible form agent of mouth to prepare the composition that comprises tobacco.Described tobacco can directly mix with described form agent or by described form agent load.For example, composition can comprise be deposited in the form agent, be mixed in the form agent, by the form agent around or the tobacco that combines with the form agent, described tobacco as as dry particles, fragment, particle, powder or slurries.Tobacco in the composition is soluble or insoluble or feels soluble (perceived to be soluble).In one embodiment, described composition is (spitless) tobacco compositions that does not spue.Composition also can comprise the mixture of agent of tobacco form or type.Composition can be foam-like or densification.The foam-like composition can be rigidity or soft, and can be based on water-soluble, water-insoluble or thermoplasticity form agent.Exemplary composition has been described here.In one embodiment, composition of the present invention does not fire.

The form agent that is applicable to composition described here comprises a mouthful compatible polymeric, as cellulose (as carboxymethyl cellulose (CMC), hydroxypropyl cellulose (HPC), hydroxyethylcellulose (HEC), hydroxypropyl methylcellulose (HPMC) and methylcellulose (MC)), natural polymer is (as starch and modified starch, konjac, collagen, inulin, soybean protein, lactalbumin, casein and wheat gluten (wheatgluten)), the marine alga derived polymer is (as carrageenan (κ, ι and λ), alginates and propylene glycol alginate), the microorganism derived polymer is (as xanthans, dextran, the Aureobasidium pullulans glycan, curdled milk glycan and exocellular polysaccharide), extract is (as locust bean gum, guar gum, tara gum, gum tragacanth, pectin (lo methoxyl group (lo methoxy) and amidated), agar, zein, the thorn Chinese parasol tree, gelatin, Asiatic plantain kind (psyllium seed), chitin and chitosan), secretion (as gum arabic (Arabic gum) and shellac), synthetic polymer is (as PVP, PEO and polyvinyl alcohol).Other useful form agent known in the prior art, for example see the Food Technology of Krochta etc., 1997,51:61-74, Glicksman Food Hydrocolloids CRC 1982, Krochta EdibleCoatings and Films to Improve Food Quality Technomic 1994, Industrial GumsAcademic 1993, Nussinovitch Water-Soluble Polymer Applications in FoodsBlackwell Science 2003.Depend on desired characteristic; composition can comprise that also filler is (as starch; microcrystalline cellulose; wood pulp is (as available from International Fibers; Inc. Solkafloc); Soluble Fiber (as Fibersol) available from Matsushita; calcium carbonate; Dicalcium Phosphate; calcium sulfate and clay); lubricant is (as lecithin; stearic acid; stearate (as Mg or K) and wax are (as glycerin monostearate; propylene glycolmonostearate and acetylizad monoglyceride)); plasticizer is (as glycerine; propane diols; polyethylene glycol; D-sorbite; mannitol; glyceryl triacetate and 1; the 3-butanediol); stabilizing agent is (as ascorbic acid and citric acid list sterol ester; BHT or BHA), or other compounds are (as vegetable oil; surfactant and anticorrisive agent).Some compounds work as plasticizer and lubricant simultaneously.

Composition of the present invention can comprise that spice extract is (as Radix Glycyrrhizae, kudzu, hydrangea, day raw white skin lily magnolia leaf, yellow chamomile, fenugreek, cloves, menthol, cornmint, Chinese anise, Chinese cassia tree, vanilla (herb), Chinese ilex (winter green), cherry, berry, peach, apple, Dramboui, bourbon's wine (bourbon), Drambuie (scotch), whiskey, spearmint, peppermint (peppermint), lavender, cardamom, celery, the card lamb's-quarters, nutmeg, santal, bergamot, geranium wilfordii (geranium), honey smart (honey essace), attar of rose, lemon oil, vanilla, orange oil, cassia bark, crowndaisy chrysanthemum, cognac wine, jasmine, add and take the pattern tree, Salvia japonica, fennel, allspice (piment), ginger, anise, coriandrum, coffee or from any kind peppermint oil of Mentha), odor masking agent, bitter taste receptor site blocking agent (bitterness receptor blocker), the receptor site reinforcing agent, sweetener is (as sucralose, dioxygen _ thiazine kalium (Ace-K), Aspartame, asccharin, cyclohexyl-n-sulfonate, lactose, sucrose, glucose, fructose, D-sorbite and mannitol), and other desired additive such as chlorophyll, mineral matter, medicinal material or breathe fresh dose (breath freshening agents).

Also can provide spices by plant material such as dried peppermint leaf, it typically is 10% perfumery oil (flavoroil) and 90% insoluble fiber.Exemplary plant further comprises Radix Glycyrrhizae, kudzu, hydrangea, day raw white trees orchid, yellow chamomile, fenugreek, cloves, cornmint, Chinese cassia tree, vanilla (herb), cherry, berry, peach, apple, lavender, celery, cardamom, the card lamb's-quarters, nutmeg, santal, geranium wilfordii, bergamot, rose, vanilla, lemon, orange, cassia bark, crowndaisy chrysanthemum, jasmine, add and take the pattern tree, Salvia japonica, fennel, allspice (piment), ginger, anise, coriandrum, coffee or Mentha any kind.

Also can provide spices to composition described herein by the composition of spice extract, plant material or its combination.Except that the natural perfume material extract, also can provide spices by Counterfeit Item, synthetic or artificial perfume composition and the admixture that comprises these compositions.Can powder, oil or capsule form agent add spices.

In specific implementations, the disintegration in mouth of described composition.The disintegration rate of composition can 60 minutes-change between less than 1 minute.Fast release composition typically less than 2 minutes and most preferably 1 minute or shorter as less than 60 seconds, 50 seconds, 45 seconds, 40 seconds, 35 seconds, 30 seconds, 25 seconds, 20 seconds, 15 seconds, 10 seconds, 5 seconds, 4 seconds, 3 seconds, 2 seconds or 1 second in disintegration takes place.Described disintegration can any mechanism take place, as dissolving, fusing, mechanical damage (as from chewing), enzyme or other chemical degradations, or interactional the breaking between described form agent and tobacco.Disintegration also can take place in described form agent or tobacco itself equally.The required time of composition generation disintegration can be controlled by the thickness that changes described composition, and depends on type, other additives and the use pattern of described form agent.When putting into mouth, described composition can temporarily adhere on the oral mucosal part.In addition, can change the duration of tobacco satisfaction.This duration is subjected to the disintegration rate of composition for example, from the extraction rate and the influence of the time of staying of described composition in mouth of the organoleptic ingredients of composition.Can be preferably 10 seconds-10 minutes and described tobacco satisfaction more preferably was provided at 30 seconds-5 minutes at least 10 seconds, 30 seconds, 45 seconds, 1 minute, 2 minutes, 3 minutes, 5 minutes, 10 minutes, 15 minutes, 30 minutes or 1 hour equal time.

In other embodiments, not disintegration in delay period in mouth of described composition.In said composition, can the tobacco organoleptic ingredients be incorporated in the mouth by dissolving, leaching (leaching), extraction or by chewing the mechanical damage that causes.

The size of single composition (individual composition) can be and is fit to fully in mouth, or size be only suitable partly in mouth.The preferred cross-sections of described composition includes but not limited to square, circle, rectangle, ellipse, avette etc.Depend on supply size and composition, can change preferred size.Typically, the full-size of single part of supplies (single serving) is for being equal to or less than 5cm.Perhaps, tobacco product can be made bigger form, from this bigger form, can cut or separate single supplies, as by chewing, gnaw or a mouthful disintegration being carried out.For example, can be put in rectangular or other lengthy motion pictures in the container and the consumer can take out desired supply size.Also the bigger composition sheet of the mouth size on the handle (handle) (or adhere to) part can be inserted in the mouth, be similar to toothpick or cigarette, and the consumer can suck or chews it.In one embodiment, described bigger sheet be good to eat disintegration and over a period to come full consumption fall.

C. technology

Film. composition of the present invention can form the film of energy mouthful disintegration.This film can comprise single or multiple lift.Monofilm for example can comprise tobacco, form agent and other compositions in homogeneous mixture.Multilayer film can comprise the multilayer that contains tobacco, and for example the kind of tobacco is measure-alike or different, as the tobacco of discernable dissolving.Can be together with laminated multi-layer.In addition, as described here, multilayer film can one or more layers neutralization comprise other compositions the layer in comprise tobacco.For example, can add each layer for fragrance, sweet taste, color, disintegration rate or stability (as during handling or during the consumption).Also can be arranged in two-layer with the agent of interlayer arrangement form tobacco or multilayer between.In interlayer one or more layers also can comprise tobacco.In having the film of multilayer, the speed generation disintegration that described layer can be identical or different, or a mouthful disintegration does not take place in layer.When disintegration rate not simultaneously, based on the disintegration of described layer, described composition can provide tobacco at different times.Monofilm or the single layer in multilayer film can foam or inflate so that desired physical characteristic or desired dissolving or disintegration rate to be provided.

The big I of film is fit to mouthful with as single supplies (serving).Perhaps, can make bigger film, therefrom divisible single supplies.For example, film can be wrapped up (wraped) or otherwise moulding is forming hollow tube or suction pipe (straw), it can and then be filled with other materials.In addition, as described here, but preparation example and is used to be used for add the preparation of the thin slice or the powder of other compositions then as comprising the film of high percentage 1%-99% tobacco based on dry weight.The preferred thickness of film typically is less than 1mm, for example less than 500,200,100,50,40,30,20,10,5,4,3,2 or 1 μ m; Be preferably 5-125 μ m.

Can use several different methods well known in the prior art to prepare film.Employed technology can be depending on the form agent of using in film.Illustrative methods comprise solution casting or extrude, melt extrude, drum dried and calendering (calendaring).In case form, the surface that for example can use printing or other coatings or modify described film is come film is carried out modification.Can or decorate to handle by printing, coating spices, colorant or tobacco are joined on the surface of film.Can use all print processes well known in the prior art, as offset printing, aniline printing, intaglio printing, ink-jet, laser, serigraphy and other typical methods.Can use the known method of prior art, as spraying, brushing, roller coat, scraping blade curtain coating, seam be coated with, squeezing and coating, hot melt deposition, deposited particles or thin slice and other typical methods coating or decorative pattern are applied to as described on the surface of film.The described film that is printed, applies or modify can comprise or not comprise tobacco.A function of described printing, coating or decorative pattern is that colorant, spices or the tobacco with additional amount is provided on the described film.Another function is to improve the dimensional stability and the outward appearance of described film.In case prepared the described film that is printed, applies or decorate, the extra play that can apply film is to cover, to protect and seal the described surface that is printed, applies or decorate.

Film embodiment

Following table has shown the exemplary composition that is used to prepare film of the present invention.

Table A 1

	Exemplary (%)	Preferably (%)	Embodiment A (%)
	Exemplary (%)	Preferably (%)	Embodiment A (%)	Water-soluble polymer	10-70	20-45	30
Tobacco	1-90	20-40	25	Water-soluble polymer	10-70	20-45	30
Tobacco	1-90	20-40	25	Spices	1-40	5-15	10
Sweetener	0.2-6	2-5	3	Spices	1-40	5-15	10
Sweetener	0.2-6	2-5	3	Fiber (solvable or insoluble)	2-40	5-20	9
Plasticizer	1-40	5-15	10	Fiber (solvable or insoluble)	2-40	5-20	9
Plasticizer	1-40	5-15	10	Surfactant	0.05-5	01-1	0.5
Starch/maltodextrin	1-40	10-20	10.5	Surfactant	0.05-5	01-1	0.5
Starch/maltodextrin	1-40	10-20	10.5	Lubricant	0.5-10	1-3	2

Embodiment B. the tobacco film

To join in the beaker that comprises the well-beaten deionized water of 450g available from the 50g mixture of the hydroxypropyl methylcellulose (HPMC) of K-3 (60%), the K-100 (35%) of Dow Chemical and K4M (5%) level, this deionized water has been heated to 180_.When mixing, the tobacco of 40g fine grinding is joined in the described HPMC solution with 15g microcrystalline cellulose (FMC), 17g starch (available from the B-700 of Grain Processing Corp.), 16g glycerine, 0.8g Tween 80 (Unichema) and 4g propylene glycolmonostearate (available from the PGMS of Danisco).When temperature is reduced to when being lower than 100_, in described solution, add 10g cinnamon flavor and 2g sucralose (artificial sweetener).Add 2g sodium carbonate to regulate pH to about 7.5.In case add all the components and evenly dispersion, described mixture is put in the water-bath and continues stirred 30 minutes, temperature is reduced to 65_.Add make-up water as required to obtain the brookfield viscosity of 5,000 centipoises when temperature is 65_.

It is that the spreader of filming of 15 Mills (0.015 inch) is applied to the above-mentioned tobacco section solution that comprises on the glass plate that use has fixing slit.Described glass plate is placed on temperature and is set in the air circulation test baking oven of 170_.After 30 minutes, from baking oven, take out glass plate, cool to room temperature, and from glass plate, take off and have the described desciccator diaphragm that thickness is 2.5 Mills (0.0025 inch).This film is cut into the less sheet that is fit to be put in the mouth.In less than 1 minute, 1.0 inches * 1.25 inches part disintegrations in mouth of described film, thus discharge described spices, sweetener and tobacco.Based on dry weight, the tobacco content of this film is 25%.

Embodiment C. opaque perfuming film

Use same procedure, made the solution that does not add tobacco as Embodiment B.When described solution is still warm, under agitation add the 32g titanium dioxide dispersion (50% titanium dioxide in water) and the 0.01g FD ﹠amp of Sensient Colors supply; C Red No.40 color lake (Sensient Colors).As the description in the Embodiment B, described solution is cooled to 65_ and be applied on the glass plate, dry and remove from described glass plate.Made and had good strength and build is the opaque light red film of 1.5 Mills (0.015 inch).

Embodiment D. duplicature

It is that the spreader of filming of 15 Mills (0.015 inch) will be applied on the glass plate from the part solution of Embodiment B that use has fixing slit.As in the Embodiment B with as described in glass plate be positioned in the test baking oven and dry.From baking oven, take out described glass plate and cool to room temperature, but do not remove described film from described glass plate.

It is that the spreader of filming of 5 Mills (0.005 inch) will be applied on the desciccator diaphragm of Embodiment B from the part solution of Embodiment C that use has fixing slit.Described glass plate was positioned in the test baking oven of 170_ 10 minutes.From described glass plate, take off and have the desciccator diaphragm that thickness is 3 Mills (0.003 inch).Described film clearly has both sides, is that the film that comprises tobacco of brown and an opposite side are red perfuming film in a side.1.0 inches * 1.25 inches parts of described film can typically disintegration in mouth in less than 1 minute.

Embodiment E. trilamellar membrane

As described above, use that to have fixing slit be that the spreader of filming of 5 Mills will be applied on the glass plate from the part solution of Embodiment C, and in the test baking oven, carry out drying.It is that the spreader of filming of 15 Mills will be applied on the described desciccator diaphragm of Embodiment C from the part solution of Embodiment B that use has fixing slit, and carries out drying as in the previous in the test baking oven.It is that the spreader of filming of 5 Mills is applied on the glass plate from the part solution of Embodiment C and carries out drying as in the previous in the test baking oven that use has fixing slit.The thickness of gained film is 3 Mills (0.003 inch) and forms by three layers, is opaque, red flavour additive laye and the intermediate layer that comprises the tobacco film at either side.1.0 inches * 1.25 inches parts of described film can typically disintegration in mouth in less than 1 minute.

Embodiment F. the film of foamed

Under vigorous stirring, comprise to 100g and to add 0.5g lauryl sodium sulfate (surfactant) in the part solution of tobacco from Embodiment B.Then this solution is mixed in high speed shear blender such as Silverson Laboratory Homogenizer, Model L4RT-W, to produce uniform bubble structure.Use then that to have fixing slit be that the spreader of filming of 4 Mills (0.040 inch) is applied to this hyperinflation solution on the glass plate, and dry in the test baking oven.When with the foam film of drying when described glass plate is removed, it has thickness is 4 Mills (0.004 inches).1.0 the weight of the same slice of the non-foam film that makes in the weight ratio Embodiment B of this foam film section of inch * 1.25 inches * 4 Mills (0.004 inch) (thickness) is little by 35%.Compare with the identical non-foamization film for preparing in the Embodiment B, the disintegration rate of described foamed film in mouth is typically faster.

Embodiment G. thin slice

By (TIC Gums Inc.) joins in the 60g deionized water with 0.4g propylene glycolmonostearate (PGMS), violent simultaneously the mixing 30 minutes, has made solution in beaker with the spray-dired gum arabic of 40g.In high-speed stirred, in this solution of 10g, add 0.01g FD; C RedNo.40 color lake is to guarantee the even dispersion of described color.This solution of capping was also placed 24 hours so that the whole dissipations of all air pockets.Use then that to have fixing slit be that the spreader of filming of 5 Mills (0.005 inch) is applied to the part of this solution on the glass plate.Described glass plate was put in the test baking oven that is set at 170_ 20 minutes, fully dry up to described film.When with described film when described glass plate is removed, its be broken into have high glaze, a plurality of fritters of bright-coloured red thin slice.With other FD ﹠amp; C repeats in the color lake this process to make the thin slice of a plurality of different colours.Also spices and artificial sweetening agent can be joined in the described thin slice.

Embodiment H. reconstituted tobacoo

The tobacco powder that in the solution that 10g embodiment G makes, adds the 4g fine grinding.As the same procedure among the embodiment G, on glass plate, make film and drying, cool off and remove.The gained thin slice is made up of the gum arabic of 50% tobacco and 50% and is had a dark brown color.If desired, spices can be joined in the described thin slice.As described in also the material as sodium carbonate can being joined in the thin slice to regulate pH.

Example I. have the tobacco film of thin slice

Made film as Embodiment B.When described film remains unchanged on described glass plate when moistening, prepared the thin slice of measured quantity and it has evenly been applied and opened up on the described wet film.Then that described glass plate is dry in the test baking oven; Described film cool to room temperature is also removed from glass plate then.Typically, to have dry weight be 1g (comprise 25% or 0.25g tobacco) to the described dry film of Embodiment B.If the 20 equal portions films that this film is divided into sections (1.0 inches * 1.25 inches * 2 Mill), each section heavily are 50mg (comprise 25% or the tobacco of 12.5mg).If 1g reconstituted tobacoo (it is the 50 weight % of tobacco) evenly applied open up on the described film, it is 2g (comprising the 0.75g tobacco altogether) that whole of described film will have dry weight.When being divided into equal section in 20 fens, each section is heavily for 100mg and comprise the tobacco of 37.5mg.The described film section of being cut into 1.0 inches * 1.25 inches can typically disintegration in mouth in less than 1 minute.

