CN1887915A - Chlorinated polyethylene drying process - Google Patents
Chlorinated polyethylene drying process Download PDFInfo
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- CN1887915A CN1887915A CN 200610045528 CN200610045528A CN1887915A CN 1887915 A CN1887915 A CN 1887915A CN 200610045528 CN200610045528 CN 200610045528 CN 200610045528 A CN200610045528 A CN 200610045528A CN 1887915 A CN1887915 A CN 1887915A
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Abstract
The present invention discloses one chlorinated polyethylene drying process. The chlorinated polyethylene drying process with hot air as drying medium includes the first stage of pulse airflow drying and the second stage of fluidized bed drying to dry chlorinated polyethylene with 30-55 % water content into product with 0.3 % below water content. The present invention has simple drying apparatus, high heat efficiency, low water content in product and other advantages.
Description
Technical field
The present invention relates to a kind of drying process, a kind of specifically chlorinated polyethylene drying process.
Background technology
As everyone knows, chlorinatedpolyethylene is to use warm air as drying medium when dry, usually it is dry to adopt the intermittent type fluidized-bed at present, and the intermittent type fluidized-bed adopts drying mode in batches, and every batch of material all will be by operations such as reinforced, intensification, insulation, cooling, dischargings.Fluidized-bed all will experience one time heating and cooling process in every batch drying process, energy wastage is serious, and intermittent type fluidized-bed output is little simultaneously, can not maximize, and labor strength is big, and the product water content fluctuates easily.
Summary of the invention
Order of the present invention is exactly for overcoming above-mentioned the deficiencies in the prior art, a kind of thermo-efficiency height that has is provided, scale is big, the chlorinated polyethylene drying process of advantages such as system stability is reliable, to improving chlorinatedpolyethylene output, reduce the difficulty of operations and maintenance, guarantee quality product, the security of raising system has good effect.
For achieving the above object, the present invention has adopted following technical scheme:
A kind of chlorinated polyethylene drying process, it is that thermal source carries out two-stage drying at least with the warm air, its processing step is,
1) one-level drying: wet stock is sent into pneumatic drier (14), fully contacts with the high temperature drying air that enters pneumatic drier (14), finishes preliminarily dried, goes into fluidisation bed dryer (8), the tail gas emptying of purification by the dust removal installation dedusting is laggard then;
2) secondary drying: after the dried material of first-stage preliminary joins fluid bed dryer (8), with the high temperature drying air mixed that enters fluid bed dryer (8), make an interior material keep stable fluidization in the fluidisation section, and in bed, finish heat exchange, drying process with material, dry good material is discharged by fluid bed dryer (8), tail gas emptying after dust removal installation purifies of discharging from fluid bed dryer (8) top.
In the described one-level drying, wet stock is sent into pneumatic drier (14) through conveyer device﹠apos (15); The high temperature drying air be by dry air after 2# air filter (17) filters, and make after 5# vapor heat exchanger (16) heat exchange, wherein 5# vapor heat exchanger (16) is connected with flash tank (1); Described dust removal installation is to be composed in series by tornado dust collector I (13) and tornado dust collector II (14).
In the described secondary drying, the high temperature drying air by dry air after the 1# air filter filters (2), sucking the pressurization back by gas blower (5) divides four the tunnel to send into 1# vapor heat exchanger (3), 2# vapor heat exchanger (4), 3# vapor heat exchanger (6), 4# vapor heat exchanger (7) respectively, each interchanger also is connected with flash tank (1) respectively, gained high temperature drying air passes air distribution plate again and enters bed through fluid bed dryer (8) bottom air compartment; Described dust removal installation is for being arranged on the tornado dust collector III (9) and the tornado dust collector IV (10) at fluid bed dryer (8) top.
Described pneumatic drier (14) adopts gas-solid phase cocurrent cooling operation, and velocity of medium is greater than 15 meter per seconds in it, and time of drying is generally at 0.5～2 second; At surperficial gasifying stage, material is in 60～65 ℃ of the wet-bulb temperature of the gas that is in contact with it all the time.5, chlorinated polyethylene drying process according to claim 1 is characterized in that: described chlorinatedpolyethylene material carries out deep dehydration in fluid bed dryer (8), be no less than 120 minutes time of drying.
