CN1475119A - Long actire insecticide containing natural plant extract and chrysanthemum ester compound and its preparation method - Google Patents
Long actire insecticide containing natural plant extract and chrysanthemum ester compound and its preparation method Download PDFInfo
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- CN1475119A CN1475119A CNA021389535A CN02138953A CN1475119A CN 1475119 A CN1475119 A CN 1475119A CN A021389535 A CNA021389535 A CN A021389535A CN 02138953 A CN02138953 A CN 02138953A CN 1475119 A CN1475119 A CN 1475119A
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
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Abstract
A durable insecticide contains natural plant extract and pyrethrin compound containing cypermethrin, permethrin, propoxur, and the extracts of oleander, castor leaf, etc. Its advantages are high durability (6 months), broad spectrum (mosquito, fly, ant, etc), high effect, and low resistance of pests.
Description
Technical field
The present invention relates to a kind of persistent pesticide, particularly a kind of insecticide that contains extracted form natural plant agent and chrysanthemum ester type compound and preparation method thereof.
Background technology
At present, indoor sanitary insect pest, in the majority with mosquito, fly, cockroach, most insecticides that adopt single component, long-term frequent the use makes sanitary insect pest have certain pesticide resistance, therefore insect killing effect is bad, and adopt the insecticide of several compound component, aspect pesticide resistance, want more durable, but also can progressively develop immunity to drugs.
Summary of the invention
The object of the present invention is to provide a kind of long-acting insecticide that contains extracted form natural plant agent and chrysanthemum ester type compound and preparation method thereof.
The technical solution of the utility model is: a kind of long-acting insecticide that contains extracted form natural plant agent and chrysanthemum ester type compound, form by following ingredients: cypermethrin 5-10 part, Permanone 7-10 part, unden 6-10 part, sweet-scented oleander extractant 5-10 part, wood green pepper extractant 15-25 part, castor bean leaf extractant 15-25 part, glycerine 5-10 part; Emulsifier 20--30 part, deionized water 500--800 part.
In more excellent technical scheme: emulsifier selects for use single or mixed alkyl benzene sulfonic acid sodium salt, fatty alcohol oxygen vinethene sodium sulfonate.
In more excellent technical scheme: sweet-scented oleander extractant, wooden green pepper extractant, castor bean leaf extractant are that water is carried or alcohol extract.
In more excellent technical scheme: also add silicon oil foam killer 3-5 part.
The long-acting preparation that contains the insecticide of extracted form natural plant agent and chrysanthemum ester type compound: with cypermethrin 5-10 part, Permanone 7-10 part, unden 6-10 part, add in the reactor, fully stir as first component with adding 20--30 part emulsifier again behind glycerine 5-10 part and the 100 parts of deionized water dissolvings; Prepare sweet-scented oleander extractant 5-10 part in addition, wooden green pepper extractant 15-25 part, castor bean leaf extractant 15-25 part is with 100 parts of deionized water dissolvings, as second component; The mixing of first and second components is added 300--600 part deionized water and stirring more evenly obtain finished product.
Cypermethrin, Permanone, unden are common insect killing substances, and it compositely can be strengthened insecticidal effect; Sweet-scented oleander, wooden green pepper, castor bean leaf is a mosquito repellent thing commonly used among the people, because of natural extract is difficult for developing immunity to drugs, wherein natural insect killing substance is extracted, again with cypermethrin, Permanone, mixing such as unden, natural insect killing substance and chemosynthesis material synergy can reduce drug resistance significantly, usually just composite compound is developed immunity to drugs through 1 year mosquito, fly, for keeping insecticidal effect, need often to change the prescription of Pesticidal compound, make troubles to enterprise; And behind the interpolation natural extract, according to observation for many years, after product of the present invention stores 5 years, still very good to the killing effect of mosquito, fly.
The adding emulsifier can reduce the surface tension of water, helps the dispersion of particulate in water.Add an amount of conventional silicon oil foam killer again, can significantly reduce the foam that produces because of high-speed stirred.The raw material that the present invention is all stirring of putting together, evenly weak effect is divided into two groups with raw material, select for use single or mixed alkyl benzene sulfonic acid sodium salt, fatty alcohol oxygen vinethene sodium sulfonate, it is very even to make that the material of two kinds of systems of first and second components mixes, and 5 years not stratified, do not precipitate.Deionized water has reduced impurity place to go in the water impurity and caused the possibility that precipitates, and is favourable to product long preservation of the present invention.
