CN1903259B - Method for extraction and separation of moutan bark - Google Patents
Method for extraction and separation of moutan bark Download PDFInfo
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- CN1903259B CN1903259B CN2005100122758A CN200510012275A CN1903259B CN 1903259 B CN1903259 B CN 1903259B CN 2005100122758 A CN2005100122758 A CN 2005100122758A CN 200510012275 A CN200510012275 A CN 200510012275A CN 1903259 B CN1903259 B CN 1903259B
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- 239000003826 tablet Substances 0.000 description 1
- 238000002560 therapeutic procedure Methods 0.000 description 1
- 230000035922 thirst Effects 0.000 description 1
- 239000012588 trypsin Substances 0.000 description 1
- 210000003462 vein Anatomy 0.000 description 1
- 239000000341 volatile oil Substances 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
- 235000019509 white turmeric Nutrition 0.000 description 1
- 239000002023 wood Substances 0.000 description 1
Images
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- Medicines Containing Plant Substances (AREA)
Abstract
Description
Tree-peony root bark component | Chromatographic retention (min) | [M-H]- | Ultraviolet maximum absorption wavelength (nm) | Compound |
fr.51 | 5.01 | 169 | 215,280 | Gallic Acid (gallic acid) [1] |
9.5 | 479 | 230 | Paeoniflorin (peoniflorin) [1] | |
fr.52 | 5.01 | 169 | 215,280 | Gallic Acid (gallic acid) [1] |
9.5 | 479 | 230 | Paeoniflorin (peoniflorin) [1] | |
fr.53 | 9.5 | 479 | 230 | Paeoniflorin (peoniflorin) [1] |
fr.54 | 9.5 | 479 | 230 | Paeoniflorin (peoniflorin) [1] |
10.8 | 631 | 215,280 | Galloyl-Paeoniflorin (gallic acid peoniflorin) [2] | |
11.6 | 615 | 215,280 | Mudanpioside h (paeonoside h) [3] | |
fr.55 | 12.0 | 599 | 230 | Mudanpioside c (paeonoside c) [4] |
12.3 | 599 | 230 | Benzoyloxypaeoniflorin (Benzoyloxypaeoniflorin) [4] [5] | |
fr.56 | 13.5 | 583 | 230 | Benzoylpaeoniflorin (benzoylpaeoniflorin) [1] [4] [6] [7] [8] |
fr.81 | 4.4 | 493 | 215,280 | Unknown |
4.6 | 463 | 215,280 | Mudanoside b (paeonoside b) [4] | |
fr.82 | 4.3 | 493 | 215,280 | Paeonidanin[9] |
4.4 | 493 | 215,280 | Unknown | |
4.6 | 463 | 215,275 | Mudanoside b (paeonoside b) [4] | |
fr.83 | 9.8 | 494 | 254 | Oxypaeoniflorin (Hydroxy peoniflorin) [4] [10] [11] |
fr.84 | 9.8 | 494 | 254 | Oxypaeoniflorin (Hydroxy peoniflorin) [4] [10] [11] |
fr.85 | 14.8 | 479 | 230 | Paeoniflorin (peoniflorin) [1] |
fr.86 | 15.7 | 787 | 215,280 | 1,2,3,6-tretra-O-gaLloly-β-D-glucose (four gallic acid glucose) [12] |
16.3 | 787 | 215,280 | 1,2,3,6-tretra-O-gaLloly-β-D-glucose (four gallic acid glucose) [12] | |
17.1 | 611 | 215,280 | Suffruticoside A or Suffruticoside B or Suffruticoside C or Suffruticoside D[2] | |
fr.87 | 18.3 | 939 | 215,280 | 1,2,3,4,6-Pentagalloylglucose (five gallic acid peoniflorins) [12] |
fr.88 | 20.1 | 1091 | 215,280 | Digalloyl-1,2,3,4-tetra-O-galloyl--D-glucopyranose six gallic acid peoniflorins [12] |
21.0 | 1091 | 215,280 | Digalloyl-1,2,3,4-tetra-O-galloyl--D-glucopyranose (six gallic acid peoniflorins) [12] | |
fr.89 | 18.3 | 939 | 215,275 | 1,2,3,4,6-Pentagalloylglucose (five gallic acid peoniflorins) [12] |
21.0 | 1091 | 215,280 | Digalloyl-1,2,3,4-tetra-O-galloyl--D-glucopyranose (six gallic acid peoniflorins) [12] | |
fr.810 | 25.2 | 599 | 230 | Mudanpioside c (paeonoside c) [4] |
26.1 | 599 | 230 | Benzoyloxypaeoniflorin (Benzoyloxypaeoniflorin) [4] [5] | |
fr.811 | 26.1 | 599 | 230 | Benzoyloxypaeoniflorin (Benzoyloxypaeoniflorin) [4] [5] |
fr.812 | 29.7 | 583 | 230 | Benzoylpaeoniflorin (benzoylpaeoniflorin) [1] [4] [6] [7] [8] |
Claims (3)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN2005100122758A CN1903259B (en) | 2005-07-29 | 2005-07-29 | Method for extraction and separation of moutan bark |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN2005100122758A CN1903259B (en) | 2005-07-29 | 2005-07-29 | Method for extraction and separation of moutan bark |
Publications (2)
Publication Number | Publication Date |
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CN1903259A CN1903259A (en) | 2007-01-31 |
CN1903259B true CN1903259B (en) | 2011-11-30 |
Family
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CN2005100122758A Expired - Fee Related CN1903259B (en) | 2005-07-29 | 2005-07-29 | Method for extraction and separation of moutan bark |
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Families Citing this family (4)
Publication number | Priority date | Publication date | Assignee | Title |
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CN103087128B (en) * | 2013-02-05 | 2015-09-02 | 菏泽尧舜牡丹生物科技有限公司 | A kind of method extracting peoniflorin from the peony seeds dregs of rice |
CN104231019B (en) * | 2013-06-06 | 2017-05-10 | 复旦大学 | Application of monoterpene glycoside compounds in preparation of anticomplement drugs |
CN104231012B (en) * | 2013-06-06 | 2017-05-31 | 复旦大学 | Phenol glycosides compound and its purposes in anticomplement medicament is prepared |
CN105726646A (en) * | 2016-03-08 | 2016-07-06 | 青岛市中心医院 | Medicine composition for treating rheumatoid arthritis through immune adjustment and preparation method of medicine composition |
-
2005
- 2005-07-29 CN CN2005100122758A patent/CN1903259B/en not_active Expired - Fee Related
Non-Patent Citations (4)
Title |
---|
Zhang Haijiang,Wu Yongjiang,Cheng yiyu.Analysis of "Shenmai"Injection by HPLC/MS/MS.Journal of Pharmaceutical and Biomedical Analysis 31.2003,(31),175-183. |
Zhang Haijiang,Wu Yongjiang,Cheng yiyu.Analysis of "Shenmai"Injection by HPLC/MS/MS.Journal of Pharmaceutical and Biomedical Analysis 31.2003,(31),175-183. * |
谢平等.中药牡丹皮的研究概况.中药材科技 4.1983,(4),44-46. |
谢平等.中药牡丹皮的研究概况.中药材科技 4.1983,(4),44-46. * |
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