The present invention as drying medium, adds secondary fluidised bed drying by the one-level pulsed pneumatic drying with warm air, is moisture content that moisture content is less than 0.3% finished product greater than 30%～55% chlorinatedpolyethylene drying.Air stream drying uses high temperature air to carry out surface water rapid drying, and fluidized-bed adopts multistage differing temps air intake air to make goods fluid, and material is carried out depth drying.
The invention has the beneficial effects as follows:
1. the chlorinatedpolyethylene dehumidification system is realized carrying out continuously from being dosed to discharging, and the centre does not have personnel's intervention operation, has reduced labor strength, and fluidized-bed bed temperature-stable does not have heating and cooling process, reduces energy wastage, the thermo-efficiency height.After the normal operation of simultaneity factor, material is residence time basically identical in bed, and the product water content is low and stable.
2. according to the drying property of chlorinatedpolyethylene, one-level adopts the pulsed gas flow drying, use high temperature air in the extremely short time, to take off the surface water of chlorinatedpolyethylene, pneumatic drier adopts gas-solid phase cocurrent cooling operation, at surperficial gasifying stage, material is in the wet-bulb temperature of the gas that is in contact with it all the time, generally be no more than 60～65 ℃, in the dry stage that latter stage, temperature of charge rose, gas temperature reduces greatly, therefore, can use high-temperature gas, the gas-solid biphase is extremely short duration of contact in drying tube, and time of drying is generally at 0.5～2 second.The thermally denature of chlorinatedpolyethylene generally is the function of temperature and time, so material can not cause overheated or decompose and influence its quality.The pulsed gas flow drying machine can be given full play to high heat and mass effect simultaneously, with intensified drying process.
3. air stream drying is owing to the gas velocity height, and particle is good dispersion in gas phase, and the exsiccant useful area increases greatly.Simultaneously, because dispersion and agitaion when dry are brought in constant renewal in the gasification surface, therefore, exsiccant conducts heat, mass transfer process intensity is bigger.
4. secondary drying adopts fluidized-bed to carry out deep dehydration, chlorinatedpolyethylene in fluidized-bed under certain wind speed, blown afloat and be suspended in by fluid and do free movement in the fluid, collision mutually mixes between particle, and bed height rises, whole bed presents the form of similar liquids, the charge level of one basic horizontal is arranged at the bed top, and the severe smaller particles is floated on it, and this phenomenon is called the solid particulate fluidised formization.And the mean wind speed of this moment is called normal fluidizing velocity, can regulate the residence time of material in bed by regulating the material thickness of material in bed, and chlorinatedpolyethylene can reach the material requirement when the bed inner drying is more than 120 minutes.
5. rationally the selection of inlet temperature divides the multistage air intake according to the difference of material dewatering degree, has both improved thermo-efficiency, does not make material overtemperature in bed again.
6. each equipment is carried out electrostatic grounding, avoids chlorinatedpolyethylene dangerous because of static focus produces.
Description of drawings
Fig. 1 is a process flow sheet of the present invention;
Wherein, 1, flash tank, 2, the 1# air filter, 3,1# vapor heat exchanger, 4,2# vapor heat exchanger, 5, gas blower, 6, the 3# vapor heat exchanger, 7,4# vapor heat exchanger heating, 8, fluid bed dryer, 9, tornado dust collector III, 10, tornado dust collector IV, 11, induced draft fan, 12, tornado dust collector II, 13, tornado dust collector I, 14, pneumatic drier, 15, conveyer device﹠apos, 16,5# vapor heat exchanger, 17, the 2# air filter, 18, air sealer.
Embodiment
The invention will be further described below in conjunction with accompanying drawing and embodiment.