Embodiment J. has the tobacco film of decorative laminate

Can use decorative laminate (as not comprising coloured thin slice of any tobacco) or coloured thin slice mixed with the thin slice that comprises tobacco and repeat to list in method in the example I.The film of gained has bright-coloured outward appearance.

Embodiment K. perfuming tobacco film

Table K1

HPMC	36.56％
HPMC	36.56％	Starch	12.18％
Tobacco	24.37％	Starch	12.18％
Tobacco	24.37％	Na ₂CO ₃	1.46％
Plasticizer	13.15％	Na ₂CO ₃	1.46％
Plasticizer	13.15％	Spices	6.82％
Sweetener	0.49％	Spices	6.82％
Sweetener	0.49％	Surfactant	0.97％
Water	4.00％	Surfactant	0.97％

Weighing and in conjunction with following composition in the container of suitable volumes:

MIX1

HM3PA2910(Wolff Cellulosics) 30.98g

HM100PA2208(Wolff Cellulosics) 15.51g

HM4000PA2910(Wolff Cellulosics) 2.60g

B700(Grain Processing Corporation) 16.36g

Tobacco powder (particle mean size＜80 μ m) 32.72g

The gained mixture is mixed until evenly.Composition in separation container below the weighing:

MIX2

Na ₂CO ₃ 1.96g

Propylene glycolmonostearate 0.65g

Lauryl sodium sulfate 0.65g

In the 3rd container, the composition below the weighing:

MIX3

Glycerine 5.89g

Propane diols 5.22g

PEG400 6.54g

Cinnamon flavor 6.54g

Tobacco spice modifier (Hagelin) 2.62g

Sucralose solution 25% (Tate ﹠amp; Lyle) 2.62g

The weighing boiling water of 619.14g altogether in rustless steel container.Described water is carried out vigorous stirring with Arrow Model1750 high speed shear blender.Xiang Shuizhong adds MIX2.Continue to stir 30 seconds, add MIX1.Continued vigorous stirring 4 minutes.In gained solution, add MIX3.Continued vigorous stirring 1 minute.Gained solution is transferred in the Silverson SS1 container that is suitable for the vacuum mixing.Described container is connected to Silverson L4RTU homogenizer electrodynamic element.(under the 20-25 inch Hg) with described solution homogenizing 2 minutes, places ice bath around described homogeneous container then under 7500RPM under vacuum.Under vacuum (20-25 inch Hg) in 10,000RPM continued homogenization 8 minutes.After homogenization is finished, the described solution of part is transferred to the 500mL Nalgene bottle that is used for storing.

The part of gained gel solution is poured in advance on the glass plate that the Mylar sheet with suitable size covers.Is that the spreader of filming of 15 Mills laterally dragged glass plate with described gel solution with having fixing slit.Described glass plate is positioned over the side that is set at 75 ℃ to purge in the forced ventilation baking oven (VWR type 1330FM) 30 minutes.The gained film that is dried to about 4% humidity is removed and is cut into the unit of suitable size from described Mylar sheet.1.0 inch * film unit's disintegration in mouth in of 1.25 inches less than 30 seconds.

From identical solution, having fixing slit by use is that the spreader of filming of 30 Mills crosses the film that (cross) glass plate made relatively slow disintegration (for example in mouth disintegration greater than 30 seconds film) with described solution casting.As above dry in an identical manner described film 40 minutes.Typically disintegration in mouth in less than 1 minute of the described film that makes.

Curtain coating is before the glass plate from same solution, described solution is carried out foamed and made supper-fast disintegration film (for example in mouth disintegration less than 15 seconds film).Carry out high speed shear by every kind of solution and mix (using Arrow Model 1750 high speed shear blenders) and finished foamed in about 3 minutes 100g, then with have fixing slit be 30 Mills film spreader with described foaming solution immediately curtain coating to glass plate.Typically disintegration in mouth in less than 15 seconds of the described film that makes.

The tobacco film of embodiment L. perfuming

Table L1

HPMC	36.56％
HPMC	36.56％	Starch	12.18％
Tobacco	24.37％	Starch	12.18％
Tobacco	24.37％	Na ₂CO ₃	1.46％
Plasticizer	10.71％	Na ₂CO ₃	1.46％
Plasticizer	10.71％	Spices	9.26％
Sweetener	0.49％	Spices	9.26％
Sweetener	0.49％	Surfactant	0.97％
Water	4.00％	Surfactant	0.97％

MIX1

HM3PA2910(Wolff Cellulosics) 30.98g

HM100PA2208(Wolff Cellulosics) 15.51g

HM4000PA2910(Wolff Cellulosics) 2.60g

B700(Grain Processing Corporation) 16.36g

Tobacco powder (particle mean size＜80 μ m) 32.72g

MIX2

Na ₂CO ₃ 1.96g

Propylene glycolmonostearate 0.65g

Lauryl sodium sulfate 0.65g

In the 3rd container, the composition below the weighing:

MIX3

Glycerine 4.58g

Propane diols 5.22g

PEG400 4.58g

Mint flavouring 9.81g

Tobacco spice modifier (Hagelin) 2.62g

Sucralose solution 25% (Tate ﹠amp; Lyle) 2.62g

The weighing boiling water of 619.14g altogether in rustless steel container.Described water is carried out vigorous stirring with Arrow Model1750 high speed shear blender.Xiang Shuizhong adds MIX2.Continue to stir 30 seconds, add MIX1.Continued vigorous stirring 4 minutes.In gained solution, add MIX3.Continued vigorous stirring 1 minute.Gained solution is transferred in the Silverson SS1 container that is suitable for the vacuum mixing.Described container is connected to Silverson L4RTU homogenizer electrodynamic element.(under the 20-25 inch Hg) with described solution homogenizing 2 minutes, places ice bath around described homogeneous container then under 7500RPM under vacuum.Under vacuum (20-25 inch Hg) in 10, lasting homogenization is 8 minutes under the 000RPM.After homogenization is finished, the described solution of part is transferred to the 500mL Nalgene bottle that is used for storing.

The part of gained gel solution is poured in advance on the glass plate that the Mylar sheet with suitable size covers.Is that the spreader of filming of 15 Mills laterally dragged glass plate with described gel solution with having fixing slit.Described glass plate is positioned over the side that is set at 75 ℃ to purge in the forced ventilation baking oven (VWR type 1330FM) 30 minutes.The gained film that is dried to about 4% humidity is removed and is cut into the unit of suitable size from described Mylar sheet.1.0 the film of inch * 1.25 inches unit is in 15-30 disintegration in mouth in second.

Perhaps, described film comprises Chinese ilex, spearmint or apple spice.

The film (as the film of disintegration in mouth) and the supper-fast disintegration film (as the film of disintegration in mouth) of relatively slow disintegration described in embodiment K, from same solution, have been made less than 15 seconds greater than 30 seconds.

Embodiment M. peach perfuming tobacco film

Table M1

HPMC	29.12％
HPMC	29.12％	Starch	9.71％
Tobacco	19.41％	Starch	9.71％
Tobacco	19.41％	Na ₂CO ₃	1.16％
Plasticizer	2.33％	Na ₂CO ₃	1.16％
Plasticizer	2.33％	Peach mud	29.66％
Spices	3.43％	Peach mud	29.66％
Spices	3.43％	Sweetener	0.39％
Surfactant	0.77％	Sweetener	0.39％
Surfactant	0.77％	Water	4.00％

MIX1

HM3PA2910(Wolff Cellulosics) 30.98g

HM100PA2208(Wolff Cellulosics) 15.51g

HM4000PA2910(Wolff Cellulosics) 2.60g

B700(Grain Processing Corporation) 16.36g

Tobacco powder (particle mean size＜80 μ m) 32.72g

MIX2

Na ₂CO ₃ 1.96g

Propylene glycolmonostearate 0.65g

Lauryl sodium sulfate 0.65g

In the 3rd container, the composition below the weighing:

MIX3

Glycerine 1.31g

Propane diols 1.31g

PEG400 1.31g

Peach mud 100.0g

Flavoring peach essence (peach flavor) 3.27g

Tobacco spice modifier (Hagelin) 2.62g

Sucralose solution 25% (Tate ﹠amp; Lyle) 2.62g

Embodiment N. is used for the perfuming tobacco film of rod/package/bag shape/vacuum forming

Table N1

HPMC	41.31％
HPMC	41.31％	Starch	13.76％
Tobacco	9.75％	Starch	13.76％
Tobacco	9.75％	Na ₂CO ₃	1.46％

Plasticizer	18.99％
Plasticizer	18.99％	Spices	9.27％
Sweetener	0.49％	Spices	9.27％
Sweetener	0.49％	Surfactant	0.98％
Water	4.00％	Surfactant	0.98％

MIX1

HM3PA2910(Wolff Cellulosics) 38.48g

HM100PA2208(Wolff Cellulosics) 19.27g

HM4000PA2910(Wolff Cellulosics) 3.24g

B700(Grain Processing Corporation) 20.32g

Tobacco powder (particle mean size＜80 μ m) 14.39g

MIX2

Na ₂CO ₃ 2.16g

Propylene glycolmonostearate 0.72g

Lauryl sodium sulfate 0.72g

In the 3rd container, the composition below the weighing:

MIX3

Glycerine 7.19g

Propane diols 7.19g

PEG400 7.19g

Glyceryl triacetate 6.47g

Cinnamon flavor 10.80g

Tobacco spice modifier (Hagelin) 2.88g

Sucralose solution 25% (Tate ﹠amp; Lyle) 2.88g

The weighing boiling water of 606.10g altogether in rustless steel container.Described water is carried out vigorous stirring with Arrow Model1750 high speed shear blender.Xiang Shuizhong adds MIX2.Continue to stir 30 seconds, add MIX1.Continued vigorous stirring 4 minutes.In gained solution, add MIX3.Continued vigorous stirring 1 minute.Gained solution is transferred in the Silverson SS1 container that is suitable for the vacuum mixing.Described container is connected to Silverson L4RTU homogenizer electrodynamic element.(under the 20-25 inch Hg) with described solution homogenizing 2 minutes, places ice bath around described homogeneous container then under 7500RPM under vacuum.Under vacuum (20-25 inch Hg) in 10, lasting homogenization is 8 minutes under the 000RPM.After homogenization is finished, the described solution of part is transferred to the 500mL Nalgene bottle that is used for storing.

The part of gained gel solution is poured in advance on the glass plate that the Mylar sheet with suitable size covers.Is that the spreader of filming of 20 Mills laterally dragged (drawn cross) glass plate with described gel solution with having fixing slit.Described glass plate is positioned over the side that is set at 75 ℃ to purge in the forced ventilation baking oven (VWR type 1330FM) 35 minutes.The gained film that is dried to about 4% humidity removed and be stored in from described Mylar sheet use after being used for the polybag.

The perfuming tobacco film that has made other according to the prescription and the method for front is as the apple perfuming.

Embodiment O. is used for perfuming/coloured tobacco film of rod/package/bag shape

Table O1

HPMC	41.31％
HPMC	41.31％	Starch	13.76％
Fibersol-2	9.75％	Starch	13.76％
Fibersol-2	9.75％	Na ₂CO ₃	1.46％
Plasticizer	18.99％	Na ₂CO ₃	1.46％
Plasticizer	18.99％	Spices	9.26％
Sweetener	0.49％	Spices	9.26％
Sweetener	0.49％	Surfactant	0.79％
Colorant	0.20％	Surfactant	0.79％
Colorant	0.20％	Water	4.00％

MIX1

HM3PA2910(Wolff Cellulosics) 38.48g

HM100PA2208(Wolff Cellulosics) 19.27g

HM4000PA2910(Wolff Cellulosics) 3.24g

B700(Grain Processing Corporation) 20.32g

Fibersol-2(Matsutani) 14.39g

FD & C Red No.40Alum Lake35-42％ 0.29g

(Sensient Colors)

MIX2

Na ₂CO ₃ 2.16g

Propylene glycolmonostearate 0.58g

Lauryl sodium sulfate 0.58g

In the 3rd container, the composition below the weighing:

MIX3

Glycerine 7.19g

Propane diols 7.19g

PEG400 7.19g

Glyceryl triacetate 6.47g

Cinnamon flavor 10.79g

Tobacco spice modifier (Hagelin) 2.88g

Sucralose solution 25% (Tate ﹠amp; Lyle) 2.88g

The weighing boiling water of 606.10g altogether in rustless steel container.Described water is carried out vigorous stirring with Arrow Model1750 high speed shear blender.Xiang Shuizhong adds MIX2.Continue to stir 30 seconds, add MIX1.Continued vigorous stirring 4 minutes.In gained solution, add MIX3.Continued vigorous stirring 1 minute.Gained solution is transferred in the Silverson SS1 container that is suitable for the vacuum mixing.Described container is connected to Silverson L4RTU homogenizer electrodynamic element.(under the 20-25 inch) with described solution homogenizing 2 minutes, places ice bath around described homogeneous container then under 7500RPM under vacuum.Under vacuum (20-25 inch) in 10, lasting homogenization is 8 minutes under the 000RPM.After homogenization is finished, the described solution of part is transferred to the 500mL Nalgene bottle that is used for storing.

The part of gained gel solution is poured in advance on the glass plate that the Mylar sheet with suitable size covers.Is that the spreader of filming of 20 Mills laterally dragged glass plate with described gel solution with having fixing slit.Described glass plate is positioned over is set at 75 ℃ of sides and purged in the forced ventilation baking ovens (VWR type 1330FM) 35 minutes.Other films of curtain coating and drying are 1 hour under 40 Mills.The gained film that is dried to about 4% humidity removed and be stored in from described Mylar sheet use after being used for the polybag.

Other spices comprise mint flavouring, Chinese ilex (winter green) spices or spearmint.Other colorants comprise FD﹠amp; C Blue Alum Lake 35-42%, FD﹠amp; C Emerald Green Lake Blend and FD﹠amp; C Blue Alum Lake+FD﹠amp; C Emerald Green Lake Blend.

Embodiment P. is used for the peach perfuming film of rod/package/bag

Table P1

HPMC	31.73％
HPMC	31.73％	Starch	10.57％
Tobacco	7.49％	Starch	10.57％
Tobacco	7.49％	Na ₂CO ₃	1.12％
Plasticizer	14.59％	Na ₂CO ₃	1.12％
Plasticizer	14.59％	Peach mud	26.01％
Spices	3.37％	Peach mud	26.01％
Spices	3.37％	Sweetener	0.37％
Surfactant	0.75％	Sweetener	0.37％
Surfactant	0.75％	Water	4.00％

MIX1

HM3PA2910(Wolff Cellulosics) 38.48g

HM100PA2208(Wolff Cellulosics) 19.27g

HM4000PA2910(Wolff Cellulosics) 3.24g

B700(Grain Processing Corporation) 20.32g

Tobacco powder (particle mean size＜80 μ m) 14.39g

MIX2

Na ₂CO ₃ 2.16g

Propylene glycolmonostearate 0.72g

Lauryl sodium sulfate 0.72g

In the 3rd container, the composition below the weighing:

MIX3

Glycerine 7.19g

Propane diols 7.19g

PEG400 7.19g

Glyceryl triacetate 6.47g

Peach mud 100.0g

Peach essence 3.60g

Tobacco spice modifier (Hagelin) 2.88g

Sucralose solution 25% (Tate ﹠amp; Lyle) 2.88g

The part of gained gel solution is poured in advance on the glass plate that the Mylar sheet with suitable size covers.Is that the spreader of filming of 20 Mills laterally dragged glass plate with described gel solution with having fixing slit.Described glass plate is positioned over the side purged in the forced ventilation baking oven (VWR type 1330FM) 35 minutes, this baking oven has been set to 75 ℃.The gained film that is dried to about 4% humidity removed and be stored in from described Mylar sheet use after being used for the polybag.

The perfuming that embodiment Q. is used to apply/White-opalescent film

Table Q1

HPMC	45.46％
HPMC	45.46％	Starch	15.15％
Fibersol-2	10.73％	Starch	15.15％
Fibersol-2	10.73％	Na ₂CO ₃	1.07％
Plasticizer	10.73％	Na ₂CO ₃	1.07％
Plasticizer	10.73％	TiO ₂	10.45％
Spices	1.07％	TiO ₂	10.45％
Spices	1.07％	Sweetener	0.27％
Surfactant	1.07％	Sweetener	0.27％
Surfactant	1.07％	Water	4.00％

MIX1

HM3PA2910(Wolff Cellulosics) 38.48g

HM100PA2208(Wolff Cellulosics) 19.27g

HM4000PA2910(Wolff Cellulosics) 3.24g

B700(Grain Processing Corporation) 20.32g

Fibersol-2(Matsutani) 14.39g

MIX2

Na ₂CO ₃ 1.44g

Propylene glycolmonostearate 0.72g

Lauryl sodium sulfate 0.72g

In the 3rd container, the composition below the weighing:

MIX3

Glycerine 3.60g

Propane diols 3.60g

PEG400 3.60g

Glyceryl triacetate 3.60g

TiO ₂Suspension 50% (Sensient Colors) 28.04g

Tobacco spice modifier (Hagelin) 1.44g

Sucralose solution 25% (Tate ﹠amp; Lyle) 1.44g

The weighing boiling water of 606.10g altogether in rustless steel container.Described water is carried out vigorous stirring with Arrow Model1750 high speed shear blender.Xiang Shuizhong adds MIX2.Continue to stir 30 seconds, add MIX1.Continued vigorous stirring 4 minutes.In gained solution, add MIX3.Continued vigorous stirring 1 minute.Gained solution is transferred in the Silverson SS1 container that is suitable for the vacuum mixing.Described container is connected to Silverson L4RTU homogenizer electrodynamic element.(under the 20-25 inch Hg) with described solution homogenizing 2 minutes, places ice bath around described homogenizer container then under 7500RPM under vacuum.Under vacuum (20-25 inch Hg) in 10, lasting homogenization is 8 minutes under the 000RPM.After homogenization is finished, the described solution of part is transferred to the 500mL Nalgene bottle that is used for storing.

