CN1849897A - Milk product containing full-valence animal bone powder - Google Patents
Milk product containing full-valence animal bone powder Download PDFInfo
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- CN1849897A CN1849897A CN 200610046712 CN200610046712A CN1849897A CN 1849897 A CN1849897 A CN 1849897A CN 200610046712 CN200610046712 CN 200610046712 CN 200610046712 A CN200610046712 A CN 200610046712A CN 1849897 A CN1849897 A CN 1849897A
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- powder
- animal bone
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- bone powder
- milk
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Abstract
The present invention relates to a milk product richly containing complete animal bone powder. It contains pure milk, in which animal bone powder is added. It is characterized by that its calcium content is high, and its animal bone powder grain size is up to nano-grade, so that it contains rich nutrients.
Description
Technical field:
The present invention relates to food, thing is not a dairy produce.
Technical field:
Milk powder is as a kind of convenience at present, nutraceutical has become people's common daily bread, old man particularly, children and student, the calcium deficiency phenomenon is often arranged, osteoporosis or rickets take place, depauperation etc., milk powder often is promptly as food, has certain calcium supplementing effect again, though present milk powder has certain nutrient value, calcium content is other food height relatively, but still can not satisfy people's needs, the people still needs other health products of replenishing the calcium greatly, and the absorption of calcium wherein and other materials also is a key issue, though contain high calcium, can be only most important for the absorption of human body utilization.
Summary of the invention:
The objective of the invention is to overcome above-mentioned not enough problem, a kind of dairy produce that is rich in animal bone powder is provided, prescription is reasonable, comprehensive nutrition.
The technical scheme that the present invention is adopted for achieving the above object is: be rich in the dairy produce of animal bone powder, contain plain chocolate, wherein be added with animal bone powder.
Be added with animal bone powder in the described dairy produce that is rich in animal bone powder smaller or equal to gross weight 20%.
Described dairy produce is fresh milk, sour milk or milk powder, and milk powder can be various milk powder such as pure milk powder, soymilk powder, peanut milk powder, chocolate milk power, fruit-vegetable-milk powder.
Described animal bone powder is that granularity reaches nano level powdery full-valence animal bone powder.
Described full-valence animal bone powder contains collagen content more than 13%, and calcium content is more than 15%, and content of mineral substances is more than 45%.
Described full-valence animal bone powder is bone 100% conversion ratio, and nutritional labeling keeps fully in the bone.
Described full-valence animal bone powder is animal bone powders such as pig bone, fish-bone, ox bone, sheep bone, chicken bone.
Described full-valence animal bone powder is to make by following processing method processing:
The first step, degreasing: fresh or freezing animal bone carries out fragmentation after removing impurity, is crushed to below the 2cm, presses bone: alkali lye=1: 5～8 weight ratios are mixed, and are heated to 30～80 ℃ after the mixing, keep 2～4 hours; Isolated by filtration is got supernatant, and supernatant is transferred pH value to 2.0～4.0 with acid solution, and cooling (below 60 ℃); Fat (bone marrow oil) come-up, the cooling solid-state taking-up in back is bone marrow oil, fat products; Protein precipitation, centrifugal (3000～4500 change/min) reclaim, and are protein organic matter product,
Second the step, Vacuum solutions from: with above-mentioned bone through the colloid mill pulverization process to the following bone meal of granularity 2mm, join Vacuum solutions in jar, add 3～7 times of deionized waters (volume), earlier under rough vacuum, add acid solution, keep pH value 1.0～3.0, vacuum is heightened after more than 0.5 hour, under pH value keeps constant substantially situation, ionization is dissociated and is just finished, filtered and recycled collagenous fibres, separation of supernatant;
The 3rd step, flocculation are reclaimed: Vacuum solutions is transferred pH value to 7.0～8.0, the Ca that dissociates out in the bone, PO from the supernatant that obtains with alkaline solution
4Again flocculation produces precipitation of hydroxyapatite, and filtered and recycled obtains hydroxyapatite after the spray-drying;
The 4th step, collagen moleculesization: the collagenous fibres that obtain after the decalcification are heated to 50～80 ℃ after suspending with lactic acid or citric acid, treat the whole molecularization of collagenous fibres after, stop heating;
The 5th step, combination drying: in the collagen liquid after the collagen moleculesization, add the hydroxyapatite that flocculation sediment obtains, after fully react, the emulsifying processing obtains full-valence animal bone powder after spray-dried.