The invention has the advantages that: product stablizing effect of the present invention is good, sprays the back efficiency time and is half a year, and it is wide to kill scope, and insects such as mosquito, fly, cockroach, ant, lice, flea are all had the good ability of killing; Because natural insect killing substance and chemosynthesis material have synergy, can reduce drug resistance significantly, insect is difficult for developing immunity to drugs.
Embodiment
Embodiment 1
A kind of long-acting insecticide that contains extracted form natural plant agent and chrysanthemum ester type compound, form by following ingredients: cypermethrin 5-10 part, Permanone 7-10 part, unden 6-10 part, sweet-scented oleander extractant 5-10 part, wood green pepper extractant 15-25 part, castor bean leaf extractant 15-25 part, glycerine 5-10 part; Emulsifier 20--30 part, deionized water 500--800 part.
Embodiment 2
A kind of long-acting insecticide that contains extracted form natural plant agent and chrysanthemum ester type compound, emulsifier selects for use single or mixed alkyl benzene sulfonic acid sodium salt, fatty alcohol oxygen vinethene sodium sulfonate.All the other are with embodiment 1.
Embodiment 3
A kind of long-acting insecticide that contains extracted form natural plant agent and chrysanthemum ester type compound, sweet-scented oleander extractant, wooden green pepper extractant, castor bean leaf extractant are that water is carried or alcohol extract.All the other are with embodiment 1.
Embodiment 4
A kind of long-acting insecticide that contains extracted form natural plant agent and chrysanthemum ester type compound adds silicon oil foam killer 3-5 part.All the other are with embodiment 1.
Embodiment 5
The long-acting preparation that contains the insecticide of extracted form natural plant agent and chrysanthemum ester type compound: with cypermethrin 5-10 part, Permanone 7-10 part, unden 6-10 part, add in the reactor, fully stir as first component with adding 20--30 part emulsifier again behind glycerine 5-10 part and the 100 parts of deionized water dissolvings; Prepare sweet-scented oleander extractant 5-10 part in addition, wooden green pepper extractant 15-25 part, castor bean leaf extractant 15-25 part is with 100 parts of deionized water dissolvings, as second component; The mixing of first and second components is added 300--600 part deionized water and stirring more evenly obtain finished product.
Embodiment 6
A kind of long-acting insecticide that contains extracted form natural plant agent and chrysanthemum ester type compound is made up of following ingredients: 5 parts of cypermethrins, 7 parts of Permanones, 6 parts of undens, 5 parts of sweet-scented oleander extractants, 15 parts of wooden green pepper extractants, 15 parts of castor bean leaf extractants, 5 parts of glycerine; 20 parts of emulsifier, 500 parts of deionized waters.
Embodiment 7
A kind of long-acting insecticide that contains extracted form natural plant agent and chrysanthemum ester type compound is made up of following ingredients: 10 parts of cypermethrins, 10 parts of Permanones, 10 parts of undens, 10 parts of sweet-scented oleander extractants, 25 parts of wooden green pepper extractants, 25 parts of castor bean leaf extractants, 10 parts of glycerine; 30 parts of emulsifier, 800 parts of deionized waters.
Embodiment 8
A kind of long-acting insecticide that contains extracted form natural plant agent and chrysanthemum ester type compound is made up of following ingredients: 8 parts of cypermethrins, 8 parts of Permanones, 8 parts of undens, 6 parts of sweet-scented oleander extractants, 18 parts of wooden green pepper extractants, 18 parts of castor bean leaf extractants, 7 parts of glycerine; 25 parts of emulsifier, 600 parts of deionized waters.
Embodiment 9
A kind of long-acting insecticide that contains extracted form natural plant agent and chrysanthemum ester type compound is made up of following ingredients: 7 parts of cypermethrins, 9 parts of Permanones, 9 parts of undens, 6 parts of sweet-scented oleander extractants, 21 parts of wooden green pepper extractants, 22 parts of castor bean leaf extractants, 6 parts of glycerine; 20 parts of sodium alkyl benzene sulfonates, 3 parts of silicon oil foam killers, 700 parts of deionized waters.