The part of gained gel solution is poured in advance on the glass plate that the Mylar sheet with suitable size covers.Is that the spreader of filming of 20 Mills laterally dragged glass plate with described gel solution with having fixing slit.Described glass plate is positioned over the side that is set at 75 ℃ to purge in the forced ventilation baking oven (VWR type 1330FM) 35 minutes.The gained film that is dried to about 4% humidity removed and be stored in from described Mylar sheet use after being used for the polybag.

The tobacco film that embodiment R. extrudes

Table R1

Tobacco	25.63％
Tobacco	25.63％	Klucel LF	61.53％
Na ₂CO ₃	3.32％	Klucel LF	61.53％
Na ₂CO ₃	3.32％	Plasticizer	6.68％
Sweetener	0.83％	Plasticizer	6.68％
Sweetener	0.83％	Water	2.00％

As described herein, with the similar mode of the granulation that is used for tablet manufacturing following composition carried out granulation, to produce tobacco particle (tobacco granulation) with humidity about 4.50%:

Klucel LF(Hercules/Aqualon) 3448.0g

Na ₂CO ₃ 181.0g

Sucralos(Tate & Lyle) 45.0g

Propane diols 363.0g

Tobacco powder (particle mean size＜80 μ m) 1451.0g

Water 2344.0g

Described tobacco particle is incorporated into Leistritz Micro-18 Twin Screw Extruder (double screw extruder) 40: in the feed zone of 1L/D, it has been disposed for extruding with the rotation in the same way of medium-sheared helical design.Being used for the described charging rate of extruding is 1-3 Pounds Per Hour.Machine barrel district temperature is 75-240_.Finish emptying by incorporate drain in the front of the blowing die head of described extruder from the volatile matter of extruding melt.

Make and have width to be about 3 inches and thickness be the tobacco film of 2-3 Mill by incorporate band extrusion die (strip die) at the discharge end of described extruder.When discharging, use the 3-roller to pile up chill roll (stacked chill roller) described tobacco film is rolled (calendaring) and cool to room temperature.From the downstream of described chill roll, described film is introduced Mylar to prevent adhesion between described rete on re-reeler.Described tobacco film is positioned in the container that is applicable to storage.

As described herein, described tobacco film is used to contain subsequently the preparation of the pouch of solvable tobacco.Described film is slowly disintegration in 2-4 minute time in mouth.

Embodiment S. has the perfuming tobacco film of gelatin

Table S1

HPMC	35.95％
HPMC	35.95％	Gelatin	0.98％
Starch	12.30％	Gelatin	0.98％
Starch	12.30％	Tobacco	23.64％
Na ₂CO ₃	1.47％	Tobacco	23.64％
Na ₂CO ₃	1.47％	Plasticizer	10.84％
Spices	9.35％	Plasticizer	10.84％
Spices	9.35％	Sweetener	0.50％
Surfactant	0.97％	Sweetener	0.50％
Surfactant	0.97％	Water	4.00％

MIX1

HM3PA2910(Wolff Cellulosics) 13.84g

HM100PA2208(Wolff Cellulosics) 7.24g

HM4000PA2910(Wolff Cellulosics) 1.21g

B700(Grain Processing Corporation) 7.63g

Gelatin 0.61g

Tobacco powder (particle mean size＜80 μ m) 15.27g

MIX2

Na ₂CO ₃ 0.91g

Propylene glycolmonostearate 0.30g

Lauryl sodium sulfate 0.30g

In the 3rd container, the composition below the weighing:

MIX3

Glycerine 2.14g

Propane diols 2.44g

PEG400 2.14g

Mint flavouring 4.58g

Tobacco spice modifier (Hagelin) 1.22g

Sucralose solution 25% (Tate ﹠amp; Lyle) 1.22g

The weighing boiling water of 288.93g altogether in rustless steel container.Described water is carried out vigorous stirring with Arrow Model1750 high speed shear blender.Xiang Shuizhong adds MIX2.Continue to stir 30 seconds, add MIX1.Continued vigorous stirring 4 minutes.In gained solution, add MIX3.Continued vigorous stirring 3 minutes.Gained solution is transferred to the suitable vessel that is used for storing.

The part of gained gel solution is poured in advance on the glass plate that the Mylar sheet with suitable size covers.Is that the spreader of filming of 20 Mills laterally dragged glass plate with described gel solution with having fixing slit.Described glass plate is positioned over the side that is set at 75 ℃ to purge in the forced ventilation baking oven (VWR type 1330FM) 35 minutes.The gained film that is dried to about 4% humidity is removed and is cut into the unit of suitable size from described Mylar sheet.1.0 inch * film unit disintegration in mouth in less than 30 seconds of 1.25 inches discharges spices, sweetener and tobacco.

Embodiment T. has the perfuming tobacco film of gelatin

Table T1

HPMC	32.01％
HPMC	32.01％	Gelatin	4.92％
Starch	12.30％	Gelatin	4.92％
Starch	12.30％	Tobacco	23.64％
Na ₂CO ₃	1.47％	Tobacco	23.64％
Na ₂CO ₃	1.47％	Plasticizer	10.84％
Spices	9.35％	Plasticizer	10.84％
Spices	9.35％	Sweetener	0.50％
Surfactant	0.97％	Sweetener	0.50％
Surfactant	0.97％	Water	4.00％

MIX1

HM3PA2910(Wolff Cellulosics) 11.40g

HM100PA2208(Wolff Cellulosics) 7.24g

HM4000PA2910(Wolff Cellulosics) 1.21g

B700(Grain Processing Corporation) 7.63g

Gelatin 3.05g

Tobacco powder (particle mean size＜80 μ m) 15.27g

MIX2

Na ₂CO ₃ 0.91g

Propylene glycolmonostearate 0.30g

Lauryl sodium sulfate 0.30g

In the 3rd container, the composition below the weighing:

MIX3

Glycerine 2.14g

Propane diols 2.44g

PEG400 2.14g

Mint flavouring 4.58g

Tobacco spice modifier (Hagelin) 1.22g

Sucralose solution 25% (Tate ﹠amp; Lyle) 1.22g

Embodiment U. has the perfuming tobacco film of gelatin

Table U1

HPMC	27.09％
HPMC	27.09％	Gelatin	9.85％
Starch	12.30％	Gelatin	9.85％
Starch	12.30％	Tobacco	23.64％
Na ₂CO ₃	1.47％	Tobacco	23.64％

Plasticizer	10.84％
Plasticizer	10.84％	Spices	9.35％
Sweetener	0.50％	Spices	9.35％
Sweetener	0.50％	Surfactant	0.97％
Water	4.00％	Surfactant	0.97％

MIX1

HM3PA2910(Wolff Cellulosics) 8.35g

HM100PA2208(Wolff Cellulosics) 7.24g

HM4000PA2910(Wolff Cellulosics) 1.21g

B700(Grain Processing Corporation) 7.63g

Gelatin 6.11g

Tobacco powder (particle mean size＜80 μ m) 15.27g

MIX2

Na ₂CO ₃ 0.91g

Propylene glycolmonostearate 0.30g

Lauryl sodium sulfate 0.30g

In the 3rd container, the composition below the weighing:

MIX3

Glycerine 2.14g

Propane diols 2.44g

PEG400 2.14g

Mint flavouring 4.58g

Tobacco spice modifier (Hagelin) 1.22g

Sucralose solution 25% (Tate ﹠amp; Lyle) 1.22g

The weighing boiling water of 288.93g altogether in rustless steel container.Described water is carried out vigorous stirring with Arrow Model1750 high speed shear blender.Xiang Shuizhong adds MIX2.Continue to stir 30 seconds, add MIX1.Continued vigorous stirring 4 minutes.In gained solution, add MIX3.Continued vigorous stirring 3 minutes.Gained solution is shifted the suitable vessel that is used for storing.

Tablet

Composition of the present invention also can be made into tablet, as supper-fast disintegration (about 15 seconds), disintegration (less than 2 minutes) fast, slow disintegration (2-10 minute) and chewable tablets.

The size of tablet can be single supplies or aliquot more, and a plurality of more aliquots have been formed single supplies.The tablet that is of a size of single supplies typically has the size of 5mm-15mm.Littler tablet typically is 2-4mm on diameter.This littler tablet can be made at the multiple colorant or the spices that are used for consuming simultaneously.Tablet may be molded to compressing tablet, convex or concavity bead, ellipse or any other known shapes concerning trade.Also tablet can be carried out foamed so that dissolving or disintegration faster to be provided in mouth.But tablet also stratification so that multiple taste or mouthfeel to be provided when tablet dissolved or the disintegration.Also tablet can be applied to change color or taste or to be used to provide the mechanical strength that is used to improve processing.In one embodiment, be designed to that quickly disintegrated tablet can apply with extremely thin water-insoluble coating in water,, applied the second water miscible coating simultaneously to provide protection to described tablet.

Can use any forming method well known in the prior art, as making tablet from the dried mix (dry mix) that is commonly referred to as direct compression or from pre-granulated materials by compacting (press), injection moulding, compression moulding, injection foam-formed (injection foam moulding) or compression foam moulding (compressionfoam molding).

Tablet embodiment

Following table has shown the exemplary composition that is used to prepare tablet of the present invention.

Table V 1

	Exemplary range (%)	EXAMPLE V fast (%)	Embodiment W fast (%)	Embodiment X slow (%)	Embodiment Y slow (%)
	Exemplary range (%)	EXAMPLE V fast (%)	Embodiment W fast (%)	Embodiment X slow (%)	Embodiment Y slow (%)	Water-soluble polymer	0-70	0	3	23	0
Tobacco	1-70	27	20	27	30	Water-soluble polymer	0-70	0	3	23	0
Tobacco	1-70	27	20	27	30	Perfumery oil	0.5-40	2	1.8	2	2
Artificial sweetener	0.05-0.4	0.15	0.15	0.15	0.1	Perfumery oil	0.5-40	2	1.8	2	2
Artificial sweetener	0.05-0.4	0.15	0.15	0.15	0.1	Sugar	1-80	64	35	45.85	33.3
Maltodextrin	0-50	0	19	0	0	Sugar	1-80	64	35	45.85	33.3
Maltodextrin	0-50	0	19	0	0	Disintegrant	0.1-15	6.35	3.0	-	-
Starch	5-80	0	17.35	-	50	Disintegrant	0.1-15	6.35	3.0	-	-
Starch	5-80	0	17.35	-	50	Releasing agent	0.1-2.0	0.5	0.5	0.5	0.5
Emulsifying agent	0.1-5.0	0	0.2	0.5	0.1	Releasing agent	0.1-2.0	0.5	0.5	0.5	0.5

The exemplary chewable tablets of embodiment Z.

Can use following composition to form chewable tablets: sompressible sugar (40%), tobacco (20%), glucose (25%), maltodextrin (13%), colouring agent (0.05%), spices (1.35%) and dolomol (0.60%).

Embodiment A A. thermoplasticity tablet

Can use following composition (umber) to form the thermoplasticity tablet: hydroxypropyl cellulose (HPC) 54, tobacco 27, microcrystalline cellulose 10, propane diols 4, artificial sweetening agent 2, spices 2 and stabilizing agent 0.2.Described composition can be carried out dry stirring and use the required barrel zone temperature (typically 340-370_) of the described HPC of fusing that it is fed in the extruder.Extrude the rod of diameter pact _ inch, and be cut into the size of enough formation tablets.

Embodiment A B. tobacco tablet

The prescription of Table A B1. tobacco tablet

Composition	% dry weight base
Composition	% dry weight base	Tobacco powder	25.00
Sweetener	32.11	Tobacco powder	25.00
Sweetener	32.11	Maltodextrin	40.22

Spices	0.75
Spices	0.75	Emulsifying agent	1.36
Na ₂CO ₃	0.56	Emulsifying agent	1.36
Na ₂CO ₃	0.56	Amount to	100.00

Table A B2. is used to prepare the prescription of the adhesive solution of tobacco tablet

Composition	％
Composition	％	Water	45.00
Maltodextrin	53.05	Water	45.00
Maltodextrin	53.05	Emulsifying agent	1.80
Sweetener	0.15	Emulsifying agent	1.80
Sweetener	0.15	Amount to	100.00

The preparation of adhesive solution

In independent container, weigh up the one-tenth component that is shown among the Table A B2.Xiang Shuizhong slowly adds the gum arabic (emulsifying agent) of pre-hydration and mixes under high speed shear stirs in rustless steel container.After dissolving is finished, in described water, slowly add M 585 maltodextrins (Grain ProcessingCorporation).In case M 585 dissolves fully, slowly add sucralose sweetener (Tate ﹠amp; Lyle) and fully mix guaranteeing and dissolve fully.

The peppermint (peppermint) and the spearmint that are shown in the formula ratio among the Table A B1 are joined in the described adhesive solution.By means of homogenizer under 9000-10000RPM with about 20 minutes of all mixture homogenization.By being shown in the appropriate amount that batch size among the Table A B1 and percentage composition are determined employed adhesive solution.The solution of homogenizing is transferred to spices to be held/pumping groove in.

The preparation of dry ingredients

Mix together and be positioned in the product groove being shown in the mannitol (sweetener) of the formula ratio among the Table A B1 and tobacco powder (base of bone dry).

The preparation of Vector Multiflo-15 fluid-bed chamber

Use Vector Multiflo-15 fluid bed coating machine that described adhesive solution is applied on the described dry ingredients mixture, to form final particle.On the control panel computer, select manual handle.The machine operation parameter among the Table A B3 is listed in input in program:

Table A B3.Vector Multiflo-15 fluid bed parameter is provided with

Parameter	Be provided with
Parameter	Be provided with	Inlet temperature (Celsius)	60
Air-flow (CFM)	150	Inlet temperature (Celsius)	60
Air-flow (CFM)	150	Flow (G/ minute)	125
Filtered pulse is (second) at interval	30	Flow (G/ minute)	125
Filtered pulse is (second) at interval	30	The afterpulse time (second)	60

The appropriate amount of injection adhesive solution also is input in the described program.Batch size by expectation determines that the amount of described adhesive solution is to obtain being shown in the percentage composition among the Table A B1.

Granulated processed

In case described dry ingredient is carried out fluidisation and obtains temperature in described fluid bed chamber be 40-45 ℃, and described adhesive solution slowly is sprayed on the described dry ingredient to form described particle.Nozzle exit pressure is set to 22psi and air-flow is 200CFM.Increase described air-flow to guarantee good product motion or the fluidization in described fluid bed chamber.In case all adhesive solutions apply, described air-flow is reduced to 200CFM.In case described product temperature reaches about 43 ℃ then stop this process.

Be used to form the preparation of granules of tablet

It is quantitative that described bulk material is carried out size by 12-order mesh screen.It is quantitative that dolomol (lubricant) is carried out size by 40-order mesh screen.The dolomol that will be shown in the formula ratio among the Table A B4 in polybag combines with described bulk material and hand 2 minutes.

Table A B4. is used to form the component prescription of tablet

Composition	The % dry weight
Composition	The % dry weight	Bulk material	99.50
Lubricant	0.50	Bulk material	99.50
Lubricant	0.50	Amount to	100.00

Tablet formation method

Described bulk material and lubricant are input in the feed hopper of forcing press.Parameter below setting is marked among the Table A B5 on Vanguard VSP 8Mini Rotary Press:

Table A B5. is used for the parameter of tobacco tablet

	Disintegration fast	Slowly disintegration
	Disintegration fast	Slowly disintegration		Parameter	Be provided with	Scope	Be provided with	Scope
Fill the degree of depth (MM)	8.0	11.3	11.3-11.4	Parameter	Be provided with	Scope	Be provided with	Scope
Fill the degree of depth (MM)	8.0	11.3	11.3-11.4	Thickness (MM)	1.3		1.8
Principal pressure (KN)	5.0		10.8-12.0	Thickness (MM)	1.3		1.8
Principal pressure (KN)	5.0		10.8-12.0	Expulsion pressure (MM)				0.03-0.12

Disintegration disintegration in 1-3 minute in mouth fast.Slowly disintegration disintegration in 5-8 minute in mouth.

Embodiment A C. tobacco tablet

The prescription of Table A C1. tobacco tablet

Composition	% dry weight base
Composition	% dry weight base	Tobacco powder	25.00
Sweetener	34.11	Tobacco powder	25.00
Sweetener	34.11	Maltodextrin	38.58
Spices	1.00	Maltodextrin	38.58
Spices	1.00	Emulsifying agent	1.31
Amount to	100.00	Emulsifying agent	1.31

Table A C2. is used to prepare the prescription of the adhesive solution of tobacco tablet

Composition	％
Composition	％	Water	45.00
Maltodextrin	53.04	Water	45.00
Maltodextrin	53.04	Emulsifying agent	1.80
Sweetener	0.16	Emulsifying agent	1.80
Sweetener	0.16	Amount to	100.00

Follow the method for before in embodiment A B1, stating that is used for the adhesive solution preparation.In adhesive solution, add peppermint (peppermint) and spearmint and the 45.00g Na that is marked in the formula ratio among the Table A C1 ₂CO ₃Follow the preparation that is used to constitute described adhesive solution, dry ingredient, the preparation and the prilling process in VectorMultiflo-15 fluid bed chamber.

Be used to form the preparation of granules of tablet

As previously mentioned, it is quantitative described bulk material to be carried out size by suitable mesh screen.The dolomol of formula ratio (be used for quick disintegration and be 0.75% or be used for slow disintegration be 1.00%) is combined and hand 2 minutes at polybag with described bulk material.