Among Fig. 1, this dehumidification system thermal source adopts warm air, the one-level drying: wet material adds pulsed gas flow drying machine 14 by conveyer device﹠apos 15, dry air filters by 2# air filter 17, fully contact with the high temperature air of 5# vapor heat exchanger 16 heat exchange, material is preliminarily dried in pulsed gas flow drying machine 14, enters fluid bed dryer 8 by the corresponding separately air sealer 18 in tornado dust collector II12 and tornado dust collector I13 bottom, tail gas after induced draft fan 11 pressurizations by the evacuated tube emptying.
Secondary drying: the material after the primary pre-drying is joined in the fluid bed dryer 8 through elephant trunk by air sealer 18.Air filters through 1# air filter 2, sucking the pressurization back by gas blower 5 divides four the tunnel to enter 1# vapor heat exchanger 3,2# vapor heat exchanger 4,3# vapor heat exchanger 6,7 heating of 4# vapor heat exchanger respectively, air admission fluid bed dryer 8 bottom air compartments after the heating pass air distribution plate again and enter bed.The air that enters bed in this process is effectively controlled, thereby makes an interior material keep stable fluidization, and with bed in finish heat exchange, drying process with material.The exsiccant material is discharged through the overflow port of fluidized-bed, enters air-transport system, and the tail gas of discharging from the fluidized-bed top purifies the back emptying through tornado dust collector III9 and tornado dust collector IV10.Flash tank 1 is connected with 1# vapor heat exchanger 3,2# vapor heat exchanger 4,3# vapor heat exchanger 6,4# vapor heat exchanger 7,5# vapor heat exchanger 16 respectively.
Velocity of medium is greater than 15 meter per seconds in the pneumatic drier 14, and the gas-solid biphase is extremely short duration of contact, and time of drying is generally at 0.5～2 second.The thermally denature of material generally is the function of temperature and time, and it is overheated therefore can not cause for the bonding material of this hot mastication of chlorinatedpolyethylene, causes danger.Pneumatic drier adopts gas-solid phase cocurrent cooling operation, and, at surperficial gasifying stage, material is in the wet-bulb temperature of the gas that is in contact with it all the time, generally is no more than 60～65 ℃, in the dry stage that latter stage, temperature of charge rose, gas temperature reduces greatly, therefore, can use high-temperature gas.
Secondary drying adopts fluidized-bed to carry out deep dehydration, chlorinatedpolyethylene in fluidized-bed under certain wind speed, blown afloat and be suspended in by fluid and do free movement in the fluid, collision mutually mixes between particle, and bed height rises, whole bed presents the form of similar liquids, the charge level of one basic horizontal is arranged at the bed top, and the severe smaller particles is floated on it, and this phenomenon is called the solid particulate fluidised formization.And the mean wind speed of this moment is called normal fluidizing velocity, can regulate the residence time of material in bed by regulating the material thickness of material in bed, and chlorinatedpolyethylene can reach the requirement of dry materials when the bed inner drying is more than 120 minutes.
Claims (5)
1, a kind of chlorinated polyethylene drying process is characterized in that: it is that thermal source carries out two-stage drying at least with the warm air, and its processing step is,
1) one-level drying: wet stock is sent into pneumatic drier (14), fully contacts with the high temperature drying air that enters pneumatic drier (14), finishes preliminarily dried, goes into fluidisation bed dryer (8), the tail gas emptying of purification by the dust removal installation dedusting is laggard then;
2) secondary drying: after the dried material of first-stage preliminary joins fluid bed dryer (8), with the high temperature drying air mixed that enters fluid bed dryer (8), make an interior material keep stable fluidization in the fluidisation section, and in bed, finish heat exchange, drying process with material, dry good material is discharged by fluid bed dryer (8), tail gas emptying after dust removal installation purifies of discharging from fluid bed dryer (8) top.
2, chlorinated polyethylene drying process according to claim 1 is characterized in that: in the described one-level drying, wet stock is sent into pulsed gas flow drying machine (14) through conveyer device﹠apos (15); The high temperature drying air be by dry air after 2# air filter (17) filters, and make after 5# vapor heat exchanger (16) heat exchange, wherein 5# vapor heat exchanger (16) is connected with flash tank (1); Described dust removal installation is to be composed in series by tornado dust collector I (13) and tornado dust collector II (14).
