CN1785911A - Preparation method of plastic pelletizing template having large size metal ceramic composite material sheet - Google Patents
Preparation method of plastic pelletizing template having large size metal ceramic composite material sheet Download PDFInfo
- Publication number
- CN1785911A CN1785911A CN 200410082891 CN200410082891A CN1785911A CN 1785911 A CN1785911 A CN 1785911A CN 200410082891 CN200410082891 CN 200410082891 CN 200410082891 A CN200410082891 A CN 200410082891A CN 1785911 A CN1785911 A CN 1785911A
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- Prior art keywords
- template
- ceramic composite
- composite material
- large size
- metal ceramic
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- 229910052751 metal Inorganic materials 0.000 title claims abstract description 40
- 239000002184 metal Substances 0.000 title claims abstract description 40
- 239000000919 ceramic Substances 0.000 title claims abstract description 36
- 239000002131 composite material Substances 0.000 title claims abstract description 31
- 238000002360 preparation method Methods 0.000 title claims abstract description 15
- 238000005453 pelletization Methods 0.000 title claims description 24
- 238000003466 welding Methods 0.000 claims abstract description 26
- 239000000843 powder Substances 0.000 claims abstract description 9
- 239000000463 material Substances 0.000 claims abstract description 8
- 239000012528 membrane Substances 0.000 claims description 17
- 238000005219 brazing Methods 0.000 claims description 12
- 239000010935 stainless steel Substances 0.000 claims description 8
- 229910001220 stainless steel Inorganic materials 0.000 claims description 8
- PZNSFCLAULLKQX-UHFFFAOYSA-N Boron nitride Chemical compound N#B PZNSFCLAULLKQX-UHFFFAOYSA-N 0.000 claims description 4
- RVTZCBVAJQQJTK-UHFFFAOYSA-N oxygen(2-);zirconium(4+) Chemical compound [O-2].[O-2].[Zr+4] RVTZCBVAJQQJTK-UHFFFAOYSA-N 0.000 claims description 4
- 229910001928 zirconium oxide Inorganic materials 0.000 claims description 4
- 229910052582 BN Inorganic materials 0.000 claims description 3
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 claims description 3
- 239000013590 bulk material Substances 0.000 claims description 3
- 229910052802 copper Inorganic materials 0.000 claims description 3
- 239000010949 copper Substances 0.000 claims description 3
- 239000003779 heat-resistant material Substances 0.000 claims description 3
- 238000002791 soaking Methods 0.000 claims description 3
- 229910000679 solder Inorganic materials 0.000 claims description 3
- 238000009491 slugging Methods 0.000 claims description 2
- 239000011159 matrix material Substances 0.000 claims 1
- 238000000034 method Methods 0.000 abstract description 6
- 238000005476 soldering Methods 0.000 abstract description 6
- 238000005469 granulation Methods 0.000 abstract description 2
- 230000003179 granulation Effects 0.000 abstract description 2
- 238000005192 partition Methods 0.000 abstract 3
- 239000003795 chemical substances by application Substances 0.000 abstract 1
- 230000004907 flux Effects 0.000 abstract 1
- 238000001816 cooling Methods 0.000 description 8
- 238000005245 sintering Methods 0.000 description 4
- 208000037656 Respiratory Sounds Diseases 0.000 description 3
- 229910045601 alloy Inorganic materials 0.000 description 3
- 239000000956 alloy Substances 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- MCMNRKCIXSYSNV-UHFFFAOYSA-N Zirconium dioxide Chemical compound O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 description 2
- 238000009413 insulation Methods 0.000 description 2
- 239000002905 metal composite material Substances 0.000 description 2
- 230000000295 complement effect Effects 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000000155 melt Substances 0.000 description 1
- 230000000630 rising effect Effects 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
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- Ceramic Products (AREA)
Abstract
The present invention relates to a preparation method of plastic granulation template with large-size metal ceramic composite material sheet. It adopts vacuum submerged-welding treatment technique, and it is characterized by that on the welding zone of template self-body are successively placed soldering flux whose thickness is 0.3-0.6mm, large-size metal ceramic composite material sheet and press block; at two sides of welding band are placed ring-shaped partition boards, between ring-shaped partition board and template self-body the welding-proof flow-resisting agent is coated, the interior of ring-shaped partition board is filled up with heat-proofing material powder, the ring-shaped cover plate is placed on it, then the above-mentioned material is placed in a vacuum soldering furnace to make heating-welding.