Tablet formation method

The mechanically actuated parameter that is marked among the Table A C3 is set on Vanguard VSP 8 Mini Rotary Press:

The tablet that Table A C3. is used for the tobacco tablet forms parameter

	Disintegration fast		Slowly disintegration
	Disintegration fast		Slowly disintegration		Parameter	Be provided with	Scope	Be provided with	Scope
Fill the degree of depth (MM)	6.8		9.9		Parameter	Be provided with	Scope	Be provided with	Scope
Fill the degree of depth (MM)	6.8		9.9		Thickness (MM)	1.1			2.0-2.1
Principal pressure (KN)		6.9-7.2		3.8-4.0	Thickness (MM)	1.1			2.0-2.1
Principal pressure (KN)		6.9-7.2		3.8-4.0	Expulsion pressure (MM)				0.03-0.15

Embodiment A D. tobacco tablet

The prescription of Table A D1. tobacco tablet

Composition	% dry weight base
Composition	% dry weight base	Tobacco powder	25.00
Filler	30.00	Tobacco powder	25.00
Filler	30.00	Maltodextrin	42.15
Spices	0.75	Maltodextrin	42.15
Spices	0.75	Emulsifying agent	1.43
Sweetener	0.12	Emulsifying agent	1.43
Sweetener	0.12	Na ₂CO ₃	0.56
Amount to	100.00	Na ₂CO ₃	0.56

Table A D2. is used to prepare the prescription of the adhesive solution of tobacco tablet

Composition	％
Composition	％	Water	45.00
Maltodextrin	53.06	Water	45.00

Emulsifying agent	1.80
Emulsifying agent	1.80	Sweetener	0.14
Amount to	100.00	Sweetener	0.14

Follow the method that before is used for the adhesive solution preparation.In adhesive solution, add cinnamon flavor and the Na that is marked in the formula ratio among the Table A D1 ₂CO ₃Following the preparation (the lactose filler that combines with tobacco powder) that is used to constitute described adhesive solution, dry ingredient, the preparation in Vector Multiflo-15 fluid bed chamber and the residue of prilling process handles.

Be used to form the preparation of granules of tablet

It is quantitative that described bulk material and dolomol are carried out size by 12-order mesh screen and 40-order mesh screen respectively.The dolomol of formula ratio (be used for quick disintegration and be 0.50% or be used for slow disintegration be 1.00%) is combined and hand 2 minutes at polybag with described bulk material.

Tablet formation method

The mechanically actuated parameter that is marked among the Table A D3 is set on Vanguard VSP 8 Mini Rotary Press:

The tablet that Table A D3. is used for the tobacco tablet forms parameter

	Disintegration fast		Slowly disintegration
	Disintegration fast		Slowly disintegration		Parameter	Be provided with	Scope	Be provided with	Scope
Fill the degree of depth (MM)	7.7		11.2	11.2-11.3	Parameter	Be provided with	Scope	Be provided with	Scope
Fill the degree of depth (MM)	7.7		11.2	11.2-11.3	Thickness (MM)	1.1		1.7	1.7-1.8
Principal pressure (KN)		5.7-6.0		3.8-4.0	Thickness (MM)	1.1		1.7	1.7-1.8
Principal pressure (KN)		5.7-6.0		3.8-4.0	Expulsion pressure (MM)		0.03-0.08		0.03-0.17

Embodiment A E. tobacco tablet

Follow the same procedure that being used among the embodiment A D prepares the tobacco tablet, difference is to use Chinese ilex (winter green) spices to replace cinnamon flavor.

Be used to form the preparation of granules of tablet

It is quantitative then the described material of finishing to be carried out size by 12-order mesh screen.It is quantitative that dolomol carries out size by 40-order mesh screen.The dolomol of formula ratio (be used for quick disintegration and be 0.50% or be used for slow disintegration be 0.75%) is combined and hand 2 minutes at polybag with described bulk material.

Tablet formation method

The parameter that is marked among the Table A E1 is set on Vanguard VSP 8 Mini Rotary Press:

The tablet that Table A E1. is used for the tobacco tablet forms parameter

	Disintegration fast		Slowly disintegration
	Disintegration fast		Slowly disintegration		Parameter	Be provided with	Scope	Be provided with	Scope
Fill the degree of depth (MM)	8.1		12.0	12.0-12.1	Parameter	Be provided with	Scope	Be provided with	Scope
Fill the degree of depth (MM)	8.1		12.0	12.0-12.1	Thickness (MM)	1.1	1.1-1.2	1.8
Principal pressure (KN)	5.7	5.7-6.0	4.5	4.5-5.2	Thickness (MM)	1.1	1.1-1.2	1.8
Principal pressure (KN)	5.7	5.7-6.0	4.5	4.5-5.2	Expulsion pressure (MM)		0.03-0.09		0.04-0.19

Embodiment A F. has the tobacco tablet of opaque white color coating

The prescription of Table A F1. tobacco tablet

Composition	% dry weight base
Composition	% dry weight base	Tobacco	25.00
Filler	30.00	Tobacco	25.00
Filler	30.00	Maltodextrin	39.74
Spices	0.75	Maltodextrin	39.74
Spices	0.75	Emulsifying agent	1.35
Sweetener	0.10	Emulsifying agent	1.35
Sweetener	0.10	Na ₂CO ₃	0.56
Tobacco spice modifier	2.50	Na ₂CO ₃	0.56
Tobacco spice modifier	2.50	Amount to	100.00

Table A F2. is used to prepare the prescription of the adhesive solution of tobacco tablet

Composition	％
Composition	％	Water	45.00
Maltodextrin	53.07	Water	45.00
Maltodextrin	53.07	Emulsifying agent	1.80
Sweetener	0.13	Emulsifying agent	1.80
Sweetener	0.13	Amount to	100.00

The preparation of adhesive solution

The described method that is used for the adhesive solution preparation before following.In adhesive solution, add apple spice, natural bitterness blocking agent (Comax) and the Na that is marked in the formula ratio among the Table A F1 ₂CO ₃Following the preparation (the lactose filler adds tobacco powder) that is used to constitute described adhesive solution, dry ingredient, the preparation in VectorMultiflo-15 fluid bed chamber and the residue of prilling process handles.

Be used to form the preparation of granules of tablet

It is quantitative then the described material of finishing to be carried out size by 12-order mesh screen.It is quantitative that dolomol carries out size by 40-order mesh screen.The dolomol (being used for slow disintegration is 0.75%) of formula ratio is combined and hand 2 minutes at polybag with described bulk material.

Tablet formation method

The parameter that is marked among the Table A F3 is set on Vanguard VSP 8 Mini Rotary Press:

The tablet that Table A F3. is used for slow disintegration tobacco tablet forms parameter

Parameter	Be provided with	Scope
Parameter	Be provided with	Scope	Fill the degree of depth (MM)	13.6	13.5-13.7
Thickness (MM)	2.4	2.4-2.5	Fill the degree of depth (MM)	13.6	13.5-13.7
Thickness (MM)	2.4	2.4-2.5	Principal pressure (KN)		4.5-5.2
Expulsion pressure (MM)		0.04-0.24	Principal pressure (KN)		4.5-5.2

The tobacco tablet applies suspension complement (Tobacco tab coating-suspension makeup)

Guidance according to the producer has prepared 20% the Opadry II aqueous solution, and mixes 45 minutes before coating.

Painting method

Tablet (5.5-6.5KG) is put in the coating pan of Vector/Freund Hi-coating machine pan coating machine, and carries out warmly reaching 45 ℃ up to delivery temperature.Described dish with less than under the 5RPMs running finish this step so that the tablet minimise wear." make air pass described dish with 100CFM under the dish pressure of water-0.5 at 75 ℃.

In case described tablet reaches temperature, described dish speed is increased to about 15RPMs and applies described Opadry coating suspension with 15-20g/ minute speed.During applying, mix described suspension continuously to prevent the solid sedimentation.Under about 70psi, use about 100 litres of air per minute described hydrojet that atomizes.The directed air porthole (directional air ports) of use on nozzle makes mist formula hydrojet form pattern, with described nozzle when about 70psi setting into about 50 litres of air per minute.

Periodically increase or reduce inlet air temperature to keep delivery temperature between 43-46 ℃.

Continue spraying and be applied to satisfy up to solid and be typically about 3% prescription demand, or visually be satisfied up to tablet with desired amount.

The solid tobacco of embodiment A G. disintegratable

Component below in independent container, taking by weighing:

Kluce EF(Hercules) 60g

Tobacco powder 75g

Tobacco spice modifier (tobacco flavor 6gmodifier)

Corn syrup (65%) 45g

Sucrose 45

B700(Grain Processing Corp.) 51g

Sucralose solution 25% (Tate ﹠amp; Lyle) 3g

Propane diols 3g

Sodium carbonate 1.5g

Water 6g

Fructus Piperis peppermint oil 4.5g

Part water 1 (heat) 120g

Part water 2 (cold) 120g

6g water is joined in the sodium carbonate, and stir described mixture.Stir this mixture in another composition that it is joined in the method.

Part water 2 (cold) is put in carries out freezingly in the ice bath, and part water 1 (heat) is heated to 60 ℃ and transfer in the rustless steel container.Stir described 60 ℃ water and Klucel EF is little by little joined in this water with Arrow Model 1750 high speed shear blenders.With this solution stirred for several minute.Then part water 2 (cold) is joined in this mixture.Below described rustless steel container, place ice bath, and mixture was stirred 15 minutes.

Stir after 15 minutes, join in the described mixture residual components is disposable.Before adding next composition, this mixture is mixed fully.Described composition adds in the following order: tobacco spice modifier, propane diols, sucralose solution, corn syrup, sodium carbonate liquor, sucrose, tobacco powder, B700 and Fructus Piperis peppermint oil.In whole mixed process, in ice bath, add ice to keep mixture ice-cold.After adding all the components, described mixing was stirred 10 minutes in addition.

From described ice bath, shift out container, and described mixture partly is distributed on the paraffin paper with the solid disintegratable, and at room temperature dry 24 hours.Remove the solid of disintegratable from described paraffin paper, and transfer to and continue drying at room temperature on another sheet paraffin paper.After lasting dry 12-24 hour, obtained being used for the desired hardness of described disintegratable solid.

The solid tobacco of embodiment A H. disintegratable

Component below in independent container, taking by weighing:

HPMC 2910 HM E5/6Bv(Celanese) 60g

Tobacco powder 75g

Tobacco spice modifier 6g

Corn syrup (65%) 45g

Sucrose 45g

B700(Grain Processing Corp.) 39g

Sucralose solution 25% (Tate ﹠amp; Lyle) 3g

Propane diols 15g

Sodium carbonate 1.5g

Water 6g

Fructus Piperis peppermint oil 4.5g

Part water 1 (heat) 120g

Part water 2 (room temperature) 120g

6g water is joined in the sodium carbonate, and stir described mixture.Stir this mixture in a back composition that it is joined in the method.

Part water 1 (heat) is heated to 80 ℃ and transfer in the rustless steel container.Stir described 80 ℃ water and HPMC is little by little joined in this water with Arrow Model1750 high speed shear blender.With this solution stirred for several minute.Then part water 2 (room temperature) is joined in this mixture, and described mixture was stirred 15 minutes.

Stir after 15 minutes, join in the described mixture residual components is disposable.Before adding next composition, this mixture is mixed fully.Described composition adds in the following order: tobacco spice modifier, propane diols, sucralose solution, corn syrup, sodium carbonate liquor, sucrose, tobacco powder, B700 and Fructus Piperis peppermint oil.After adding all the components, described mixing was stirred 10 minutes in addition.

Be assigned to described mixture on the paraffin paper and at room temperature dry 24 hours in batches (in portions).Remove the solid of disintegratable from described paraffin paper, and transfer to and continue drying at room temperature on another sheet paraffin paper.After lasting dry 12-24 hour, obtained being used for the desired hardness of described disintegratable solid.

Use identical prescription, mixed process and assigning process to obtain similar articles, but described disintegratable solid is in the pressurized air baking oven that is set at 32 ℃ (forced air oven) (VWR Model1330FM) dry 1 hour.Then described disintegratable solid is removed from baking oven and at room temperature dry 24 hours.In addition, the disintegratable solid is following dry 18 hours in 32 ℃ in described pressurized air baking oven.Use this drying process, obtained having the bigger a little disintegratable solid of hardness that (dull finish) handled in delustring.

Embodiment A I. multilayer tablet

The pressure apparatus that can use commerce to obtain prepares the tablet with two or more evident layers.The composition of these layers can be identical or different in composition.Single layer can there are differences aspect color, fragrance, tobacco type, tobacco content, dissolution velocity and other similar characteristics.For example, one deck rapidly disintegration discharge spices or smell is sheltered composition.Comprise the second layer disintegration more lentamente of tobacco powder, thereby little by little expose tobacco.

Profiled member

Thereby tobacco compositions may be molded to abundant rigidity easy to handle goods.These moulded products can there are differences on the physical property and arrive between the high hardened component in high flexibility.These goods can form Any shape and can be fine and close or foamed.These compositions typically have the 2-50% of finished weight, the moisture content of preferred 5-10%.Exemplary shape comprises pipe, toothpick, rod, helical form or solid bar (solid rod).Typically, can delay to suck or chew profiled member in mouth, to discharge the tobacco organoleptic ingredients.Profiled member can or cannot mouthful disintegration.Disintegration preferably took place in 1-10 minute at 1-60 minute in the parts of disintegratable.

The size of profiled member can be suitable fully or improper in mouth.Can partly insert the composition bigger than mouth.The typical full-size of profiled member is 6 inches, more preferably 2.5 inches.

Profiled member can comprise discontinuity zone, as has each zone of identical or different spices or colorant or size or the agent of tobacco form, and described tobacco is as perceptible tobacco of when dissolving.For example, the helical form profiled member can comprise single rope, and each rope has different spices or color or size or the agent of tobacco form.As further embodiment, can prepare profiled member by multistep process, wherein molding or extrusion molding spare are made of multilayer, and two-layer or multilayer wherein comprises different spices, colorant or size or the agent of tobacco form.

Can use that any known method prepares the profiled member composition in the prior art, as extrude, compression moulding, injection moulding, drawing, foam-formed, blowing and overmolded.In addition, profiled member can be based on water-soluble or thermoplasticity form agent.In one embodiment, make water base profiled member by the viscous paste (as by the Hobar method) that forms described form agent, water, tobacco and other compositions, and described slurry is pressed into mould (form), extrudes or form thin slice by die head, therefrom cut this shape.Then can dry described section or form part and make that moisture is the 2-50% of finished weight, be preferably 5-10% to be used for high rigid element and 10-50% to be used for the high flexibility parts.In another embodiment, water paste as described in can in twin-stage expressing technique (as by the Wenger double screw extruder), forming, wherein in the mixing of described machinery or pre-extrusion grade, mix described form agent, water, tobacco and other compositions, and the twin-screw that the gained slurry is fed directly into described machinery is extruded in the element, and extrude to form shape by die head, be dried desired moisture then.For example, handle component mixed by PK agitator, high intensity mixer, prefabricated grain machine or granulation (fluid bed or Hobart) and make thermoplastic matrix's profiled member.Mixed then component can be extruded to form profiled member by routine list or double screw extruder, perhaps described mixture can be fed in injection machine or other thermoplasticity processing equipments to form profiled member.

Profiled member embodiment

Embodiment A J. injection molding part

Following table provides the exemplary profiled member that forms by injection moulding.

Table A J1.

	1	2	3	4	5	6	7	8
	1	2	3	4	5	6	7	8	Composition	％	％	％	％	％	％	％	％
Tobacco	47.98	45.59	67.18	63.83	78.22	74.32	29.33	27.87	Composition	％	％	％	％	％	％	％	％
Tobacco	47.98	45.59	67.18	63.83	78.22	74.32	29.33	27.87	Low viscosity HPC	48.02	45.62	28.84	27.40	19.59	18.61	68.48	65.06
Water	4	3.80	3.98	3.78	2.19	2.08	2.19	2.08	Low viscosity HPC	48.02	45.62	28.84	27.40	19.59	18.61	68.48	65.06
Water	4	3.80	3.98	3.78	2.19	2.08	2.19	2.08	Propane diols		4.99		4.99		4.99		4.99

The thermal treatment zone is district 1-300-340_, district 2-350-370_, district 3-300-340_; Molding temperature is an environment temperature.Be fed in the screw rod enough compositions feasible identical with an infusion cycles; Be injected into material in the mould immediately; Open mould after 10 seconds, and shift out profiled member.Described profiled member is classification color chips (stepped color chip), 1/8 ^Th, 1/4 ^ThWith 3/8 ^ThClassification on the inch thickness, 2 inches * 3 inches.

Embodiment A K. compression molding spare

Following table provides the exemplary profiled member that is formed by compression moulding.

Table A K1

	A	B	C	D	E	F	G
	A	B	C	D	E	F	G	Composition	％	％	％	％	％	％	％
Tobacco	26.47	25.00	25.00	30.00	25.00	25.00	25.00	Composition	％	％	％	％	％	％	％
Tobacco	26.47	25.00	25.00	30.00	25.00	25.00	25.00	Cornstarch	49.41	30.30		9.50	60.60	30.30	56.60
Starch B-820			30.30					Cornstarch	49.41	30.30		9.50	60.60	30.30	56.60
Starch B-820			30.30					Maltodextrin						30.30
Low viscosity HPC				45.00				Maltodextrin						30.30
Low viscosity HPC				45.00				Soluble fibre		30.30	30.30
Chinese cassia tree	4.41	5.00	5.00	5.00	5.00	5.00	5.00	Soluble fibre		30.30	30.30
Chinese cassia tree	4.41	5.00	5.00	5.00	5.00	5.00	5.00	Perfumery oil	4.41	5.00	5.00	5.00	5.00	5.00	5.00
Sucralose	0.88	0.90	0.90	0.90	0.90	0.90	0.90	Perfumery oil	4.41	5.00	5.00	5.00	5.00	5.00	5.00
Sucralose	0.88	0.90	0.90	0.90	0.90	0.90	0.90	Sodium carbonate	2.65	2.50	2.50	2.50	2.50	2.50	2.50
Glycerine		1.00	1.00	2.00	1.00	1.00	5.00	Sodium carbonate	2.65	2.50	2.50	2.50	2.50	2.50	2.50
Glycerine		1.00	1.00	2.00	1.00	1.00	5.00	Propane diols	11.77

10-50g water is joined in the capacity compound of every 100g drying with softening described compound and make it by being installed in the paste mould (pasta die) on the blender.Die parameters is as follows:

Table A K2

Mold temperature	220-280_
Mold temperature	220-280_	The time of staying	5-60 second
The toothpick die cavity	5/32 inch diameter * 2 3/8 ^thLong	The time of staying	5-60 second
The toothpick die cavity	5/32 inch diameter * 2 3/8 ^thLong	The rod die cavity	3/8 ^thInch diameter * 2 3/8 ^thLong
The disk die cavity	3/4 inch diameter * 1/4 is inch dark	The rod die cavity	3/8 ^thInch diameter * 2 3/8 ^thLong

As long as between the extensin period of described profiled member, allow the free emptying of steam, then the time of staying long more, can make the more profiled member of rigidity.Still keep flexible after also can using additive to make described profiled member from mould, take out.Be held on (40-60 second) in the mould for a long time if will comprise the profiled member of most low viscosity HPC, then formed good workpiece (piece).Comprise plasticizer and increased the speed that moisture absorbs from environment, this has caused some profiled members along with the time takes place softening.