NaOH solution or the NaHCO of 0.2～0.3M adopted in described first step degreasing with alkali lye
3Solution; Acid solution adopts the HCI solution of 5～7M.
The described second step Vacuum solutions is from the HCI solution that adopts 5～7M with acid solution.
The NaOH solution that alkaline solution adopts 8-11M is reclaimed in described the 3rd step flocculation.
Lactic acid or the citric acid of described the 4th step collagen molecules employing 0.4～0.7M suspend.
170～240 ℃ of spray-drying inlet temperatures, 60～100 ℃ of outlet temperatures, whole moisture 4～12% are reclaimed in described the 3rd step flocculation.
170～240 ℃ of described the 5th step combination drying spray and the dry inlet temperatures of mist, 60～100 ℃ of outlet temperatures, whole moisture 4～12%.
The preparation method of milk powder of the present invention is a routine fashion:
At first fresh milk is gone into milk-storage tank after the degassing, filtration, cooling, again it is squeezed into compensating groove, heat centrifugal other batchings of back adding and stir, spray-drying after vacuum concentrates after filtration is distributed into finished product milk powder.
The present invention adds bone meal in dairy produce, compare with similar high calcium product, calcium content height wherein, calcium is easier to be absorbed by human body, when particularly adopting granularity to reach nano level full-valence animal bone powder, nutritional labeling is close to identical with bone component, meet the human nutrition needs, using as various food additives does not influence food processing and quality, mouthfeel, and purposes is more extensive, preparation method's uniqueness of full-valence animal bone powder brush, keep nutritional labeling, simple to operation, cost is low, contamination-free produces, and satisfies the needs that large industrialized is produced.
The specific embodiment:
Embodiment 1
At first with fresh milk or goat milk through the degassing, to filter, go into after the cooling milk-storage tank standby.
It is standby to prepare full-valence animal bone powder then as follows:
First step degreasing: fresh or freezing pig bone carries out fragmentation earlier, is crushed to below the 2cm, presses bone: alkali lye=weight ratio was mixed in 1: 6; Alkali lye adopts the NaOH solution of 0.25M.Be heated to 50 ℃ after the mixing, kept 2～4 hours; Isolated by filtration is got supernatant, and supernatant is transferred pH value to 3.0 with the HCI of 6M, and is cooled to below 60 ℃; Fat (bone marrow oil) come-up, the cooling solid-state taking-up in back is bone marrow oil, fat products; Protein precipitation, it is centrifugal that (3500 change/min) reclaim, and are protein organic matter product;
Second the step. Vacuum solutions from: above-mentioned bone is controlled at the following bone meal of 2mm through colloid mill pulverization process to granularity, join Vacuum solutions in jar, add 5 times of deionized waters (volume), the HCI solution that adds earlier 6M under rough vacuum is kept pH value and vacuum is heightened after more than 2.0,0.5 hours, under pH value keeps constant substantially situation, ionization is dissociated and is just finished, filtered and recycled collagenous fibres, separation of supernatant;
The 3rd step, flocculation are reclaimed: Vacuum solutions is transferred pH value to 7.0, the Ca that dissociates out in the bone, PO from the supernatant that obtains with the NaOH solution of 10M
4Again flocculation produces precipitation of hydroxyapatite, and filtered and recycled obtains hydroxyapatite after the spray-drying (essential condition: 190 ℃ of inlet temperatures, 80 ℃ of outlet temperatures, whole moisture about 5%).
The 4th step, collagen moleculesization: after lactic acid (or citric acid) suspension of the collagenous fibres that obtain after the decalcification with 0.5M, be heated to 65 ℃, after treating the whole molecularization of collagenous fibres, stop heating, spray-drying (essential condition: 190 ℃ of inlet temperatures, 80 ℃ of outlet temperatures, whole moisture about 6%) obtain collagen protein powder.