Description
Technical field:
The present invention relates to large size wear-and corrosion-proof metal ceramic composite and low-alloy stainless-steel vacuum soldering interconnection technique, provide a kind of especially and be connected technology of preparing with the plastic pelletizing template that the low-alloy stainless steel constitutes by large size wear-and corrosion-proof metal ceramic composite.
Background technology:
Plastic pelletizing template is an important spare part on the chemical industry plastic granulator, and in the plastic pelletizing template manufacturing process, (80 * 50mm) sintering metal sheets are gordian techniquies with the technology that is connected of template body to large size, generally adopt the vacuum brazing method of attachment at present.Because the difference of large size metal ceramic sheet two kinds of material coefficient of thermal expansion coefficients when being connected with the template body and between the two volume differ greatly, in vacuum brazing furnace brazing insulation process of cooling, the speed of cooling of large size metal ceramic sheet is often greater than the speed of cooling of template body, easily causes to crack on the sintering metal sheet after the welding or tiny crack and the pelletizing template that causes preparing are scrapped.
Summary of the invention:
Generation for fear of above-mentioned situation, improve large size wear-and corrosion-proof metal ceramic composite pelletizing template and make the yield rate that vacuum brazing connects, the invention provides and a kind ofly prevent that the method for crackle or tiny crack from appearring in the vacuum brazing process pelletizing template work zone.
The invention provides a kind of preparation method, adopt vacuum slugging treatment technology, it is characterized in that with plastic pelletizing template of large size metal ceramic composite material sheet:
---on the welding region of template body, place the thick braze of 0.3～0.6mm, large size metal ceramic composite material sheet, briquetting successively;
---toroidal membrane is placed in the both sides at the welding band, and scribbles anti-welding stop-off gent between toroidal membrane and template body;
---in toroidal membrane, fill up and have high-melting-point adhesion characteristic powdered heat-resistant material;
---above annular cover plate is placed on;
---put into vacuum brazing furnace and add thermo-welding.
The present invention has among the preparation method of plastic pelletizing template of large size metal ceramic composite material sheet, the bulk material of related plastic pelletizing template is chosen as 1Cr13 stainless steel or SUS440C alloy, large size wear-and corrosion-proof metal ceramic plate preferably is chosen as the TiC/NiCrMo ceramic-metal composite, 0.3 the thick braze of～0.6mm is high-temperature copper-based solder (CuMnCo or CuMnNi), the temperature of vacuum brazing is 1030～1050 ℃, and soaking time is 10～20min.
The present invention has among the preparation method of plastic pelletizing template of large size metal ceramic composite material sheet, and when selecting above-mentioned materials for use, anti-welding stop-off gent is preferably selected boron nitride powder for use.The material powder that wherein has high-melting-point adhesion characteristic is preferably Zirconium oxide powder, and its granularity requirements is at 50～150 μ m.
The present invention has among the preparation method of plastic pelletizing template of large size metal ceramic composite material sheet, heat-resistance stainless steel that can not softening transform when the material of described toroidal membrane and annular cover plate adopts welding, thickness 5～the 10mm of toroidal membrane, the thickness 10～20mm of annular cover plate.The outer shroud of toroidal membrane can be placed on the outer optional position of arriving the template body edges of template body welding band, and ring can be placed on the optional position of arriving template body center in the template body welding band in the toroidal membrane.