When filling die cavity fully, densification and rigid element have been made with the molding compounds material.When the mould capacity that described die cavity is filled to about 75%, under expansion steam pressure (expanding steampressure), described compound has formed the foamed parts, and these parts have favorable rigidity, good fragrance and disintegration easily in mouth.

In mixture as described in surfactant (as lauryl sodium sulfate) is incorporated into, and making beating to be introducing air, thereby finishes foaming in Aquo System; Also can be under the high speed shear, by finishing foamed or inflation in the Aquo System as described in gas (as nitrogen) is incorporated at described composition.Then described Aquo System is dried to desired moisture with preparation stable foam composition.In one embodiment, Aquo-composition is introduced with partially filled pressing mold; Seal described pressing mold; Mold temperature is elevated to the boiling point that is higher than water forming steam, the described Aquo-composition of this steam expansion is to be full of void area and to produce the profiled member of foamed.For thermoplastic systems, water can be incorporated in tobacco/form agent composition and finish foaming; The rising temperature is higher than the boiling point of water with formation steam with when described tobacco compositions leaves die head, and described steam expansion is to produce foaming structure.In another embodiment, gas (as nitrogen or carbon dioxide) was incorporated into before composition discharges from extruder in the thermoplasticity tobacco compositions of fusing, thereby in the tobacco compositions of moulding, produces foaming structure highly uniformly.Other thermoplasticity foaming methods (as the spray foam moulding) that are known in the art can be used to prepare the tobacco compositions and the profiled member of foamed.

The exemplary moisture profiled member of embodiment A L.

Table A L1 and AL2 have shown the exemplary composition that is used to prepare moisture profiled member of the present invention.Add enough water to form the slurry of thickness.

Table A L1

	Exemplary (part)	Preferably	Embodiment
	Exemplary (part)	Preferably	Embodiment	Tobacco	1-80	30-50	54
Spices	0.5-4	2.5-3	3	Tobacco	1-80	30-50	54
Spices	0.5-4	2.5-3	3	Insoluble fiber	4.5-3.6	22.5-27	27
Water soluble (CO) polymers	1-50	5-20	10CMC 7MF (medium-viscosity)	Insoluble fiber	4.5-3.6	22.5-27	27
Water soluble (CO) polymers	1-50	5-20	10CMC 7MF (medium-viscosity)	Filler/disintegrant	1-50	10-30	30 microcrystalline celluloses
Artificial sweetener	0.05-5	0.1-2	0.2 sucralose	Filler/disintegrant	1-50	10-30	30 microcrystalline celluloses
Artificial sweetener	0.05-5	0.1-2	0.2 sucralose	Dispersant	0.1-20	0.1-2	0.2 lauryl sodium sulfate

Table A L2

	Exemplary (part)	Preferably	Embodiment
	Exemplary (part)	Preferably	Embodiment	Tobacco	1-80	20-50	27
Spices	0.5-4	1-3	1	Tobacco	1-80	20-50	27
Spices	0.5-4	1-3	1	Insoluble fiber	4.5-36	9-27	9
Water soluble (CO) polymers	1-50	5-25	18 low viscosity HPC	Insoluble fiber	4.5-36	9-27	9
Water soluble (CO) polymers	1-50	5-25	18 low viscosity HPC	Filler/disintegrant	1-50	10-30	10 microcrystalline celluloses
Artificial sweetener	0.05-3	0.1-1	0.5 sucralose	Filler/disintegrant	1-50	10-30	10 microcrystalline celluloses
Artificial sweetener	0.05-3	0.1-1	0.5 sucralose	Dispersant	0.1-20	0.1-2	0.2 lauryl sodium sulfate

Embodiment A M. exemplary hot plastic forming spare

Table A M1 has shown the exemplary composition that is used to prepare thermoplastic molding's part of the present invention.

Table M1

	Exemplary (part)	Preferably	1	2	3
	Exemplary (part)	Preferably	1	2	3	Tobacco	10-80	25-80	76.6	50	25
Plasticizer	1-20	1-20	3 propane diols	4.6 propane diols	5.6 propane diols	Tobacco	10-80	25-80	76.6	50	25
Plasticizer	1-20	1-20	3 propane diols	4.6 propane diols	5.6 propane diols	Water soluble (CO) polymers	10-80	20-50	20	30	40
Filler	0-60	0-30	-	15	29	Water soluble (CO) polymers	10-80	20-50	20	30	40
Filler	0-60	0-30	-	15	29	Stabilizing agent	0.1-0.5	0.2-0.4	0.4	0.4	0.4

Embodiment A N. tobacco rod

Tobacco rod is made up of tobacco (54 parts), spices (2), insoluble fiber (28), CMC (10), artificial sweetener (0.2) and microcrystalline cellulose (30).Add the water (as 140 parts) that enough forms viscous paste, and described slurry can be processed by extruder suitably.Suitable extruder can be the Kitchen Aid mixer that is equipped with paste extruder and die head.To use by the rod that extruding of paste die head makes then and act on the formation axle (forming mandrel) of coiled coil machine and can use the film that comprises tobacco to form packaging material (wrapping) around described tobacco core.

The Chinese cassia tree perfuming tobacco rod of embodiment A O. compression moulding

Table A O1

Tobacco	23.84％
Tobacco	23.84％	Starch	24.09％
HPMC	4.97％	Starch	24.09％
HPMC	4.97％	Spices	15.90％

Filler	19.27％
Filler	19.27％	Na ₂CO ₃	2.98％
Sweetener	0.99％	Na ₂CO ₃	2.98％
Sweetener	0.99％	Plasticizer	4.97％
Water	3.00％	Plasticizer	4.97％

Weighing and in the container of appropriate volume in conjunction with following composition.

MIX1

HM100PA2208(Wolff Cellulosics) 11.16g

B700(Grain Processing 55.77gCorporation)

Chinese cassia tree powder 24.54g

Fibersol-2(Matsutani) 44.61g

Na ₂CO ₃ 6.69g

Sucralose (Tate ﹠amp; Lyle) 2.22g

Tobacco powder (particle mean size＜80 μ m) 55.77g

MIX2

Glycerine 11.16g

Cinnamon flavor 11.16g

MIX1 is joined in the stainless steel mixing tank of Kitchen Aid formula blender.Medium-low speed connect under the help of paddle, in described mixture, in 3 minutes, slowly incorporate MIX2 into.After the adding, in mixture, add 76.92g water in the same manner.The gained slurry was at room temperature left standstill 5 minutes.

After this time, described slurry feed is formed unit (strand forming unit) by the rope that is connected to 1/8 inch perforate on the described Kitchen Aid blender.It is the 1_-2 inch that the rope that is produced is cut into length, and is stored in the suitable containers.

2 inches * 1/4 inch the secondary platen of having that faces die cavity is heated to 300-330_.Formed rope is put in the lower chamber, and by the described mold of buffer seal.Described mold cuts out 30-60 second, be provided for the starch ingredients of the described unit of boiling and the means of release portion volatile component.

Be about the inside that 2 inches * 1/8 inch new formation rod comprises level and smooth rigid outer layer and rigid foams shape through measurement.Described unit can disintegration in 1-2 minute in mouth.

The apple perfuming tobacco rod of embodiment A P. compression moulding

Table A P1

Tobacco	23.84％
Tobacco	23.84％	Starch	24.09％
HPMC	4.97％	Starch	24.09％
HPMC	4.97％	Spices	6.45％
Filler	19.27％	Spices	6.45％
Filler	19.27％	Na ₂CO ₃	2.98％
Sweetener	10.42％	Na ₂CO ₃	2.98％
Sweetener	10.42％	Plasticizer	4.97％
Water	3.00％	Plasticizer	4.97％

MIX1

HM100PA2208(Wolff Cellulosics) 11.16g

B700(Grain Processing 55.77gCorporation)

Sucrose 22.29g

Fibersol-2(Matsutani) 44.61g

Na ₂CO ₃ 6.69g

Sucralose (Tate ﹠amp; Lyle) 1.11g

Malic acid 2.22g

Tobacco powder (particle mean size＜80 μ m) 55.77g

MIX2

Glycerine 11.16g

Apple spice 12.27g

MIX1 is joined in the stainless steel mixing tank of the vertical blender of Kitchen Aid.Medium-low speed connect under the help of paddle, in described mixture, in 3 minutes, slowly incorporate MIX2 into.After the adding, in mixture, add 76.95g water in the same manner.The gained slurry was at room temperature left standstill 5 minutes.

After this time, described slurry feed is formed the unit by the rope that is connected to 1/8 inch perforate on the described Kitchen Aid blender.It is the 1_-2 inch that the rope that is produced is cut into length, and is stored in the suitable containers.

Be about the inside that 2 inches * 1/8 inch new formation rod comprises rigid outer layer and rigid foams shape through measurement.Described unit can disintegration in 1-2 minute in mouth.

The tobacco rod that embodiment A Q. extrudes

Table A Q1

Tobacco	24.34％
Tobacco	24.34％	Starch	58.48％
Na ₂CO ₃	3.17％	Starch	58.48％
Na ₂CO ₃	3.17％	Plasticizer	6.34％
Sweetener	0.79％	Plasticizer	6.34％
Sweetener	0.79％	Spices	4.88％
Water	2.00％	Spices	4.88％

With the identical prilling process that is used for preparation tablets following composition is carried out granulation, produced tobacco particle with about 4.5% humidity.

B700(Grain Processing 3327.1gCorporation)

B825(Grain Processing 120.0gCorporation)

Na ₂CO ₃ 181.4g

Sucralose (Tate ﹠amp; Lyle) 45.4g

Glycerine 362.9g

Tobacco powder (particle mean size＜80 μ m) 1451.5g

Water 3473.0g

Tobacco particle is incorporated into Leistritz Micro-18 Twin Screw Extruder 40: in the feed zone of 1L/D, it has been carried out the moderate shear helical design and be used for rotating in the same way extruding with configuration.The described charging rate of extruding be the 1-3 pound per hour.Machine barrel district temperature is 75-100_.It is 5% of process flow rate that setting spices applies speed; Therefore cinnamon flavor can be incorporated into the process downstream of described granulation charging.By before the discharging punch die of described extruder, incorporating ventilating opening into, can finish emptying from the volatile matter of extruding melt.

Can make and have the about 1/8 inch solid tobacco rod of diameter by incorporate the rope punch die at the discharge end of described extruder.During discharge, can on the air cooling conveyer belt, flexible tobacco rope cool to room temperature also be hardened, and can be cut into about 2_ inchage.Formed tobacco rod is put in the suitable vessel that is used for storing.Described rod can slowly disintegration in 5-10 minute in mouth.

Gel and gel bead. composition of the present invention also can be made into gel or gel bead.Described composition can comprise the solvable or insoluble gel that contains tobacco.Gel can be used for sealing other materials, or other materials can be sealed gel.Gel can comprise the hydrated form agent that reaches 70% water and be consumed.The parts that also can dry described gel comprise 1-70% water with generation.The amount that is retained in the water in the described gel depends on performance desired in finished product.Can prepare the gel that comprises the tobacco that multiple organ sensory characteristic can be provided.

The example gel form agent that is used for solvable or insoluble gel comprises kappa carrageen glue, mosanom, carboxymethyl cellulose, gelatin, pectin, agar and starch.

By the described form agent of dissolving under heating up,, under 180_, and tobacco powder joined in this solution as kappa carrageen glue, continue violent the mixing simultaneously, can form the sol gel that comprises tobacco.Then hot mixt is deposited in the mold.Gelatin at room temperature provides weak gel, but can increase its hardness and stability by adding agar or starch.Can form other gel form agent in a similar manner.

By being joined, crosslinking agent forms insoluble gel in predissolve solution or the slurries.Described solution is deposited in the mold forming desired shape, and solidifies by cooling and/or drying.In most cases, solution must be maintained high temperature as greater than under the 180_ to prevent from before depositing to mold to take place gelatification early.After described gel hardens into its net shape, can pack described gel or it further is dried to desired water content by original state.Crosslinking agent comprises the potassium ion that is used for carrageenan, be used for the calcium ion of alginates and LM and be used for the trivalent ion such as the aluminium of carboxymethyl cellulose.In insoluble gel (being the gel that those can not mouthful disintegration), when containing clothes or chew gel in mouth, tobacco organ sensation compound can leach from described gel.

In one embodiment, gel combination is that bead has solid or liquid center.The exemplary solid center comprises smokeless tobacco.The dissolution characteristics that depends on the described Zhu Bi of sealing, inner liquid can be moisture, non-water or heterogeneous.Water fluid typically can be encapsulated in the water-fast gel, described gel can machinery or chemical disintegration in mouth.Seal the gel form agent and can comprise polymer and crosslinking agent.Exemplary system comprises carrageenan and monovalent cation (as potassium), alginates or pectin and divalent ion (as calcium), carboxymethyl cellulose and trivalent ion (as aluminium), and gelatin and gum arabic.Described center can comprise or not comprise tobacco.

In another embodiment, water-soluable gel has been sealed non-water filler as using ethanol, ethylene glycol, vegetable oil or mineral oil.Described water-soluable gel and/or described non-water filler can comprise tobacco described here and other compositions.Liquid, aqueously also can be encapsulated in the water-soluable gel by adding additive such as sugar or salt, described additive fully combines available moisture in filler, has prevented that therefore water-soluble in liquid from having separated described sealant.Gel sealant also can comprise hard standard and soft standard gelatin capsule, and it can be full of liquid or solid.

The center of these gel combinations can comprise or not comprise as the tobacco as the tobacco slurries.Described gel sealant also can comprise or not comprise tobacco.The exemplary solid center comprises smokeless tobacco.Described center also can comprise colorant, sweetener, spices or odor masking agent, and what it can be with described gel sealant is identical or different.The disintegration rate at described gel sealant and center can be identical or different.Gel with center typically has the full-size that is 10mm to the maximum, as is 5mm to the maximum.Can be incorporated in the solution by drop, cause the gelation of the outer surface of described gel bead, and keep described liquid center and make gel bead with liquid center with tobacco/form agent composition.Can use by Morishita Jintan Company and other exploitation and refer generally to form pearl into " seamless liquid encapsulation " or the industrial method of " Sealmess capsule technology ".In addition, the supplier of alginates, carrageenan and pectin polymer has developed the widely-used method that is used for forming all types gel (comprising bead), and it is known in the art.By the concentration of the concentration that changes described form agent, described crosslinking agent (as salt), the temperature and the time of staying of gel bead in curing solution of curing solution, can control the amount of gelation, thereby can control the thickness of gel sealant.Described solution can comprise crosslinking agent maybe can come initiated gelization by other modes such as temperature change.

Solid gel is soluble or insoluble.For solid gel, can will have additive or not have the described tobacco of additive and form agent typically to mix, and make described form agent gelling.Can use from-gel natural gum gelatin such as gellan gum or kappa carrageen glue, or use by changing polymer such as the gelatin that temperature solidifies and make the solubility gel.Can use crosslinking agent to make the insoluble solid gel.Can contain water crosslinking and make this solvable or insoluble gel to form sphere in bathing by drop being incorporated in the oil bath as canola oil or being incorporated into.Also it can be entered into water base crosslinker solution by oil prepares.Gel also can form or carry out cross cutting from sheet material in mold.

In another embodiment, gel combination is for example supplied with the powder type agent as the dry mixing mixture of form agent, crosslinking agent (as salt) and tobacco, its before the consumer uses by solvation.Solvation makes described gel combination form the solid that can be placed in the mouth.Typically, the user is put in the described dry mixing mixture of gel component in the mold, and is incorporated as the solvent of moisture or non-water.Described then mixture fast hydrating, thus the gel that the shape with described mold is cured formed.Can use solvation liquid to give described composition with fragrance or other tastes or mouthfeel characteristic.Perhaps, the consumer can be put in described dry mixing mixture in the mouth and dissolve.Described solvent can give described composition with fragrance or color.

Gel embodiment

Embodiment A R. gel bead

4% solution and the 20g tobacco of 100g CMC-7MF are mixed.Drop is deposited to water miscible edible trivalent salt (as AlCl ₃Or Al ₂(SO ₄) ₃)) 5% solution in.With air drying or gentle oven drying drying is carried out on the surface of drop then.

100g2% kappa carrageen glue and tobacco mixed and be heated to 180-190_.Drop deposits in the cold soln of 5%KCl.

Under 150-170_, 100g4% medium-viscosity mosanom and tobacco are mixed.Drop is deposited to the edible divalent salts (as CaCl ₂Or calcium citrate) in 5% cold soln.

Can deposit to by drop in the low speed liquid stream of warm gelatin solution (for example 130_) of dilution and make the bead that comprises gelatin wall and tobacco slurries center cold tobacco slurries (for example 60_).Apply the outside of cold drop with described warm gelatin, and when described gelatin cooling and curing, around described liquid center, formed gelatin wall.

From described solution, obtained bead again by standard method.

The solid gel of the good to eat disintegration of embodiment A S.

10g gelatin and 90g water are mixed and be heated to 140_ with the dissolving gelatin.Adding 20g tobacco also is injected in the mold.Can be by replacing with 6g gelatin and 4g agar and being heated to 190_ to dissolve the intensity that increases described gel.

Table A S1 has shown the exemplary composition that is used to prepare good to eat disintegration gel of the present invention.

Table A S1

	Embodiment 1 (part)	Embodiment 2 (part)
	Embodiment 1 (part)	Embodiment 2 (part)	Gelatin	8	6
Tobacco	40	40	Gelatin	8	6
Tobacco	40	40	Spices	2	2
Insoluble fiber	18	18	Spices	2	2
Insoluble fiber	18	18	Sweetener	0.2	0.2
Agar	4	6	Sweetener	0.2	0.2
Agar	4	6	Soluble fibre	15	15
Anticorrisive agent	0.1	0.1	Soluble fibre	15	15
Anticorrisive agent	0.1	0.1	Water	200	200

The exemplary insoluble solids gel of embodiment A T.