Embodiment 10
A kind of long-acting insecticide that contains extracted form natural plant agent and chrysanthemum ester type compound is made up of following ingredients: 7 parts of cypermethrins, 9 parts of Permanones, 9 parts of undens, 6 parts of sweet-scented oleander extractants, 21 parts of wooden green pepper extractants, 22 parts of castor bean leaf extractants, 6 parts of glycerine; 20 parts of fatty alcohol oxygen vinethene sodium sulfonates, 5 parts of silicon oil foam killers, 700 parts of deionized waters.
Embodiment 11
A kind of long-acting insecticide that contains extracted form natural plant agent and chrysanthemum ester type compound is made up of following ingredients: 7 parts of cypermethrins, 9 parts of Permanones, 9 parts of undens, 6 parts of sweet-scented oleander extractants, 21 parts of wooden green pepper extractants, 22 parts of castor bean leaf extractants, 6 parts of glycerine; 10 parts of sodium alkyl benzene sulfonates, 10 parts of fatty alcohol oxygen vinethene sodium sulfonates, 4 parts of silicon oil foam killers, 700 parts of deionized waters.
Embodiment 12
The insecticide of embodiment 11 is done toxicological detection
Measure, the oral LD50 of its male rat is 3330-5420mg/kg, and the oral LD50 of female rats is 4820-9350mg/kg, this product safety
The insecticide of embodiment 11 is done the evaluation of pesticide effectiveness of killing mosquitos and flies and cockroach.
(1) mosquitos and flies: medicament " is coated on glass plate, paint plank, the lime plate face; and 0 day after the dispenser and 48-52 ℃ of baking 1 week (being equivalent to deposit half a year under the normal temperature), two Time Slot were carried out efficacy testing to mosquitos and flies equably by dispenser dosage 40a.i.mg/M.Test method is carried out according to GB GB 13917.1-92.(2) cockroach: medicament is coated on paint plank, the cement board surface equably by dispenser dosage 70a.i.mg/M, and 0 day after the dispenser and and 48-52 ℃ the baking 1 week (being equivalent to deposit half a year under the normal temperature) two Time Slot cockroach is carried out the evaluation of pesticide effectiveness, test method is carried out according to GB GB 13917.1-92.Every kind of panel triplicate of above-mentioned test.
Above-mentioned detection shows: 24 hours lethality of mosquitos and flies all greater than 80%, are met hygienic insecticide A grade standard.72 hours lethality of cockroach all greater than 80%, are also met hygienic insecticide A grade standard.Different plates is faced mosquitos and flies and cockroach all has good lethal effect.This medicine special efficacy time is long, can be used for indoor delay and sprays the control sanitary insect pest.
Claims (4)
1, a kind of long-acting insecticide that contains extracted form natural plant agent and chrysanthemum ester type compound, it is characterized in that: form: cypermethrin 5-10 part by following ingredients, Permanone 7-10 part, unden 6-10 part, sweet-scented oleander extractant 5-10 part, wood green pepper extractant 15-25 part, castor bean leaf extractant 15-25 part, glycerine 5-10 part; Emulsifier 20--30 part, deionized water 500--800 part.
2, the long-acting insecticide that contains extracted form natural plant agent and chrysanthemum ester type compound according to claim 1 is characterized in that: emulsifier selects for use single or mixed alkyl benzene sulfonic acid sodium salt, fatty alcohol oxygen vinethene sodium sulfonate.
3, the long-acting insecticide that contains extracted form natural plant agent and chrysanthemum ester type compound according to claim 1 is characterized in that: also add silicon oil foam killer 3-5 part.