Preparation method's the groundwork principle of plastic pelletizing template that the present invention has large size metal ceramic composite material sheet is as follows:
In the temperature-fall period of soldering insulation back, because large size metal ceramic composite material sheet is embedded in the Zirconium oxide powder, heat distributes slowly, can be along with the cooling synchronously simultaneously of template body, reduced the difference of rate of cooling between template body and the large size metal ceramic composite material sheet like this, thereby avoided owing to metal ceramic composite material sheet and the big crackle that produces on the large size metal ceramic composite material sheet that causes of template body rate of cooling difference, thereby improved welding quality, reduced the scrap rate of product.
Description of drawings:
Fig. 1 is the structural representation with plastic pelletizing template of large size metal ceramic composite material sheet;
Fig. 2 is the vacuum brazing frock signal of the plastic pelletizing template of the present invention with large size metal ceramic composite material sheet.
Embodiment:
Plastic pelletizing template as shown in Figure 1, the template bulk material adopts the 1Cr13 stainless steel, be of a size of diameter 665mm * high 95mm, large size wear-and corrosion-proof metal ceramic composite sheet material is the TiC/NiCrMo ceramic-metal composite, be of a size of 100 * 50 * 4mm, 0.3 the thick braze of～0.6mm is high-temperature copper-based CuMnCo solder, ring-type flute profile dividing plate and cover plate adopt the thick stainless steel plate of 5mm to make, and size dimension and shape are defined as cylindrical 520mm * interior round 180mm * high 130mm according to the width of template body and sintering metal sheet and granulation band.On the work zone of template body, place scolder, large size metal ceramic sheet, briquetting; Place toroidal membrane in the both sides of welding band again, and between toroidal membrane and template parent, scribble anti-welding stop-off gent; In toroidal membrane, fill up Zirconium oxide powder then; Above annular cover plate is placed on, put into soldering furnace and add thermo-welding, as shown in Figure 2.Annular baffle (2) should be smooth with template body (1) contact surface, and scribble the stop-off gent boron nitride (3) that prevents with template body (1) seam.Brazing temperature is 1035 ℃, soaking time 15min.Along with the rising of brazing temperature, braze (7) progressively melts, because the effect of anti-welding stop-off gent (3), the scolder of fusing can not flow between annular baffle (2) and the template body (1).After reaching welding temperature, sintering metal sheet (6) links together with template body (1) under the scolder effect, because the effect of annular baffle (2), cover plate (5) and zirconia powder (4), large size wear-and corrosion-proof metal ceramic composite sheet (6) cooling rate more almost is complementary with template body (1) cooling rate, thus the generation of large size metal ceramic composite material sheet crackle when preventing soldering.
Claims (7)
1, a kind of preparation method with plastic pelletizing template of large size metal ceramic composite material sheet adopts vacuum slugging treatment technology, it is characterized in that:
---on the welding region of template body, place the thick braze of 0.3～0.6mm, large size metal ceramic composite material sheet, briquetting successively;
---toroidal membrane is placed in the both sides at the welding band, and scribbles anti-welding stop-off gent between toroidal membrane and template body;
---in toroidal membrane, fill up and have high-melting-point adhesion characteristic powdered heat-resistant material;
---above annular cover plate is placed on;
---put into vacuum brazing furnace and add thermo-welding.
2, according to the described preparation method of claim 1 with plastic pelletizing template of large size metal ceramic composite material sheet, it is characterized in that: described template bulk material is 1Cr13 stainless steel or SUS440C, large size metal ceramic composite material sheet is a TiC based ceramic metal matrix material, and the thick braze of 0.3～0.6mm is high-temperature copper-based solder (CuMnCo or CuMnNi).
3, according to the described preparation method with plastic pelletizing template of large size metal ceramic composite material sheet of claim 2, it is characterized in that: the temperature of vacuum brazing is 1030～1050 ℃, and soaking time is 10～20min.
4, according to the described preparation method with plastic pelletizing template of large size metal ceramic composite material sheet of claim 1, it is characterized in that: described powdered heat-resistant material with high-melting-point adhesion characteristic is a Zirconium oxide powder, granularity 50～150 μ m.