Following table and describe and to have shown the exemplary composition that is used to prepare insoluble gel of the present invention, gel that promptly can not mouthful disintegration.

Table A T1. carrageenan gel

	Part
	Part	Kappa carrageen glue	8
Water	240	Kappa carrageen glue	8
Water	240	Tobacco	54
Sweetener	0.5	Tobacco	54
Sweetener	0.5	Soluble fibre	27
KCl	1.5	Soluble fibre	27

Adding KCl and fully mixing the back in the described composition of 180_ curtain coating.

Table A T2. alginate jelly

	Part
	Part	Mosanom	10
Water	240	Mosanom	10
Water	240	Tobacco	54
Sweetener	0.5	Tobacco	54
Sweetener	0.5	Soluble fibre	27
CaCl ₂	1	Soluble fibre	27

Adding CaCl ₂The back is in the described composition of 180_ curtain coating.

Table A T3. carboxymethyl cellulose gel

	Part
	Part	CMC-7MF	10
Water	240	CMC-7MF	10
Water	240	Tobacco	54
Sweetener	0.5	Tobacco	54
Sweetener	0.5	Soluble fibre	27
Al ₂(SO ₄) ₃	1	Soluble fibre	27

Adding Al ₂(SO ₄) ₃The back is in the described composition of 180_ curtain coating.

Embodiment A U. sol gel

3.9% kappa carrageen glue and 51.0g tobacco that 416g is moisture mix.Follow stirring that described solution is heated to 180_-190_, then described solution is deposited in the mold with desired shape.In case desired tobacco concentration and gel consistency (gel consistency) are taken out the gained solid forms and are dried in cooling from mold.

In other method, greater than in the 1000ml rustless steel container that is equipped with overhead blender, mixing rod and hot plate, adding 400ml water under the 200_.Water is continued to stir and heating and adding 16.0g kappa carrageen glue (Gelcarin GP 812, FMC Biopolymer) in 2 minutes.The gained mixture was stirred 20 minutes in addition, or dissolve fully, in described homogeneous solution, add tobacco then, keeping under the optimum temperature of 180_ the other stirring of described mixture 2 minutes up to all kappa carrageen glue.Under strong agitation, in this solution, add the sucralose and the 7.0g cinnamon oil (Wixon Industries) of 0.8g powdered.Stirred in addition then 1 minute, and used pipette (internal diameter is 0.5cm) the gained mixture to be transferred to fast in the metal mold of teflon-lining to obtain desired shape.Behind the cool to room temperature, the gained gel taken out from mold and at room temperature carry out air dry 1 hour-a couple of days, up to having obtained desired gel consistency.

Table A U1. carrageenan gel

	Umber
	Umber	Kappa carrageen glue	16
Water	400	Kappa carrageen glue	16
Water	400	Tobacco	51
Sweetener	0.8	Tobacco	51

Cinnamon oil

7.0

Embodiment A V. sol gel

20% gelatin and 33g tobacco that 100g is moisture mix.Follow stirring that described solution is heated to 140_-150_, then described solution is deposited in the mold with desired shape.Depended on desired solidness subsequently freezing several minutes-several days, and the gained solid forms was taken out and is dried to desired tobacco concentration and gel consistency from mold.

In other method, under 140_, in the 400ml rustless steel container that is equipped with overhead blender, mixing rod and hot plate, add 80ml water.Water is continued to stir and heating and adding 20.0g gelatin (Type A 250 Bloom 40 Mesh, Gum Technology) in 2 minutes.The gained mixture was stirred 5 minutes in addition, or, in 2 minutes, add the 33g tobacco then in batches up to the gelatin dissolving.Described mixture was stirred 1 minute in addition, the sucralose and the 1.0g Fructus Piperis peppermint oil that add the 0.3g powderization then are (refining, and keeping under the temperature of 140_ Blend SX 0910001, Essex Labs), with other 1 minute of gained mixture strong agitation.Use pipette (internal diameter is 0.5cm) the gained mixture to be transferred in the metal mold of teflon-lining to obtain desired shape.Behind the cool to room temperature, the gained gel is taken out from mold, and depend on the desired solidness of finished parts and under 40_, described gelatin is solidified 1 hour-a couple of days.

Table A V1. gelatin gel

	Umber
	Umber	Gelatin	20
Water	80	Gelatin	20
Water	80	Tobacco	33
Sweetener	0.3	Tobacco	33
Sweetener	0.3	Fructus Piperis peppermint oil	1.0

Embodiment A W. gel bead

By the 12g mosanom being joined in the 288g water that is heated to boiling, subsequently by on heating plate, water being stirred and continuing heating 30 minutes or become uniformly 4% solution that (liquid storage A) makes mosanom (Keltone LV, International Specialty Products) up to solution.By the 33.5g sodium phosphate dibasic heptahydrate is dissolved in the 200ml water, carry out gained solution warm and stirring, up to the salt dissolving, water is regulated described solution makes the 0.50M of sodium hydrogen phosphate to 250ml second kind of solution subsequently.In the 0.50M of the 100g disodium hydrogen phosphate aqueous solution, add the 20g tobacco, and gained solution is stirred 5 minutes (liquid storage B).4% aqueous solution (liquid storage A) that in 50g gained tobacco slurries (liquid storage B), adds the 50ml mosanom, and with gained mixture stirring 5 minutes.For flavouring, in gained tobacco/mosanom slurries (solution C), add the sucralose and the 0.80g Fructus Piperis peppermint oil (refining, Blend SX 0910001, Essex Labs) of 0.20g powdered, and stir described mixing 2 minutes.

For preparation gel bead from solution C, under agitation pass through 5g CaCl ₂Join in the 95g water and dissolve (solution D) fully, and make 5% aqueous solution of CaCl2 up to described calcium chloride.Use pipette from 10 inches height, solution C to be added drop-wise to the solution D then.The external coating of each drop is exposed in the solution D and is cured, and has formed solid gel shape external coating, and it has the liquid center of the bottom that sinks to calcium chloride solution.Described gel bead is retained in the calcium chloride solution 2-4 minute, takes out the line space of going forward side by side air dry number minute.

Solution A

	Umber
	Umber	Mosanom	12
Water	288	Mosanom	12

Solution B

	Umber
	Umber	Sodium phosphate dibasic heptahydrate	13.4
Water	86	Sodium phosphate dibasic heptahydrate	13.4
Water	86	Tobacco	20

Solution C

	Umber
	Umber	Solution A	50
Solution B	50	Solution A	50
Solution B	50	Sucralose	0.2
Fructus Piperis peppermint oil	0.8	Sucralose	0.2

Solution D

	Umber
	Umber	Calcium chloride	5
Water	95	Calcium chloride	5

But consumption unit (consumable units). also can be used as consumption unit and prepare composition of the present invention.These units can pack as edible or unedible material.In one embodiment, but described consumption unit comprises tobacco (as smokeless tobacco) or tobacco compositions, as thin slice, tablet, bead, particle or other tobacco compositions and the packaging material such as the pouch of description described here.In one embodiment, described packaging material can be used as adhesive so that described composition becomes one, as make a plurality of tablets, bead, thin slice etc. become one.Perhaps, the salable described composition of described packaging material is as loose tablet, bead, thin slice etc.Described composition also can comprise liquid such as tobacco slurries.Described packaging material can be or for mouthful disintegration.Can use mouthful disintegration packaging material to be used for sealing moisture or on-aqueous liquid.When using with the water soluble package material when liquid, aqueous, described liquid comprises the reagent that is used for preventing described packaging material dissolving.Exemplary agents comprises sugar, salt and other hydrophilic reagents, described hydrophilic reagent can be fully in conjunction with water so that the water activity is reduced to the level that water no longer influences and dissolve described water soluble package material.The also salable moldable tobacco compositions that meets mouth or in mouth, keep its shape of described packaging material.In one embodiment, the packaging material of good to eat disintegration have sealed smokeless tobacco, as at when dissolving perceptible snuff or tobacco (as granularity less than 80 μ m).The smokeless tobacco composition of good to eat disintegration can be incorporated in the consumption part packing, on continuous thermoforming or horizontal versions agent/filling/water-tight equipment or use other suitable package equipment, form this packing according to the edible film (it can contain or not contain tobacco) of subject technology preparation.Consumption unit also can comprise two or more independently tobacco package parts, as all being included in the bigger packing, and a part that comprises other, or these parts do not comprise another part.When using a plurality of part, any two can have identical or different spices, colorant, the agent of tobacco form or disintegration rate.

The exemplary packet package material comprise from based on form agent such as HPMC, CMC, pectin, alginates, amylopectin and as those other commercial available edible film described herein form the film composition of polymer and the film that forms.Other packaging material can comprise from gelatin, HPMC, starch/carrageenan or other commerce can get material and the pre-formation capsule that makes.These packaging material can comprise the tobacco as composition.Not the packaging material of good to eat disintegration can comprise fabric or non-woven, coating or do not have coated paper, or the sponge plastics film that obtains of perforation or alternate manner.Packaging material are also coloured.Exemplary consumption unit comprises those that form by any method that is used for commercial packing, commercial packing method such as bubbling plastic gasket packing and stik-pak (as the inner wrapping that forms on vertical in form agent/filling/sealing and packing machine).

The embodiment of consumption unit

But following description provides the exemplary composition that is used to prepare consumption unit of the present invention.

Embodiment A X. seals the film or the capsule of bead, powder, tablet etc.

Available film or capsule are sealed any composition as described herein.Described encapsulation agent can provide color, stability (as during storing, handle or consuming), or organoleptic attribute (as fragrance, sweet taste, sense of smell or mouthfeel).Described encapsulation agent also can comprise tobacco.

Designed the vacuum forming instrument, it has a series of cavity, and described cavity is formed as that to have diameter be 3/4 ^ThThe inch and the degree of depth are 3/8 ^ThThe circle of inch.Prepared the film that has or do not have tobacco as composition as described herein.These films are incorporated in the vacuum forming machine with vacuum forming mould.Being put in described film above the heating element heater and being warming to temperature is 200_.Then described film is placed on the described vacuum forming mould fast, and inhales into vacuum so that film is drawn in the described cavity.Cool off described film then with solidification shape.Then tobacco powder is incorporated in each cavity.Select prepared second diaphragm that has or do not have tobacco and the thin layer of water applied (by described surface) to produce the adhesive surface of thickness with the wet felt Wiping film.Described thickness surface is put in the top of described formed sheet, and wherein each cavity has been full of tobacco product.But described sheet material is pressed onto together to form airtight consumption unit.From described vacuum forming sheet material, cut each cavity then to produce single unit.Unit is put in the mouth, and wherein said film disintegration also disperses described tobacco in the oral cavity.

The tobacco particle of embodiment A Y. in water-soluble bag

Smokeless tobacco particle or powder such as snuff can be put in the bag of water-disintegratable.In the time of in being put in mouth, disintegration takes place in described bag after the prescribed time-limit.Described bag can comprise the single part of supplies of tobacco.Also can comprise other additives as described herein.In case described packaging material disintegration, described tobacco also can the oneself adhere to as moldable embolism (moldable plug).

Use film as described herein can form the bag of described disintegratable.Can use packaging facilities that commerce can get such as vertical in form agent/filling/sealing machine (vertical form/fill/seak machines) (as the rod package packing machine), horizontal versions agent/filling/sealing machine, flow wrap machines (flow wrappers), thermoforming machine (bubbling plastic gasket package packing machine) and known other equipment of prior art with as described in film form bag.

The tobacco particle of embodiment A Z. in film/fabric laminate.

Smokeless tobacco particle or powder can be put in from the bag that the packaging material of opening or high hole form, described packaging material such as fabric, paper or plastic foil have been laminated into it water miscible packaging material film.During storing and handling, described water soluble film layer can provide protection and prevent that tobacco from moving through the opening of non-dissolved material described tobacco content.In case described bag is put in the mouth described water soluble film layer dissolving or disintegration.

Embodiment B A. comprises the film bag of tobacco

The film that use is described in film embodiment N, O, P and Q prepares the band that comprises tobacco.Cut off the individual unit of about 1 inch * 1_ inch from each sheet material of obtained film.Folding along the longitudinal described unit also uses Clamco Model 210-8E impulse sealer to carry out heat seal.Also seal an end of described formation unit in the same way.The perfuming tobacco particle is fed to the inside of described formation pouch, and carries out finally sealed as described to seal described pouch.Comprise pouch disintegration in 20 seconds-1 minute in mouth of tobacco, discharge the content of described bag.

Insoluble matrix. also tobacco can be applied or is collected in the inside of insoluble matrix.When forming film, tobacco can disperse to form slurries in the aqueous solution of form agent; These slurries can be coated on the insoluble matrix or be used for the insoluble matrix of saturated porous.Described slurries can be become solvable or insoluble gel then, or it be carried out simple dry to form coating.When will apply/when the part of saturated insoluble matrix is put in the mouth, by dissolving, chew or the leaching of organ sensation composition has taken place other modes.In one embodiment, will be incorporated into the tobacco in the form agent in the porous matrix, in open-cell polyurethane foams or high fluffy polyester non-woven structure.Described insoluble matrix can all be put in the mouth, or can handle on rod or other handles, and its part during consuming is retained in a mouthful outside.In another embodiment, tobacco in the form agent mixes with inconsistent liquid, as the dispersion of the Brazil wax in water, it is put in the mold, and cooling is separated to cause rapidly, thereby in wax shape structure, described tobacco slurries have been disposed.These matrix also can be masticable.

The form agent that is used for described tobacco is retained in described insoluble matrix can comprise any film that forms polymer as described herein, gel quav system as described herein and any coating material as described herein.

Insoluble matrix embodiment

Embodiment B B. polyurethane foam A.

To comprise as described herein the film-forming composition of fine grinding tobacco and be used for saturated open-cell polyurethane foams (Stephenson ﹠amp; Lawyer, Inc.Grand Rapids, piece MI) (as 12 inches * 12 inches * 1 inch).Be put in described saturated foam on the metal tray and be put in and be made as in the 175_ air circulation experiment baking oven 1 hour.When described foam is taken out from described baking oven, the be dried coating in all slits of having formed even covering polyurethane foam of the composition that comprises tobacco.Described coating foam is cut into size be fit to be put in piece (as 1 inch * 1 inch * 1 inch) in the mouth.After the use, from mouth, take out described polyurethane foam and abandon.

Embodiment B C. polyurethane foam B.

To comprise the mosanom of fine grinding tobacco as described herein and calcium salt gel combination and be used for saturated open-cell polyurethane foams (as 12 inches * 12 inches * 1 inch).Described alginate jelly is remained under the temperature of 180_ to solidify the morning that prevents described gel.Hot alginate jelly is poured on the described polyurethane foam that is put on the metal tray, and in the refrigerator of 40_, cools off to solidify described gel fast.Then foam is put in to be made as in the 175_ air circulation experiment baking oven and with the described gel of dry tack free and based on the gel dry weight moisture was reduced to 50% in 10 minutes.Make the gel-filled space in described polyurethane foam of part drying.Described foam cut into piece and put and mouthful in.By the described gel of drying to than low moisture content (as based on as described in the gel dry weight be 10%) obtain other embodiment of the gel in insoluble matrix.The gel that comprises tobacco has demonstrated robustness, rubber-like structure in foam matrix, and can be rehydrated lentamente when chewing when being put in a mouthful neutralization.After the use, from mouth, take out described polyurethane foam and abandon.

Hollow shape. as mentioned above, the film or the thin slice of material can be packed, extrude, blowing or other moulding to be to form pipe, suction pipe or other hollow shape.Exemplary film or sheet material are disclosed in the membrane portions here.Described hollow shape can be single or multiple lift.When using multilayer, some can comprise tobacco, and other comprise colorant, spices, sweetener or other compounds as described herein.During also different layers can being used to handle stability or in order during consuming, to control disintegration.The hollow shape that spiral twines can need adhesive (as CMC or guar gum) to unclamp with prevention as pipe or suction pipe.Described layer in the multilayer hollow shape can comprise identical or different colorant or spices, and this layer can identical or different speed carry out disintegration.With film, also tobacco can be placed in one or more layers, or be placed in the middle of the layer with mezzanine configurations.Described hollow shape can comprise that also disintegrant is to accelerate disintegration.

That above-mentioned composition can be hollow or be filled.Described filler can comprise tobacco, spices, sweetener, odor masking agent or colorant.The spices of described filler or colorant and hollow shape identical or different.Described filler typically is gel (solid or flowable), but also can be mechanical rigid or can form by powder or other product form agent.Exemplary filler material comprises gel as described herein.Hollow shape also available than described shape disintegration faster composition fill, as being used for providing tobacco at different time based on disintegration rate.

In one embodiment, tobacco core (as preparing with tobacco and form agent) can be expressed into the co-extrusion head mold from list or double screw extruder.In list that separates or double screw extruder, can with water-soluble, thermoplasticity is outer (as preparing with form agent and spices) be incorporated into as described in the co-extrusion head mold with generation coating rod.Available formulation based on the hydroxypropyl cellulose of extruding between the temperature of 220-370_ (HPC) provides typical heat plasticity skin.In addition, rigidity is extruded tobacco rod and is become the core that the packaging material film is surrounded.

In one embodiment, the thermoplasticity formulation that comprises hydroxypropyl cellulose, tobacco, spices and sweetener can carry out blowing to form hollow shape.

In another embodiment, film described herein can be used to prepare in addition spiral and twine suction pipe and/or rod.Cut out from every of film of preparation and to be about 10 inches * 3/4 inch film bar.Downcut the paper slip of same size and the stainless steel mandrel that spiral twines 3/16 inch diameter.Tie up with adhesive tape at every end and to make the fastening mandrel of described paper.Twine described paper with film bar spiral in the same manner, overlapping 1/16 inch of each spiral.On each was overlapping, the gum arabic solution with 30% made described film bar oneself bonding.Repeat described method with other two membranes.Described mandrel and the new spiral stretch film suction pipe/rod that forms are put in 75 ℃ side to be swept in the forced ventilation baking oven (VWR model 1330FM) and to carry out drying in 15 minutes.In case from described baking oven, take out, described spiral is twined suction pipe/rod take off, and paper " core " is taken out from the inside of described suction pipe/rod from described mandrel.Gained suction pipe/rod is cut into a plurality of sizes.

