CN1865420A - Aqueous cleaning agent for liquid crystal display - Google Patents
Aqueous cleaning agent for liquid crystal display Download PDFInfo
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- CN1865420A CN1865420A CN 200610014438 CN200610014438A CN1865420A CN 1865420 A CN1865420 A CN 1865420A CN 200610014438 CN200610014438 CN 200610014438 CN 200610014438 A CN200610014438 A CN 200610014438A CN 1865420 A CN1865420 A CN 1865420A
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- liquid crystal
- crystal display
- aqueous cleaning
- cleaning agent
- agent
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Abstract
The invention discloses a LCD water-based abluent of amine alkali and non-ion surface activator, which comprises the following parts: 20-70 percent amine alkali, 5-40 percent JFC, 5-20 percent non-ion surface activator and deionized water. The invention is beneficial to remove the surface residues, which improves the surface finishment of product.
Description
Technical field
The present invention relates to a kind of clean-out system, in particular, relate to a kind of aqueous cleaning agent that is applicable to the scavenging solution crystal display screen.
Background technology
Liquid crystal is the material that a class has property, it under liquid state, keep within the specific limits crystal distinctive three-dimensional space can ordered arrangement feature.The liquid crystal material that uses on the liquid crystal display is the organic compound with class formations such as cholesterol ester, cyanobiphenyl, Santosol 360s.Liquid crystal material is encapsulated into after two conductive glass centres, unnecessary liquid crystal material is arranged in that its periphery is always residual, as not removing the performance that will influence liquid-crystal display, when serious even the corrosion target lead-in wire, cause complete machine to scrap.Along with the develop rapidly of microelectronics, the surface clearness of liquid crystal display (LCD) and other substrate glass and various device substrate is had higher requirement.
The clean-out system that is applicable to LCD has three types of aqueous cleaning agents, half aqueous cleaning agent, solvent cleaner, and water base and half water base cleaning is applicable to ultrasonic washing process route, and solvent cleaner is applicable to gas phase ultrasonic cleaning operational path.At present, the main ingredient in the half water base and leaning solvent is solvency action based on alkane to liquid crystal, cleaning machine manufacture-illegal Chang Danyi, and cleaning efficiency is low.Simultaneously, the alkanes component all is low-flash, and is inflammable, and therefore explosive material causes a kind of potential to threaten to the production of factory and workman's safety.And because the alkanes component can not recycle, therefore the discharging back pollutes environment.Aqueous cleaning agent is then because advantages such as its low toxicity, environmental protection become the development trend that LCD cleans.But the aqueous cleaning agent that both at home and abroad can adopt now is imperfections all also.The residual liquid crystal of water base cleaning removal LCD is the emulsifying effect based on tensio-active agent and liquid crystal, and emulsification is bigger to ultransonic dependency, and the surface tension of water is bigger than solvent, and is relatively poor to the wettability of slit, influences the cleaning of residual LCD in the slit.Use at present the colored king who is preferably Japan, still limited it and promote the use of owing to it costs an arm and a leg.
Summary of the invention
The present invention is in order to overcome weak point of the prior art, provide a kind of mixing solutions of amine alkali and nonionogenic tenside that uses to eliminate residue, improve product surface smooth finish, good to the wettability of slit, security simultaneously is good, the aqueous cleaning agent for liquid crystal display that price is low.
The present invention is achieved through the following technical solutions:
A kind of aqueous cleaning agent for liquid crystal display is characterized in that being made up of following component by weight percentage: amine alkali 20~70%, JFC 5~40%, nonionogenic tenside 5~20%, balance of deionized water.
Described amine alkali is any in trolamine, diethanolamine, the hydroxyethylethylene diamine.
Described nonionogenic tenside is FA/O series or peregal series or op series non-ionic surfactants.
The present invention has following technique effect:
1. aqueous cleaning agent of the present invention is made up of amine alkali, JFC and nonionogenic tenside, use amine alkali has substituted the mineral alkali in the existing water machine clean-out system, utilize similar principle and organic bases the Decomposition that mixes of high infiltration structure to fat etc., realized that reduction surface tension and strong seepage force enter in the seam, utilize dissolving, decompose the effect of grade and remove organism.Amine alkali has certain solvency action to organism, and chemical reaction can take place amine alkali and organism, helps eliminating the residue of product surface, has improved the smooth finish of product surface.
2. owing to used water and various low toxicity reagent, as amine alkali, JFC, nonionogenic tenside, good environmental protection has been protected workers'health, and not flammable, do not explode simultaneously, security is good.And cost is low, has reduced cleaning charge usefulness, and dilution is used, and cleaning charge is lower.
3. multiple degree of freedom.Clean-out system technological design of the present invention, prescription and concentration have very big degree of freedom, can specialized designs or preparation satisfying specific cleaning needs, thereby can obtain excellent cleaning effect such as particulate, organic film, oil and fat.