The 5th step, combination drying: in the collagen liquid after the degraded, add the hydroxyapatite that flocculation sediment obtains, after fully having reacted, handle with the homogenizer emulsifying, obtain active quick dissolving full pig nutrients for bones after spray-dried (essential condition: 190 ℃ of inlet temperatures, 80 ℃ of inlet temperatures, whole moisture about 5%), proterties: white or milky floury powder (granularity is a nanoscale), free from extraneous odour, free from admixture are the milkiness shape under the liquid state.
The 1.0 kg of pure milk that will refrigerate are at last squeezed into compensating groove, heat centrifugally, squeeze into allotment, will 0.08 kilogram of full-valence animal bone powder add in the milk to stir.
The goat milk method for making is identical with milk basically, and just many steps take off and have a strong smell, and 0.05 kilogram of full-valence animal bone powder of adding stirs and gets final product in the every kilogram of goat milk in back.
Embodiment 2
Prepare soymilk powder as stated above, each raw material and consumption (kilogram) are as follows:
Bean powder 100, milk 100, full-valence animal bone powder 30, white granulated sugar 20 mix above-mentioned raw materials and get final product.Also can be after soybean is pulverized through peeling, the enzyme-added flavor that takes off, vacuum drying gets the sugar-free bean powder, adds other raw materials then, mixes and makes soymilk powder.
Embodiment 3
Produce sour milk, fresh milk double centner, 20 kilograms of full-valence animal bone powders by following material quantity and method for making, sugar, fruit flavor agent etc. a little, in milk, add beneficial bacterium (leavening) again after the fresh milk process Ma Shi sterilization, after sending out alcohol, cool off can again and make the fruity yoghurt.
Claims (9)
1, is rich in the dairy produce of animal bone powder, it is characterized in that: contain pure milk, wherein be added with animal bone powder.
2, according to the described dairy produce that is rich in animal bone powder of claim 1, it is characterized in that: wherein be added with animal bone powder smaller or equal to gross weight 20%.
3, according to the described dairy produce that is rich in animal bone powder of claim 1, it is characterized in that: animal bone powder is that granularity is a nanoscale powdery full-valence animal bone powder.
4, according to the described dairy produce that is rich in animal bone powder of claim 1, it is characterized in that: animal bone powder contains collagen content more than 13%, and calcium content is more than 15%, and content of mineral substances is more than 45%.
5, according to the described dairy produce that is rich in animal bone powder of claim 1, it is characterized in that: animal bone powder is animal bone powders such as pig bone, fish-bone, ox bone, sheep bone, chicken bone.
6, according to the described dairy produce that is rich in animal bone powder of claim 1, it is characterized in that: animal bone powder prepares by following processing method:
The first step, degreasing: fresh or freezing animal bone carries out fragmentation after removing impurity, is crushed to below the 2cm, presses bone: alkali lye=1: 5～8 weight ratios are mixed, and are heated to 30～80 ℃ after the mixing, keep 2～4 hours; Isolated by filtration is got supernatant, and supernatant is transferred pH value to 2.0～4.0 with acid solution, and cooling (below 60 ℃); Fat (bone marrow oil) come-up, the cooling solid-state taking-up in back is bone marrow oil, fat products; Protein precipitation, centrifugal (3000～4500 change/min) reclaim, and are protein organic matter product,
Second the step, Vacuum solutions from: with above-mentioned bone through the colloid mill pulverization process to the following bone meal of granularity 2mm, join Vacuum solutions in jar, add 3～7 times of deionized waters (volume), earlier under rough vacuum, add acid solution, keep pH value 1.0～3.0, vacuum is heightened after more than 0.5 hour, under pH value keeps constant substantially situation, ionization is dissociated and is just finished, filtered and recycled collagenous fibres, separation of supernatant;
The 3rd step, flocculation are reclaimed: Vacuum solutions is transferred pH value to 7.0～8.0, the Ca that dissociates out in the bone, PO from the supernatant that obtains with alkaline solution
4Again flocculation produces precipitation of hydroxyapatite, and filtered and recycled obtains hydroxyapatite after the spray-drying;
The 4th step, collagen moleculesization: the collagenous fibres that obtain after the decalcification are heated to 50～80 ℃ after suspending with lactic acid or citric acid, treat the whole molecularization of collagenous fibres after, stop heating;
The 5th step, combination drying: in the collagen liquid after the collagen moleculesization, add the hydroxyapatite that flocculation sediment obtains, after fully react, the emulsifying processing obtains full-valence animal bone powder after spray-dried.