For example, the film that comprises tobacco described of the perfuming tobacco film that uses embodiment N to be used for rod/parcel/bag shape/vacuum forming has made spiral winding suction pipe/rod goods.One deck of the film that comprises embodiment N, two-layer and suction pipe/rod goods of three layers have been made as described.When being put in it in mouth, described suction pipe/rod disintegration gradually in 1-5 minute.

In another embodiment, use has made suction pipe/rod goods as the two membranes of describing among the embodiment N.Perfuming/the Coloured film that is used for rod/packing/pouch that in the top of described suction pipe/rod or periphery provide trilamellar membrane-as embodiment O, has prepared.From the film of embodiment O is that red, Chinese cassia tree perfuming does not contain tobacco.When being put in this suction pipe/rod in the mouth, disintegration gradually in 1-5 minute.

In another embodiment, use and to be used for the trilamellar membrane that the peach perfuming film of rod/packing/pouch describes as embodiment P and to have made suction pipe/rod goods.Film from embodiment P comprises tobacco powder and peach mud.As above prepared suction pipe/rod.Described suction pipe/rod is disintegration gradually in 1-5 minute.

Still in another embodiment, use has made suction pipe/rod goods as the trilamellar membrane of describing among embodiment N and the embodiment Q.Used the monofilm that comprises tobacco that in embodiment N, prepares.To be wrapped on the ground floor of film as the second layer opaque white color film for preparing among the embodiment Q and be offset 1/8 ^ThInch.The 3rd layer of preparing among the embodiment N contained the tobacco film to be wrapped on the second layer and to be offset 1/8 once more ^ThInch.This effect provides the suction pipe/rod of the spiral winding with striped outward appearance.In the time of in being put in mouth, described suction pipe/rod is disintegration gradually in 1-5 minute.

In another embodiment, use method among the embodiment A Q that is similar to profiled member to make and have the hollow tobacco suction pipe of diameter range as the 1/8-1/4 inch.Yet, in the preparation of described suction pipe, used the pipe punch die.Described suction pipe is slowly disintegration in 5-10 minute in mouth.Use known method of the prior art (as co-extrusion), prepared similar articles with filler.

D. modification

Can carry out modification to any tobacco compositions described herein in many ways.For example, composition can be applied into single or multiple lift.This coating is used for as processing, disintegration rate, taste or color.Exemplary coatings comprises HPMC.Can use the known method of prior art, as spraying, brushing, roller coat, scraping blade curtain coating, seam be coated with, squeezing and coating, hot melt deposition, precipitation particulate or thin slice and other typical methods, coating or decorative pattern are applied on the surface of described film.Coating can be lacklustre or glossiness.Coating can comprise as colorant described herein, spices or odor masking agent.Colorant in described coating, sweetener or taste masked agent can be with following composition identical or different.In addition, a plurality of coatings also can comprise identical or different colorant, spices, sweetener or odor masking agent.Described coating also can be different with following composition speed generation disintegration.For example, the disintegration of coating can be faster than the composition below described to provide a burst of spices or other organoleptic ingredients.Mouthful disintegration coating also can be positioned at can not mouthful disintegration composition above.Coating that can not mouthful disintegration can be positioned at can mouthful disintegration composition above, and can be as removing this coating by chewing.Also can use coating to prevent the evaporation of the volatile component in the composition and prevent the machinery dipping of composition before use.Coating also can comprise tobacco.

Also pattern can be printed on the surface of composition.Printed patterns also can comprise dust or intersperse compound on the surface of composition.Described pattern can be random or for styles design as sign.Can use all printing processes known in the prior art, as offset printing, aniline printing, intaglio, ink-jet, laser, serigraphy and other typical methods.As described herein, described printed patterns can comprise or not comprise colorant, spices, sweetener or odor masking agent.Composition below described colorant, condiment, sweetener or odor masking agent in pattern can be same or different from.In addition, a plurality of patterns also can comprise identical or different colorant, spices, sweetener or odor masking agent.The pattern of described printing also can comprise tobacco as up to 1-99%, is preferably 10-50%.This pattern on the percentage mode or on the absolute sense comparable composition below described comprise more tobacco.

Also thin slice can be joined in the composition described here.Thin slice can be mixed in the described composition, can be placed in the space of described composition, or can be placed on the surface, as adhering to by coating.As described here, thin slice can comprise or not comprise colorant, spices, sweetener or odor masking agent.Colorant in described thin slice, spices, sweetener or odor masking agent also can with described below identical or different in the composition.In addition, a plurality of thin slices also can comprise identical or different colorant, spices, sweetener or odor masking agent.Thin slice also can comprise tobacco as up to 99%, preferably up to 50%.Can make thin slice by standard film formation technology as described herein.Thin slice the agent of percentage form or on absolute sense comparable composition below described comprise more tobacco.

In case made described printing, coating or decorating film, can apply additional tunic to cover, to protect and to seal described printing, coating or combination with decorative surfaces.

Composition of the present invention agent in a variety of forms carries out moulding, as workshop (plant) and geometry (as circle, square, rectangle triangle, ellipse, octagonal etc.).In addition, composition can comprise embossing pattern (pattern in relief) (erect image or negative-appearing image) from the teeth outwards.This pattern can be styles design as sign.

The present invention has also estimated complex composition, promptly comprises the composition of two or more dissimilar products described here.For example, profiled member can comprise the zone of gel combination, as has multiple spices.In another embodiment, tablet can by gel institute around.Complex composition also can have different disintegration rates.

E. pack

Single composition can be packed, the content of composition is suitable.Preferably, composition can be stored in the water-proof container, and is stable between 40-120_.When storing composition dry typically, flexible with non-adhesive.Perhaps, can between supplies, use non-sticky barrier such as plastic foil or paper to come packaging compositions.Can also provide composition, separate single supplies thus with the bulk form agent.

In another embodiment, described packing is fluid-tight and water-fast, and but the tobacco in liquid, slurries or the agent of flow-gel form is in the inside of described packing such as easy compression plastics package, bellows (bellow) or spray bottle, and can be assigned in the mouth from described packing.Compressible described bellows is to be used for a mouthful use.Prepared the solution or the slurries that in plastic foil box container or other similar consumer package containers, use, wherein described liquid has been injected in the mouth by pushing described packing.Thixotropic polymerized thing is mixed the more high-viscous solution that is applicable to other containers with preparation with tobacco and other compositions.Tobacco particle can be more large scale, but must be still enough little of to pass the opening of described container.For spray bottle, in described bottle, comprise stable tobacco slurries; Tobacco particle is of a size of and can passes nozzle and non-occlusion of openings; With the described tobacco slurries of in the oral cavity, directly spraying.By thixotropic polymer such as xanthans, exocellular polysaccharide or dextran are dissolved in the water, and tobacco particle are suspended in the solution of low viscosity (as＜50 centipoises) and make the liquid spraying.Can in described solution, add other compounds such as spices, sweetener and dispersant.With tobacco particle be ground to certain particle size (as＜80 microns) make as described in homogeneous solution can pass the opening of spray bottle.Tobacco is extruded or be used for emitting to available other mode of other packings in mouth.

F. solution

Following tobacco solution can be contained in any composition as described herein.

Embodiment B D. sprayable solution

By 0.2g xanthans (from the Kelzan of C.P.Kelco) is blended in the 78.6g cold water, vigorous stirring 30 minutes and make solution simultaneously.In this solution, add tobacco, 0.2g sucralose and the 2g cinnamon flavor of 20g fine grinding, continue vigorous stirring simultaneously.It is 50 centipoises that water is adjusted to viscosity with described solution viscosity.

The dense thick solution of Embodiment B E.

(from the Kelzan of C.P.Kelco) mixes with 76.8g cold water with the 1g xanthans, simultaneously violent mixing 30 minutes and make solution.In this solution, add the thin tobacco of 20g, 0.2g sucralose and 2g cinnamon flavor, continue violent the mixing simultaneously.Solution viscosity is 1,500 centipoise.

Embodiment B F. slurry

(available from Hercules, the CMC 7MF of Inc.) joins in the mixture of 35.8g cold water and 40g glycerine with the moderately viscous carboxymethyl cellulose of 2g, simultaneously violent mixing 30 minutes and make slurry.In this mixture, add the thin tobacco of 20g, 0.2g sucralose and 2g cinnamon flavor.Prepared the high shear sensitivity underflow.This slurry can be incorporated in pipe or other compressible package, wherein reduce the viscosity of described slurry, make it to flow from the shearing force of extruding.

Other embodiments

The description of specific implementations of the present invention is used for illustrative purpose.Particular form agent as described herein is neither at large neither be used for limiting the scope of the invention.Although, be appreciated that for a person skilled in the art and can make the multiple modification that does not break away from as under the spirit and scope of the present invention of setting forth in the claim by having described the present invention with reference to a plurality of embodiments.All patents, patent application and the publication of institute's reference are here incorporated into to come in by reference.Other embodiments within the scope of the claims.

Claims

1. comprise the tobacco compositions of tobacco and form agent, wherein said composition is easy to disintegration in mouth.

2. the described composition of claim 1, it comprises the composition of listing in the Table I

Table I Composition Percentage Water-soluble polymer 10-70 Tobacco 1-90 Spices 1-40 Sweetener 0.2-6 Fiber 2-40 Plasticizer 1-40 Surfactant 0.05-5 Starch/maltodextrin 1-40 Lubricant 0.5-10

3. the described composition of claim 1, it comprises the composition of listing in the Table II

Table II Composition Percentage Water-soluble polymer 20-45 Tobacco 20-40 Spices 5-15 Sweetener 2-5 Fiber (solvable or soluble) 5-20 Plasticizer 5-15 Surfactant 0.1-1 Starch/maltodextrin 10-20 Lubricant 1-3

4. the described composition of claim 1, wherein said composition is a film.

5. the described composition of claim 1, wherein said composition comprises individual layer.

6. the described composition of claim 1, wherein said composition comprises the foamed layer.

7. the described composition of claim 1, wherein said composition comprises multilayer.

8. the described composition of claim 7 will be two-layer at least laminated together wherein.

9. the described composition of claim 7, wherein said tobacco is placed between two layers.

10. the described composition of claim 7, two-layer at least different spices or the colorant of comprising in the wherein said multilayer.

11. the described composition of claim 1, the disintegration in of wherein said composition less than 2 minutes.

12. the described composition of claim 1, the thickness of wherein said composition are 0.001-1.0mm.

13. the described composition of claim 1, wherein said form agent comprises carboxymethyl cellulose (CMC), hydroxypropyl cellulose (HPC), hydroxyethylcellulose (HEC), hydroxypropyl methylcellulose (HPMC), methylcellulose (MC), starch, amylose, high amylose starches, the high amylose starches of hydroxypropylation, konjac, karaya, collagen, inulin, soybean protein, lactalbumin, casein, wheat gluten, kappa carrageen glue, the ι carrageenan, the λ carrageenan, alginates, propylene glycol alginate, xanthans, dextran, the Aureobasidium pullulans glycan, the curdled milk glycan, exocellular polysaccharide, locust bean gum, guar gum, tara gum, gum tragacanth, pectin, agar, zein, karaya, gelatin, the Asiatic plantain kind, chitin, chitosan, gum arabic (Arabic gum), shellac, PVP, PEO or polyvinyl alcohol.

14. comprise the tobacco compositions of tobacco and form agent, wherein made described composition as tablet.

15. the described composition of claim 14, it comprises the composition of listing in the Table III

Table III Composition Percentage Water-soluble polymer 0-70 Tobacco 1-70 Perfumery oil 0.5-4.0 Artificial sweetener 0.05-0.4

Sugar 1-80 Maltodextrin 0-50 Disintegrant 0.1-15 Starch 5-80 Releasing agent 0.1-2.0 Emulsifying agent 0.1-5.0

16. the described composition of claim 14, wherein said tablet are supper-fast disintegrations.

17. the described composition of claim 14, wherein said tablet is quickly disintegrated.

18. the described composition of claim 14, wherein said tablet are slow disintegrations.

19. the described composition of claim 14, wherein said tablet is masticable.

20. the described composition of claim 14, wherein said tablet full-size is 2-4mm.

21. the described composition of claim 14, wherein said tablet is shaped to disk or bead.

22. the described composition of claim 14, it further comprises non-water-soluble coating and water-soluble coating, and wherein said non-water-soluble coating is configured between described form agent and the described water-soluble coating.

23. the described composition of claim 22, wherein said water-soluble coating provides mechanical stability.

24. comprise the tobacco compositions of a plurality of tablets of claim 20.

25. the described composition of claim 24, wherein said a plurality of tablets comprise multiple spices or colorant.

26. comprise the Cigarette with protective device grass composition of tobacco and form agent, wherein said composition is moulding.

27. the described composition of claim 26, it comprises the composition of listing in the Table IV

Table IV Composition Part Tobacco 1-80 Spices 0.5-4 Insoluble fiber 4.5-36 Water-soluble polymer 1-50 Filler/disintegrant 1-50

Artificial sweetener 0.05-5 Dispersant 0.1-20

28. the described composition of claim 27, it comprises the composition of listing in the Table V

Table V Composition Part Tobacco 30-50 Spices 2.5-3 Insoluble fiber 22.5-27 Water-soluble polymer 5-20 Filler/disintegrant 10-30 Artificial sweetener 0.1-2 Dispersant 0.1-2

29. the described composition of claim 26, it comprises the composition of listing in the Table VI

Table VI Composition Part Tobacco 1-80 Spices 0.5-4 Insoluble fiber 4.5-36 Water-soluble polymer 1-50 Filler/disintegrant 1-50 Artificial sweetener 0.05-3 Dispersant 0.1-20

30. the described composition of claim 29, it comprises the composition of listing in the Table VII

Table VII Composition Part Tobacco 20-50 Spices 1-3

Insoluble fiber 9-27 Water-soluble polymer 5-25 Filler/disintegrant 10-30 Artificial sweetener 0.1-1 Dispersant 0.1-2

31. the described composition of claim 26, it comprises the composition of listing in the Table VIII

Table VIII Composition Part Tobacco 10-80 Plasticizer 1-20 Water-soluble polymer 10-80 Filler 0-60 Stabilizing agent 0.1-0.5

32. the described composition of claim 26, it comprises the composition of listing among the Table I X

Table I X Composition Part Tobacco 25-80 Plasticizer 1-20 Water-soluble polymer 20-50 Filler 0-30 Stabilizing agent 0.2-0.4

33. the described composition of claim 26, the water content of wherein said composition are 2-50%.

34. the described composition of claim 26, wherein said composition are good to eat disintegrations.

35. the described composition of claim 34, the disintegration in 1-60 minute of wherein said composition.

36. the described composition of claim 26, the size that wherein makes described composition is for partly in mouth.

37. the described composition of claim 26, wherein said composition has the full-size less than 6 inches.

38. the described composition of claim 26, wherein said composition has the full-size less than 3 inches.

39. the described composition of claim 26, wherein said composition be shaped as tubulose, toothpick, rod, helical form or rod.

40. the described composition of claim 26, it further comprises one or more zone of dispersions, and wherein each zone comprises spices or colorant.

41. the described composition of claim 40, wherein each zone comprises that rope and each rope are intertwined and forms described composition.

42. the described composition of claim 40, wherein at least one zone comprises spices or the colorant different with described form agent.

43. the described composition of claim 40, it comprises at least two zones, and wherein each zone comprises different spices or colorant.

44. the described composition of claim 26, wherein by injection moulding, compression moulding, overmolded, extrude or the described composition of slurry method moulding.

45. comprise the Cigarette with protective device grass composition of tobacco and gel form agent.

46. the described composition of claim 45, wherein said gel form agent comprises kappa carrageen glue, mosanom, carboxymethyl cellulose, gelatin, pectin, agar or starch.

47. the described composition of claim 45, the center has been sealed in wherein said gel form agent.

48. the described composition of claim 45, wherein said form agent comprises polymer and crosslinking agent.

49. the described composition of claim 48, wherein said polymer comprise that carrageenan and described crosslinking agent comprise univalent cation.

50. the described composition of claim 49, wherein said univalent cation is a potassium.

51. the described composition of claim 48, wherein said polymer comprise that alginates and described crosslinking agent comprise bivalent cation.

52. the described composition of claim 51, wherein said bivalent cation is a calcium.

53. the described composition of claim 48, wherein said polymer comprise that carboxymethyl cellulose and described crosslinking agent comprise Tricationic.

54. the described composition of claim 53, wherein said Tricationic is an aluminium.

55. the described composition of claim 48, wherein said polymer comprise that pectin and described crosslinking agent comprise bivalent cation.

56. the described composition of claim 55, wherein said bivalent cation is a calcium.

57. the described composition of claim 45, wherein said form agent comprises gelatin.

58. the described composition of claim 48, wherein said form agent comprises gelatin and gum arabic.

59. the described composition of claim 47, wherein said center comprises solid material.

60. the described composition of claim 47, wherein said center comprises fluent material.

61. the described composition of claim 60, wherein said fluent material is moisture.

62. the described composition of claim 60, wherein said fluent material is water-free.

63. the described composition of claim 60, wherein said fluent material is uneven.

64. the described composition of claim 62, wherein said not hydrous material comprises ethanol or oil.

65. the described composition of claim 47, wherein said center comprises tobacco.

66. the described composition of claim 47, wherein said center comprises the tobacco slurries.

67. the described composition of claim 47, wherein said center comprise tobacco and sugar or salting liquid.

68. the described composition of claim 47, wherein said center does not comprise tobacco.

69. the described composition of claim 47, wherein said center comprises colorant, sweetener, spices or odor masking agent.

70. the described composition of claim 47, wherein said center comprise and the different colorant of described form agent.

71. the described composition of claim 47, wherein said center comprise and the different spices of described form agent.

72. the described composition of claim 47, wherein said center have and the different disintegration rate of described form agent.

73. the described composition of claim 45, wherein said composition are good to eat disintegrations.

74. the described composition of claim 45, wherein said composition is masticable.

75. the described composition of claim 45, wherein full-size is 15mm to the maximum.

76. the described composition of claim 45, wherein full-size is 5mm to the maximum.

77. the described composition of claim 45, wherein said form agent is a gelatine capsule.

78. comprise the tobacco compositions of the composition of multiple claim 45.