3, chlorinated polyethylene drying process according to claim 1, it is characterized in that: in the described secondary drying, the high temperature drying air by dry air after the 1# air filter filters (2), sucking the pressurization back by gas blower (5) divides four the tunnel to send into 1# vapor heat exchanger (3), 2# vapor heat exchanger (4), 3# vapor heat exchanger (6), 4# vapor heat exchanger (7) respectively, each interchanger also is connected with flash tank (1) respectively, gained high temperature drying air passes air distribution plate again and enters bed through fluid bed dryer (8) bottom air compartment; Described dust removal installation is for being arranged on the tornado dust collector III (9) and the tornado dust collector IV (10) at fluid bed dryer (8) top.
4, chlorinated polyethylene drying process according to claim 1 is characterized in that: described pneumatic drier (14) adopts gas-solid phase cocurrent cooling operation, and velocity of medium is greater than 15 meter per seconds in it, and time of drying is generally at 0.5～2 second; At surperficial gasifying stage, material is in 60～65 ℃ of the wet-bulb temperature of the gas that is in contact with it all the time.
5, chlorinated polyethylene drying process according to claim 1 is characterized in that: described chlorinatedpolyethylene material carries out deep dehydration in fluid bed dryer (8), be no less than 120 minutes time of drying.
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| Application Number | Priority Date | Filing Date | Title |
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| CNB2006100455286A CN100443509C (en) | 2006-07-19 | 2006-07-19 | Chlorinated polyethylene drying process |
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| CNB2006100455286A CN100443509C (en) | 2006-07-19 | 2006-07-19 | Chlorinated polyethylene drying process |
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Cited By (11)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN101979322A (en) * | 2010-10-07 | 2011-02-23 | 赵家春 | Drying method for use in potassium nitrate production |
| CN102603937A (en) * | 2012-04-09 | 2012-07-25 | 山东科院天力节能工程有限公司 | Flash drying and internal heated fluidized bed drying system and process special for chlorinated polyethylene |
| CN102620526A (en) * | 2012-03-16 | 2012-08-01 | 甘肃银光聚银化工有限公司 | Method for drying poly carbonate (PC) |
| CN102645085A (en) * | 2012-02-24 | 2012-08-22 | 青岛科技大学 | Method for continuously drying polycarbonate |
| CN102863565A (en) * | 2011-07-08 | 2013-01-09 | 倪隆 | Process for continuous separation of chlorinated polyethylene (cpe) clinker at high temperature |
| CN103900350A (en) * | 2014-04-11 | 2014-07-02 | 山东省食品发酵工业研究设计院 | Method for preventing sodium gluconate wet crystals from caking in drying process |
| CN107428032A (en) * | 2015-03-20 | 2017-12-01 | 沙特基础工业全球技术公司 | Improved drying means |
| CN107655311A (en) * | 2017-10-17 | 2018-02-02 | 太仓塑料助剂厂有限公司 | The drying device and method of haloflex |
| CN107940900A (en) * | 2017-10-12 | 2018-04-20 | 浙江工业大学 | The multilevel drying method and drying device of a kind of potassium fluoride in high activity |
| CN111023704A (en) * | 2019-12-23 | 2020-04-17 | 济南岳丰能源科技有限公司 | Drying system and process for high chlorinated polyethylene resin |
| CN111829292A (en) * | 2020-07-27 | 2020-10-27 | 潍坊硕邑化学有限公司 | Chlorinated polyethylene rubber drying equipment and process thereof |
Family Cites Families (4)