4. the mechanism of cleaning more.Nonionogenic tenside can lower surface tension, have effects such as wetting, infiltration, dispersion, emulsification, foaming, washing, make the cleaning function of aqueous cleaning agent that number of mechanisms be arranged, except that dissolving, also comprise saponification, soak into, emulsification, dispersion, interfacial activity power etc.Thereby, reduced ultransonic dependency owing to adopted many cleaning mechanism to overcome serious dependence emulsive problem.
5. adopt JFC (fatty alcohol-polyoxyethylene ether) can be penetrated into the liquid crystal crack as permeate agent, good to the wettability of slit, help removing liquid crystal residual in the slit.
Embodiment
Below in conjunction with specific embodiment to the detailed description of the invention.
Amine alkali can adopt any in trolamine, diethanolamine, the hydroxyethylethylene diamine among the present invention, and amine alkali has following effect to organism:
Solvency action: amine alkali itself also is a kind of organism, and therefore according to the similar principle that mixes, it also can dissolve liquid crystal.
Chemical reaction: amine alkali energy and organism generation saponification reaction.
Nonionogenic tenside adopts FA/O series, peregal series and op series non-ionic surfactants among the present invention.The FA/O series non-ionic surfactants is the Liu Yuling of a Hebei University of Technology professor result of many years of research, and result of use is very good for many years aborning.Can adopt FA/O I type promoting agent, FA/O II type promoting agent.Peregal series promoting agent such as O-10, O-20, op series promoting agent such as oP-7, oP-10.Nonionogenic tenside has following effects:
Wetting, osmosis: make surface tension of liquid less, liquid is just sprawled at solid surface.
Emulsification, dissemination: the hydrophilic group of tensio-active agent (emulsifying agent) molecule dissolves in water, and oleophilic group dissolves in oil, forms unimolecular layer, has improved the stability of emulsion.
Foaming, froth breaking effect: when gas formed bubble, the oleophilic group of tensio-active agent stretched in the bubble, and unimolecular film has reduced surface tension, makes foam stabilization.
Cleaning function: the cleaning function of nonionogenic tenside is wetting, infiltration, emulsification, dispersive synthesis result.
Embodiment 1:
Get trolamine 70g respectively, JFC 5g, FA/O I type promoting agent 5g, deionized water 20g mixes the back and fully stirs, and obtains aqueous cleaning agent for liquid crystal display.
Embodiment 2:
Get hydroxyethylethylene diamine 30g respectively, JFC 5g, FA/O II type promoting agent 15g, deionized water 50g mixes the back and fully stirs, and obtains aqueous cleaning agent for liquid crystal display.
Embodiment 3:
Get trolamine 20g respectively, JFC 5g, O-20 promoting agent 5g, deionized water 70g mixes the back and fully stirs, and obtains aqueous cleaning agent for liquid crystal display.
Embodiment 4:
Get hydroxyethylethylene diamine 20g respectively, JFC 40g, O-10 promoting agent 5g, deionized water 35g mixes the back and fully stirs, and obtains aqueous cleaning agent for liquid crystal display.
Embodiment 5:
Get diethanolamine 60g respectively, JFC 5g, O-10 promoting agent 5g, deionized water 30g mixes the back and fully stirs, and obtains aqueous cleaning agent for liquid crystal display.
Embodiment 6:
Get trolamine 50g respectively, JFC 15g, oP-7 promoting agent 5g, deionized water 30g mixes the back and fully stirs, and obtains aqueous cleaning agent for liquid crystal display.
Embodiment 7:
Get trolamine 20g respectively, JFC10g, oP-10 promoting agent 20g, deionized water 50g mixes the back and fully stirs, and obtains aqueous cleaning agent for liquid crystal display.
Embodiment 8:
Get diethanolamine 20g respectively, JFC 20g, oP-10 promoting agent 10g, deionized water 50g mixes the back and fully stirs, and obtains aqueous cleaning agent for liquid crystal display.
Embodiment 9:
Get trolamine 70g respectively, JFC 5g, oP-10 promoting agent 5g, deionized water 20g mixes the back and fully stirs, and obtains aqueous cleaning agent for liquid crystal display.
Embodiment 10:
Get hydroxyethylethylene diamine 30g respectively, JFC 5g, o-10 promoting agent 15g, deionized water 50g mixes the back and fully stirs, and obtains aqueous cleaning agent for liquid crystal display.
Adopt above clean-out system that liquid crystal cell is cleaned laggard line sampling and detect, adopt following three kinds of methods to observe:
1, under fluorescent lamp 1000LX illumination, apart from liquid crystal cell 30cm place's visualize;
2, on polarisation check light platform, the check of rotation polaroid;
3, use polarized light microscope observing,
Detected result is as follows:
Interventions Requested defect type defect state
The residual nothing of (glass and ITO) LC
Granular substance does not have
Streak, flow path does not have
The narrow residual nothing of LC of meeting
Other residual (clean-out system, water etc.) do not have
Frame adhesive is peeled off, and gas leakage does not have
ITO corrodes nothing
The sealing compound colour-change does not have
Changes in hardness does not have
Bonding strength changes not to be had
Floating glue, the nothing of coming unstuck
Detecting the back qualification rate all can reach more than 99%.