79. the described composition of claim 78, wherein said multiple multiple spices or the colorant of comprising.

80. the described composition of claim 45, it further comprises a plurality of zone of dispersions of gel, and wherein each zone comprises spices or colorant.

81. the described composition of claim 80, wherein at least two zones have different spices or colorant.

82. the described composition of claim 80, at least two of wherein said zone are common center arrangement.

83. the described composition of claim 45, wherein said form agent are not good to eat disintegrations.

84. the described composition of claim 45, wherein said form agent comprises polymer and crosslinking agent.

85. the described composition of claim 84, wherein said polymer, tobacco and crosslinking agent are solvations not, wherein the adding of solvent makes described polymer and crosslinking agent form insoluble gel.

86. the described composition of claim 85, wherein said polymer comprise that carrageenan and described crosslinking agent comprise univalent cation.

87. the described composition of claim 86, wherein said univalent cation is a potassium.

88. the described composition of claim 85, wherein said polymer comprise that alginates and described crosslinking agent comprise bivalent cation.

89. the described composition of claim 88, wherein said bivalent cation is a calcium.

90. the described composition of claim 85, wherein said polymer comprise that carboxymethyl cellulose and described crosslinking agent comprise Tricationic.

91. the described composition of claim 90, wherein said Tricationic is an aluminium.

92. the described composition of claim 85, wherein said polymer comprise that pectin and described crosslinking agent comprise bivalent cation.

93. the described composition of claim 92, wherein said bivalent cation is a calcium.

94. the described composition of claim 85, wherein said solvent is moisture.

95. the described composition of claim 85, wherein said solvent is water-free.

96. the described composition of claim 85, wherein said solvent is uneven.

97. the described composition of claim 85 wherein makes described composition by phase separation process.

98. kit comprises the mixture of (i) tobacco and form agent and (ii) mold, wherein in described mold, when solvent being joined in the described mixture, has formed insoluble gel with the shape of described mold.

99. the described kit of claim 98, wherein said form agent comprises polymer and crosslinking agent.

100. the described kit of claim 99, wherein said polymer comprise that carrageenan and described crosslinking agent comprise univalent cation.

101. the described kit of claim 100, wherein said univalent cation is a potassium.

102. the described kit of claim 99, wherein said polymer comprise that alginates and described crosslinking agent comprise bivalent cation.

103. the described kit of claim 102, wherein said bivalent cation is a calcium.

104. the described kit of claim 99, wherein said polymer comprise that carboxymethyl cellulose and described crosslinking agent comprise Tricationic.

105. the described kit of claim 104, wherein said Tricationic is an aluminium.

106. the described kit of claim 99, wherein said polymer comprise that pectin and described crosslinking agent comprise bivalent cation.

107. the described kit of claim 106, wherein said bivalent cation is a calcium.

108. the described kit of claim 98, wherein said form agent comprises the insoluble polymer of dissolvable agents swelling.

109. the described kit of claim 108, the insoluble polymer of wherein said dissolvable agents swelling comprises polyvinyl alcohol.

110. the described kit of claim 98, wherein said solvent is moisture.

111. the described kit of claim 98, wherein said solvent is water-free.

112. the described kit of claim 98, wherein said solvent is uneven.

113. do not fire composition, comprise that (i) comprises the tobacco compositions of tobacco and form agent and (ii) packaging material.

114. the described composition of claim 113, wherein said tobacco compositions comprises a plurality of parts.

115. the described composition of claim 114, wherein said parts comprise thin slice, tablet or pearl.

116. the described composition of claim 114, wherein said parts are embedded in the described packaging material.

117. the described composition of claim 114, wherein said parts are not embedded in the described packaging material.

118. the described composition of claim 113, wherein said packaging material are good to eat disintegrations.

119. the described composition of claim 113, wherein said packaging material are not good to eat disintegrations.

120. the described composition of claim 113, wherein said packaging material comprise HPMC, CMC, pectin, alginates or Aureobasidium pullulans glycan.

121. the described composition of claim 113, wherein said packaging material comprise fabric or paper.

122. the described composition of claim 113, wherein said tobacco compositions comprises liquid.

123. the described composition of claim 113, wherein said liquid comprises sugar or salt, and wherein said sugar or salt have prevented that described packaging material are by described liquid disintegration.

124. the described composition of claim 113, wherein said form agent and tobacco have formed moldable embolism.

125. the described composition of claim 113 wherein uses vertical in form agent/filling/sealing machine, horizontal versions agent/filling/sealing machine, flow wrap machines or hot former that moulding is carried out in described form agent.

126. comprise the tobacco compositions of tobacco and good to eat disintegration packing, wherein described tobacco be positioned in the described packing.

127. the described composition of claim 126, wherein said tobacco comprise dry snuff or moist smokeless tobacco.

128. the described composition of claim 126, the packing of wherein said good to eat disintegration comprise HPMC, CMC, pectin, alginates or Aureobasidium pullulans glycan.

129. the described composition of claim 126 wherein uses vertical in form agent/filling/sealing machine, horizontal versions agent/filling/sealing machine, flow wrap machines or hot former that moulding is carried out in described form agent.

130. comprise the tobacco compositions of insoluble perforate matrix, tobacco and form agent, wherein said tobacco is placed in the described matrix, and is retained in the matrix by described form agent.

131. the described composition of claim 130, wherein said perforate matrix comprises fabric, foam or paper.

132. the described composition of claim 131, wherein said foam comprises polyurethane.

133. the described composition of claim 130, wherein said composition is masticable.

134. the described composition of claim 130 is wherein placed described perforate matrix on rod or handle.

135. the described composition of claim 130, it comprises the composition of listing in the Table X

Table X Composition Percentage Water-soluble polymer 10-70 Tobacco 1-90 Spices 1-40 Sweetener 0.2-6 Fiber 2-40 Plasticizer 1-40 Surfactant 0.05-5 Starch/maltodextrin 1-40 Lubricant 0.5-10

136. the described composition of claim 130, it comprises the composition of listing among the Table X I

Table X I Composition Percentage Water-soluble polymer 20-45 Tobacco 20-40 Spices 5-15 Sweetener 2-5 Fiber (solvable or soluble) 5-20 Plasticizer 5-15

Surfactant 0.1-1 Starch/maltodextrin 10-20 Lubricant 1-3

137. comprise the tobacco compositions of tobacco and form agent, wherein form described form agent with hollow shape.

138. the described composition of claim 137, it comprises the composition of listing in Table X II

Table X II Composition Percentage Water-soluble polymer 10-70 Tobacco 1-90 Spices 1-40 Sweetener 0.2-6 Fiber 2-40 Plasticizer 1-40 Surfactant 0.05-5 Starch/maltodextrin 1-40 Lubricant 0.5-10

139. the described composition of claim 137, it comprises the composition of listing among the Table X III

Table X III Composition Percentage Water-soluble polymer 20-45 Tobacco 20-40 Spices 5-15 Sweetener 2-5 Fiber (solvable or soluble) 5-20 Plasticizer 5-15 Surfactant 0.1-1 Starch/maltodextrin 10-20

Lubricant 1-3

140. the described composition of claim 137, wherein said form agent is twined by spiral.

141. the described composition of claim 137, it further comprises adhesive, wherein places described adhesive and unclamps preventing.

142. the described composition of claim 137 wherein forms described hollow shape by extruding.

143. the described composition of claim 137, wherein said tobacco and form agent form individual layer.

144. the described composition of claim 137, wherein said composition comprises multilayer.

145. the described composition of claim 144 will be two-layer at least laminated together wherein.

146. the described composition of claim 144, wherein said tobacco be placed on two-layer between.

147. the described composition of claim 144, two-layer at least different spices or the colorant of comprising in the wherein said multilayer.

148. the described composition of claim 137, it further comprises the filler that is placed in the described hollow shape.

149. the described composition of claim 148, wherein said filler comprises tobacco.

150. the described composition of claim 148, wherein said filler comprises colorant, sweetener, spices or odor masking agent.

151. the described composition of claim 148, wherein said filler comprise and described variform colorant or spices.

152. the described composition of claim 148, wherein said filler comprises gel.

153. the described composition of claim 137, it further comprises disintegrant.

154. comprise the Cigarette with protective device grass composition of tobacco and the agent of foamed form.

155. the described composition of claim 154, wherein said composition is moulding.

156. the described composition of claim 154 wherein is processed as film with described composition molding.

157. the described composition of claim 154, wherein said form agent is water miscible.

158. the described composition of claim 154, wherein said form agent is thermoplastic.

159. each described composition of claim 1-158, it further comprises spices or odor masking agent.

160. the described composition of claim 159, wherein said spices comprises Radix Glycyrrhizae, kudzu, hydrangea, day raw white skin lily magnolia leaf, yellow chamomile, fenugreek, cloves, menthol, cornmint, Chinese anise, Chinese cassia tree, vanilla (herb), Chinese ilex (winter green), cherry, berry, Dramboui, bourbon's wine (bourbon), Drambuie (scotch), whiskey, spearmint, peppermint (peppermint), lavender, cardamom, celery, the card lamb's-quarters, nutmeg, santal, bergamot, geranium wilfordii (geranium), honey smart (honey essace), attar of rose, vanilla, lemon oil, orange oil, cassia bark, crowndaisy chrysanthemum, cognac wine, jasmine, add and take the pattern tree, Salvia japonica, fennel, allspice (piment), ginger, anise, coriandrum, coffee or from any kind peppermint oil of Mentha.

161. each described composition of claim 1-158, it further comprises sweetener.

162. the described composition of claim 161, wherein said sweetener comprises sucrose, sucralose, dioxygen _ thiazine kalium, Aspartame, asccharin, cyclohexyl-n-sulfonate, lactose, sucrose, glucose, fructose, D-sorbite and mannitol.

163. each described composition of claim 1-158, it further comprises surfactant.

164. each described composition of claim 1-158, it further comprises plasticizer.

165. the described composition of claim 164, wherein said plasticizer comprise glycerine, propane diols, polyethylene glycol, D-sorbite/mannitol, acetylizad single monoglyceride, glyceryl triacetate or 1,3-butanediol.

166. each described composition of claim 1-158, it further comprises filler.

167. the described composition of claim 166, wherein said filler comprises starch, microcrystalline cellulose, wood pulp, soluble fibre, calcium carbonate, Dicalcium Phosphate, calcium sulfate or clay.

168. each described composition of claim 1-158, it further comprises lubricant or wax.

169. the described composition of claim 168, wherein said lubricant comprise stearic acid or stearate (ester).

170. the described composition of claim 168, wherein said wax are lecithin, glycerin monostearate or propylene glycolmonostearate.

171. each described composition of claim 1-158, it further comprises anticorrisive agent.

172. the described composition of claim 171, wherein said anticorrisive agent comprises methylparoban or potassium sorbate.

173. each described composition of claim 1-158, it further comprises stabilizing agent.

174. the described composition of claim 173, wherein said stabilizing agent comprise ascorbic acid, citric acid list sterol ester, BHT or BHA.

175. each described composition of claim 1-158, it further comprises coating.

176. the described composition of claim 175, wherein said coating is unglazed.

177. the described composition of claim 175, wherein said coating is glossiness.

178. the described composition of claim 175, wherein said coating comprises colorant, spices, sweetener or odor masking agent.

179. the described composition of claim 175, wherein said coating comprise and the different spices of described form agent.

180. the described composition of claim 175, wherein said coating have and the different disintegration rate of described form agent.

181. the described composition of claim 175, wherein said coating comprises tobacco.

182. the described composition of claim 175, wherein said coating comprises colorant.

183. the described composition of claim 175, wherein said coating comprise and the different colorant of described form agent.

184. each described composition of claim 1-158, it further comprises printed patterns.

185. the described composition of claim 184, wherein said printed patterns comprises sign.

186. the described composition of claim 184, wherein said printed patterns comprises colorant.

187. the described composition of claim 184, wherein said printed patterns comprises tobacco.

188. the described composition of claim 184, wherein said printed patterns comprises spices, sweetener or odor masking agent.

189. each described composition of claim 1-158, the surface of wherein said composition comprises embossing pattern (pattern in relief).

190. each described composition of claim 1-158, wherein said tobacco comprises powder, particle or fragment.

191. each described composition of claim 1-158, wherein said tobacco is to feel soluble in mouth.

192. each described composition of claim 1-158, it further comprises thin slice.

193. the described composition of claim 192, wherein said thin slice comprises tobacco.

194. the described composition of claim 192, wherein said thin slice comprises multiple spices or colorant.

195. each described composition of claim 1-158, wherein said composition is the shape that is fit to be applied in the oral cavity.

196. each described composition of claim 1-158, wherein said composition provides the tobacco satisfaction.

197. described tobacco satisfaction wherein took place in each described composition of claim 1-158 during 10 seconds-30 minutes.

198. comprise the composition of fluid-tight, water-fast packing and tobacco, wherein said tobacco is positioned in the described packing, and can be assigned in the mouth from described packing.

199. the described composition of claim 198, wherein said packing comprises bellows, and compresses described bellows so that described tobacco to be provided to mouth.

200. the described composition of claim 198, wherein said packing comprises spray bottle.

201. the described composition of claim 198, wherein said tobacco is positioned in the gel.

202. obtain the method for tobacco satisfaction, described method comprises each at least a portion of composition of claim 1-197 is put in the mouth, thereby obtains the tobacco satisfaction.

203. prepare the method for tobacco compositions, described method comprises that step (i) is shaped to the form agent film and (ii) adds tobacco in described form agent or film.

204. the described method of claim 203, wherein by solution casting, extrude, melt extrude, drum is dry or calendering (calendaring) forms described film.

205. the described method of claim 203 wherein joined described tobacco in the described form agent before described moulding.

206. the described method of claim 203 wherein joins described tobacco in the described film after described moulding.

207. the described method of claim 203 wherein further comprises second form agent is shaped to second film, and carries out film and described second film of (i) bonding.

208. the described method of claim 203, wherein said tobacco are placed between the described film and described second film of (i).

209. prepare the method for tobacco compositions, described method comprises that step (i) is shaped to tablet with the form agent and (ii) tobacco is joined in described form agent or the tablet.

210. the described method of claim 209 is wherein used compacting, injection moulding, compression moulding, injection is foam-formed or compression foam moulding and the described form agent of moulding.

211. prepare the method for tobacco compositions, described method comprises that step (i) is shaped to shape with the form agent and (ii) tobacco is joined in described form agent or the shape.

212. the described method of claim 211, wherein by extrude, compression moulding, injection moulding, punch forming, foam-formed, blowing, overmolded or slurry process be shaped to shape with described formation.

213. the described method of claim 211, wherein said form agent is the described shape of die-cut formation from sheet material.

214. the described method of claim 211, wherein said form agent is a foamed.

215. prepare the method for tobacco compositions, described method comprises that step (i) combines the gel form agent to form gel and (ii) tobacco to be joined in described gel form agent, solvent or the gel with solvent.

216. the described method of claim 215, wherein said form agent comprises polymer and crosslinking agent.

217. the described method of claim 215 wherein forms described gel in mold.

218. the described method of claim 215 is wherein by extruding profile and forming described gel by the described profile of extruding of certain-length cutting.

219. prepare the method for tobacco compositions, described method comprises that step (i) provides the liquid mixture of tobacco and polymer and (ii) described liquid is put in the bath, wherein said bath has caused the curing reaction of described polymer.

220. the described method of claim 219, wherein said bath comprise the crosslinking agent of the crosslinked described polymer of energy.

221. the described method of claim 219, wherein said bath are under the temperature that can cause described polymer cure.

222. the described method of claim 219, the center of wherein said composition is a liquid.

223. prepare the method for tobacco compositions, described method comprises tobacco is positioned in the gelatine capsule.

224. prepare the method for tobacco compositions, described method comprises that step (i) provides the mixture of tobacco and form agent and (ii) liquid joined in described tobacco and the form agent, wherein said form agent generation solvation has also formed solid.

225. the described method of claim 224, wherein step (ii) before, described mixture is put in the mold, and step (ii) after, described composition has kept the shape of described mold.

226. preparation method for compositions, described method comprise that step (i) provides tobacco compositions and (ii) described tobacco compositions combined with packaging material.

227. the described method of claim 226 wherein is embedded in described tobacco compositions in the described packaging material.

228. the described method of claim 226, wherein said tobacco compositions is not embedded in the described packaging material.

229. the described method of claim 226 is wherein used vertical in form agent/filling/sealing machine, horizontal versions agent/filling/sealing machine, flow wrap machines or the described packaging material of hot former moulding.

230. prepare the method for tobacco compositions, described method comprises that the mixture with tobacco and form agent is incorporated in the perforate matrix, wherein said form agent is adhered to described tobacco on the described matrix, and the disintegration of described matrix right and wrong mouth.

231. prepare the method for tobacco compositions, described method comprises (i) mixture and the non-miscible liquid blend that comprises host material with tobacco and form agent; (ii) cause being separated and solidification of described host material, thereby described mixture is positioned in the host material of described curing.

232. prepare the method for tobacco compositions, described method comprises that step (i) provides the form that is shaped to sheet material agent; (ii) spiral twines described sheet material to form hollow tube and (iii) tobacco to be joined in described form agent or the pipe.

233. prepare the method for tobacco compositions, described method comprises that step (i) is shaped to hollow shape with the form agent and (ii) tobacco is joined in described form agent or the shape.

234. the described method of claim 233, it further comprises with liquid, gel or solid fills described shape.

235. the described method of claim 233, wherein said moulding comprise extrude, injection moulding or blowing.

236. prepare the method for tobacco compositions, described method comprises that the flowable liquids that will comprise tobacco is put in the water-fast container.

237. the described method of claim 236, wherein said container is a spray bottle.

238. the described method of claim 236, wherein said container comprises bellows.

239. each described method of claim 203-235, it further comprises in described composition and adds coating.

240. the described method of claim 239, wherein by spraying, brushing, roller coat, scraping blade curtain coating, seam be coated with, squeezing and coating or hot melt deposit and apply described coating.

241. each described method of claim 203-235, it further is included in printed patterns on the described film.

242. the described method of claim 241 is wherein carried out described printing by offset printing, aniline printing, intaglio, ink-jet, laser or screen printing.

243. each described method of claim 203-235, it further comprises in described form agent or composition and adds spices, colorant or odor masking agent.