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| CN2511921Y (en) * | 2001-07-12 | 2002-09-18 | 宁夏北方淀粉股份有限公司 | Horizontal impulse air flow drier |
| CN100404989C (en) * | 2002-12-18 | 2008-07-23 | 兰州瑞德干燥技术有限公司 | Nitrogen-cycle engineering plastic air current and fluidized bed drying method |
| CN2775579Y (en) * | 2005-03-14 | 2006-04-26 | 王初阳 | High wet material drying unit |
| CN100348937C (en) * | 2005-09-05 | 2007-11-14 | 吉化集团公司 | Method and apparatus for drying copolymer of methyl methacrylate-styrene-butadiene |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN101979322A (en) * | 2010-10-07 | 2011-02-23 | 赵家春 | Drying method for use in potassium nitrate production |
| CN101979322B (en) * | 2010-10-07 | 2012-10-03 | 赵家春 | Drying method for use in potassium nitrate production |
| CN102863565A (en) * | 2011-07-08 | 2013-01-09 | 倪隆 | Process for continuous separation of chlorinated polyethylene (cpe) clinker at high temperature |
| CN102645085A (en) * | 2012-02-24 | 2012-08-22 | 青岛科技大学 | Method for continuously drying polycarbonate |
| CN102645085B (en) * | 2012-02-24 | 2014-01-15 | 青岛科技大学 | Method for continuously drying polycarbonate |
| CN102620526A (en) * | 2012-03-16 | 2012-08-01 | 甘肃银光聚银化工有限公司 | Method for drying poly carbonate (PC) |
| CN102620526B (en) * | 2012-03-16 | 2014-05-21 | 甘肃银光聚银化工有限公司 | Method for drying poly carbonate (PC) |
| CN102603937A (en) * | 2012-04-09 | 2012-07-25 | 山东科院天力节能工程有限公司 | Flash drying and internal heated fluidized bed drying system and process special for chlorinated polyethylene |
| CN103900350A (en) * | 2014-04-11 | 2014-07-02 | 山东省食品发酵工业研究设计院 | Method for preventing sodium gluconate wet crystals from caking in drying process |
| CN103900350B (en) * | 2014-04-11 | 2015-07-22 | 山东省食品发酵工业研究设计院 | Method for preventing sodium gluconate wet crystals from caking in drying process |
| CN107428032A (en) * | 2015-03-20 | 2017-12-01 | 沙特基础工业全球技术公司 | Improved drying means |
| US10406494B2 (en) | 2015-03-20 | 2019-09-10 | Sabic Global Technologies B.V. | Drying methods |
| CN107940900A (en) * | 2017-10-12 | 2018-04-20 | 浙江工业大学 | The multilevel drying method and drying device of a kind of potassium fluoride in high activity |
| CN107655311A (en) * | 2017-10-17 | 2018-02-02 | 太仓塑料助剂厂有限公司 | The drying device and method of haloflex |
| CN107655311B (en) * | 2017-10-17 | 2019-06-18 | 太仓塑料助剂厂有限公司 | The drying device and method of haloflex |
| CN111023704A (en) * | 2019-12-23 | 2020-04-17 | 济南岳丰能源科技有限公司 | Drying system and process for high chlorinated polyethylene resin |
| CN111023704B (en) * | 2019-12-23 | 2021-05-07 | 济南岳丰能源科技有限公司 | Drying system and process for high chlorinated polyethylene resin |
| CN111829292A (en) * | 2020-07-27 | 2020-10-27 | 潍坊硕邑化学有限公司 | Chlorinated polyethylene rubber drying equipment and process thereof |
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| CN100443509C (en) | 2008-12-17 |
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Owner name: SHANDONG TIANLI DRYING CO., LTD. Free format text: FORMER OWNER: TIANLI DRYING EQUIPMENT CO., LTD., SHANDONG Effective date: 20110516 |
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Effective date of registration: 20110516 Address after: 250101, Shandong Province, Ji'nan hi tech Zone, No. 554 Feng Feng Road, environmental science and Technology Park, building 8, Feng Feng building, room 230 Patentee after: Shandong Tianli Drying Co., Ltd. Address before: 250014 Shandong Province, Lixia District of Ji'nan city ten Road East Shouke Hospital Road No. 19 Patentee before: Tianli Drying Equipment Co., Ltd., Shandong |