7, according to the described dairy produce that is rich in animal bone powder of claim 6, it is characterized in that: NaOH solution or the NaHCO of 0.2～0.3M adopted in the first step degreasing of animal bone powder processing method with alkali lye
3Solution; Acid solution adopts the HCI solution of 5～7M;
The second step Vacuum solutions is from the HCI solution that adopts 5～7M with acid solution;
The NaOH solution that alkaline solution adopts 8-11M is reclaimed in the flocculation of the 3rd step; The flocculation of the 3rd step is reclaimed and is sparged 170～240 ℃ of dry inlet temperatures, 60～100 ℃ of outlet temperatures, whole moisture 4～12%;
Lactic acid or the citric acid of the 4th step collagen molecules employing 0.4～0.7M suspend;
The 5th step was mixed in 170～240 ℃ of the dry inlet temperatures of dry spray and mist, 60～100 ℃ of outlet temperatures, whole moisture 4～12%.
8, according to the arbitrary described dairy produce that is rich in animal bone powder of claim 1-7, it is characterized in that: dairy produce is fresh milk, sour milk or milk powder.
9, the described according to Claim 8 dairy produce that is rich in animal bone powder is characterized in that: milk powder can be various milk powder such as pure milk powder, soymilk powder, peanut milk powder, chocolate milk power, fruit-vegetable-milk powder.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2006100467122A CN100433985C (en) | 2006-05-23 | 2006-05-23 | Milk product containing full-valence animal bone powder |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2006100467122A CN100433985C (en) | 2006-05-23 | 2006-05-23 | Milk product containing full-valence animal bone powder |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1849897A true CN1849897A (en) | 2006-10-25 |
| CN100433985C CN100433985C (en) | 2008-11-19 |
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| Application Number | Title | Priority Date | Filing Date |
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| CNB2006100467122A Expired - Fee Related CN100433985C (en) | 2006-05-23 | 2006-05-23 | Milk product containing full-valence animal bone powder |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101999462A (en) * | 2010-10-12 | 2011-04-06 | 李国勇 | Milk powder for preventing and treating osteoporosis |
| CN103283842A (en) * | 2013-04-26 | 2013-09-11 | 蚌埠市福淋乳业有限公司 | Black-tea cherry yoghourt and preparation method thereof |
| CN104170985A (en) * | 2014-07-16 | 2014-12-03 | 安徽金菜地食品有限公司 | Calcium-supplementing bone meal milk and preparation method thereof |
| CN105076419A (en) * | 2015-08-27 | 2015-11-25 | 广州市全能鲜骨粉生物食品有限公司 | Fresh bone tankage-contained milk beverage and manufacturing method thereof |
| CN105475585A (en) * | 2015-11-18 | 2016-04-13 | 彭贵书 | Calcium-supplementing bone-paste chocolate and manufacture method |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1173975A (en) * | 1997-08-01 | 1998-02-25 | 天津天狮集团有限公司 | High-calcium milk powder and its production |
-
2006
- 2006-05-23 CN CNB2006100467122A patent/CN100433985C/en not_active Expired - Fee Related
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101999462A (en) * | 2010-10-12 | 2011-04-06 | 李国勇 | Milk powder for preventing and treating osteoporosis |
| CN103283842A (en) * | 2013-04-26 | 2013-09-11 | 蚌埠市福淋乳业有限公司 | Black-tea cherry yoghourt and preparation method thereof |
| CN104170985A (en) * | 2014-07-16 | 2014-12-03 | 安徽金菜地食品有限公司 | Calcium-supplementing bone meal milk and preparation method thereof |
| CN105076419A (en) * | 2015-08-27 | 2015-11-25 | 广州市全能鲜骨粉生物食品有限公司 | Fresh bone tankage-contained milk beverage and manufacturing method thereof |
| CN105475585A (en) * | 2015-11-18 | 2016-04-13 | 彭贵书 | Calcium-supplementing bone-paste chocolate and manufacture method |
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| Publication number | Publication date |
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| CN100433985C (en) | 2008-11-19 |
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Granted publication date: 20081119 |