5, according to the described preparation method of claim 1 with plastic pelletizing template of large size metal ceramic composite material sheet, it is characterized in that: the material of described toroidal membrane and annular cover plate adopts the on-deformable heat-resistance stainless steel of high temperature, thickness 5～the 10mm of toroidal membrane, the thickness 10～20mm of annular cover plate.
6, according to the described preparation method with plastic pelletizing template of large size metal ceramic composite material sheet of claim 1, it is characterized in that: described anti-welding stop-off gent is selected boron nitride powder for use.
7, according to the described preparation method of claim 1 with plastic pelletizing template of large size metal ceramic composite material sheet, it is characterized in that: the outer shroud of described toroidal membrane is placed on the outer optional position to the template body edges of template body welding band, and the interior ring of toroidal membrane is placed on the optional position of arriving template body center in the template body welding band.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2004100828916A CN1321945C (en) | 2004-12-08 | 2004-12-08 | Preparation method of plastic pelletizing template having large size metal ceramic composite material sheet |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2004100828916A CN1321945C (en) | 2004-12-08 | 2004-12-08 | Preparation method of plastic pelletizing template having large size metal ceramic composite material sheet |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1785911A true CN1785911A (en) | 2006-06-14 |
| CN1321945C CN1321945C (en) | 2007-06-20 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CNB2004100828916A Expired - Fee Related CN1321945C (en) | 2004-12-08 | 2004-12-08 | Preparation method of plastic pelletizing template having large size metal ceramic composite material sheet |
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| Country | Link |
|---|---|
| CN (1) | CN1321945C (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101905406A (en) * | 2010-07-07 | 2010-12-08 | 沈阳金锋特种刀具有限公司 | Method for repairing plastic granulating die plate by replacing granulating belt |
| CN102950442A (en) * | 2012-11-13 | 2013-03-06 | 深圳市芭田生态工程股份有限公司 | Machining process for extrusion die |
| CN113664399A (en) * | 2021-08-16 | 2021-11-19 | 西安远航真空钎焊技术有限公司 | Machining method of K-shaped partition plate cavity |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO1994016859A1 (en) * | 1993-01-25 | 1994-08-04 | University Of Cincinnati | Combustible slurry for joining metallic or ceramic surfaces or for coating metallic, ceramic and refractory surfaces |
| JP3682552B2 (en) * | 1997-03-12 | 2005-08-10 | 同和鉱業株式会社 | Method for producing metal-ceramic composite substrate |
| CN1184168C (en) * | 2000-12-29 | 2005-01-12 | 中国科学院金属研究所 | Simultaneous process of sintering titanium carbide cermet and welding to steel structure |
| JP3941455B2 (en) * | 2001-10-23 | 2007-07-04 | 宇部興産株式会社 | Bonding method for high heat resistant inorganic fiber bonded ceramics |
-
2004
- 2004-12-08 CN CNB2004100828916A patent/CN1321945C/en not_active Expired - Fee Related
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101905406A (en) * | 2010-07-07 | 2010-12-08 | 沈阳金锋特种刀具有限公司 | Method for repairing plastic granulating die plate by replacing granulating belt |
| CN101905406B (en) * | 2010-07-07 | 2012-06-13 | 沈阳金锋特种刀具有限公司 | Method for repairing plastic granulating die plate by replacing granulating belt |
| CN102950442A (en) * | 2012-11-13 | 2013-03-06 | 深圳市芭田生态工程股份有限公司 | Machining process for extrusion die |
| CN102950442B (en) * | 2012-11-13 | 2015-02-04 | 深圳市芭田生态工程股份有限公司 | Machining process for extrusion die |
| CN113664399A (en) * | 2021-08-16 | 2021-11-19 | 西安远航真空钎焊技术有限公司 | Machining method of K-shaped partition plate cavity |
| CN113664399B (en) * | 2021-08-16 | 2023-10-24 | 西安远航真空钎焊技术有限公司 | Processing method of K-shaped baffle cavity |
Also Published As
| Publication number | Publication date |
|---|---|
| CN1321945C (en) | 2007-06-20 |
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Granted publication date: 20070620 Termination date: 20101208 |