Although relate to a kind of aqueous cleaning agent for liquid crystal display and carried out special description disclosed with reference to embodiment, embodiment described above is illustrative and not restrictive, under the situation that does not break away from the spirit and scope of the present invention, all variations and modification are all within the scope of the present invention.
Claims (6)
1, a kind of aqueous cleaning agent for liquid crystal display is characterized in that being made up of following component by weight percentage: amine alkali 20~70%, JFC 5~40%, nonionogenic tenside 5~20%, balance of deionized water.
2, aqueous cleaning agent for liquid crystal display according to claim 1 is characterized in that described amine alkali is any in trolamine, diethanolamine, the hydroxyethylethylene diamine.
3, aqueous cleaning agent for liquid crystal display according to claim 1 is characterized in that described nonionogenic tenside is FA/O promoting agent or peregal series or op series non-ionic surfactants.
4, aqueous cleaning agent for liquid crystal display according to claim 3 is characterized in that the FA/O promoting agent is FA/O I type promoting agent or FA/O II type promoting agent.
5, aqueous cleaning agent for liquid crystal display according to claim 3 is characterized in that described peregal series promoting agent is 0-10 or 0-20.
6, aqueous cleaning agent for liquid crystal display according to claim 3 is characterized in that described op series promoting agent is oP-7 or oP-10.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN 200610014438 CN1865420A (en) | 2006-06-23 | 2006-06-23 | Aqueous cleaning agent for liquid crystal display |
Applications Claiming Priority (1)
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---|---|---|---|
CN 200610014438 CN1865420A (en) | 2006-06-23 | 2006-06-23 | Aqueous cleaning agent for liquid crystal display |
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CN1865420A true CN1865420A (en) | 2006-11-22 |
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CN 200610014438 Pending CN1865420A (en) | 2006-06-23 | 2006-06-23 | Aqueous cleaning agent for liquid crystal display |
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Cited By (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101879509A (en) * | 2010-07-21 | 2010-11-10 | 河北工业大学 | Liquid crystal screen cleaning method |
CN104745317A (en) * | 2013-12-25 | 2015-07-01 | 安徽明讯新材料科技有限公司 | Coating equipment drying tunnel cleaning compound |
CN105013755A (en) * | 2015-05-13 | 2015-11-04 | 湖北鸿创科技有限公司 | Pre-cleaning method used for pretreatment on liquid crystal display production line |
CN107216961A (en) * | 2017-05-20 | 2017-09-29 | 合肥市惠科精密模具有限公司 | A kind of AMOLED cleaning glass substrates liquid |
CN107354018A (en) * | 2017-05-20 | 2017-11-17 | 合肥市惠科精密模具有限公司 | A kind of high-efficiency environment friendly LCDs cleaning agent |
CN108559660A (en) * | 2018-06-25 | 2018-09-21 | 安徽全兆光学科技有限公司 | A kind of liquid crystal display detergent |
CN111763573A (en) * | 2019-04-02 | 2020-10-13 | 昆山欣谷微电子材料有限公司 | Alkaline glass substrate cleaning fluid composition |
CN113122398A (en) * | 2021-04-23 | 2021-07-16 | 广州亦盛环保科技有限公司 | Water-based liquid crystal cleaning agent and preparation method and application thereof |
-
2006
- 2006-06-23 CN CN 200610014438 patent/CN1865420A/en active Pending
Cited By (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101879509A (en) * | 2010-07-21 | 2010-11-10 | 河北工业大学 | Liquid crystal screen cleaning method |
CN104745317A (en) * | 2013-12-25 | 2015-07-01 | 安徽明讯新材料科技有限公司 | Coating equipment drying tunnel cleaning compound |
CN105013755A (en) * | 2015-05-13 | 2015-11-04 | 湖北鸿创科技有限公司 | Pre-cleaning method used for pretreatment on liquid crystal display production line |
CN107216961A (en) * | 2017-05-20 | 2017-09-29 | 合肥市惠科精密模具有限公司 | A kind of AMOLED cleaning glass substrates liquid |
CN107354018A (en) * | 2017-05-20 | 2017-11-17 | 合肥市惠科精密模具有限公司 | A kind of high-efficiency environment friendly LCDs cleaning agent |
CN108559660A (en) * | 2018-06-25 | 2018-09-21 | 安徽全兆光学科技有限公司 | A kind of liquid crystal display detergent |
CN111763573A (en) * | 2019-04-02 | 2020-10-13 | 昆山欣谷微电子材料有限公司 | Alkaline glass substrate cleaning fluid composition |
CN113122398A (en) * | 2021-04-23 | 2021-07-16 | 广州亦盛环保科技有限公司 | Water-based liquid crystal cleaning agent and preparation method and application thereof |
CN113122398B (en) * | 2021-04-23 | 2022-07-08 | 广州亦盛环保科技有限公司 | Water-based liquid crystal cleaning agent and preparation method and application thereof |
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Open date: 20061122 |