4, a kind of long-acting method for producing insecticide that contains extracted form natural plant agent and chrysanthemum ester type compound, it is characterized in that: with cypermethrin 5-10 part, Permanone 7-10 part, unden 6-10 part, add in the reactor, fully stir as first component with adding 20--30 part emulsifier again behind glycerine 5-10 part and the 100 parts of deionized water dissolvings; Prepare sweet-scented oleander extractant 5-10 part in addition, wooden green pepper extractant 15-25 part, castor bean leaf extractant 15-25 part is with 100 parts of deionized water dissolvings, as second component; The mixing of first and second components is added 300--600 part deionized water and stirring more evenly obtain finished product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNA021389535A CN1475119A (en) | 2002-08-17 | 2002-08-17 | Long actire insecticide containing natural plant extract and chrysanthemum ester compound and its preparation method |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNA021389535A CN1475119A (en) | 2002-08-17 | 2002-08-17 | Long actire insecticide containing natural plant extract and chrysanthemum ester compound and its preparation method |
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| Publication Number | Publication Date |
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| CN1475119A true CN1475119A (en) | 2004-02-18 |
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| CNA021389535A Pending CN1475119A (en) | 2002-08-17 | 2002-08-17 | Long actire insecticide containing natural plant extract and chrysanthemum ester compound and its preparation method |
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| CN (1) | CN1475119A (en) |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102242215A (en) * | 2011-07-13 | 2011-11-16 | 中国人民解放军军事医学科学院微生物流行病研究所 | Kit for detecting drug resistance of culex pipiens and special primer thereof |
| CN102373280A (en) * | 2011-11-03 | 2012-03-14 | 中国人民解放军军事医学科学院微生物流行病研究所 | Anopheles sinensis drug resistance AS-PCR (Polymerase Chain Reaction) detection kit and special primers thereof |
| CN102373282A (en) * | 2011-11-03 | 2012-03-14 | 中国人民解放军军事医学科学院微生物流行病研究所 | PCR-RFLP (Polymerase Chain Reaction-Amplified Fragment Length Polymorphism) assay kit for drug resistance of anopheles sinensis and special primer of same |
| CN103609621A (en) * | 2013-10-25 | 2014-03-05 | 青岛华仁技术孵化器有限公司 | Traditional Chinese medicine insecticidal composition |
| CN103772785A (en) * | 2014-01-03 | 2014-05-07 | 山东省塑料研究开发中心 | Polyethylene master batch for preventing ant and rat bite from damaging plastic pipelines and preparation method thereof |
| CN104054680A (en) * | 2014-07-04 | 2014-09-24 | 泰山医学院 | Composite fly poisoning rope with oleander water extractive |
| CN113367165A (en) * | 2018-03-02 | 2021-09-10 | 中国农业科学院棉花研究所 | Method for extracting castor-containing insecticidal active substance and combined application of castor-containing insecticidal active substance and pyrethroid insecticide |
-
2002
- 2002-08-17 CN CNA021389535A patent/CN1475119A/en active Pending
Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102242215A (en) * | 2011-07-13 | 2011-11-16 | 中国人民解放军军事医学科学院微生物流行病研究所 | Kit for detecting drug resistance of culex pipiens and special primer thereof |
| CN102373280A (en) * | 2011-11-03 | 2012-03-14 | 中国人民解放军军事医学科学院微生物流行病研究所 | Anopheles sinensis drug resistance AS-PCR (Polymerase Chain Reaction) detection kit and special primers thereof |
| CN102373282A (en) * | 2011-11-03 | 2012-03-14 | 中国人民解放军军事医学科学院微生物流行病研究所 | PCR-RFLP (Polymerase Chain Reaction-Amplified Fragment Length Polymorphism) assay kit for drug resistance of anopheles sinensis and special primer of same |
| CN102373282B (en) * | 2011-11-03 | 2013-04-10 | 中国人民解放军军事医学科学院微生物流行病研究所 | PCR-RFLP (Polymerase Chain Reaction-Amplified Fragment Length Polymorphism) assay kit for drug resistance of anopheles sinensis and special primer of same |
| CN102373280B (en) * | 2011-11-03 | 2013-04-10 | 中国人民解放军军事医学科学院微生物流行病研究所 | Anopheles sinensis drug resistance AS-PCR (Polymerase Chain Reaction) detection kit and special primers thereof |
| CN103609621A (en) * | 2013-10-25 | 2014-03-05 | 青岛华仁技术孵化器有限公司 | Traditional Chinese medicine insecticidal composition |
| CN103772785A (en) * | 2014-01-03 | 2014-05-07 | 山东省塑料研究开发中心 | Polyethylene master batch for preventing ant and rat bite from damaging plastic pipelines and preparation method thereof |
| CN103772785B (en) * | 2014-01-03 | 2016-06-22 | 山东省塑料研究开发中心 | A kind of preventing from being eaten by ant and mouse plastic conduit polyethylene master batch and preparation method thereof |
| CN104054680A (en) * | 2014-07-04 | 2014-09-24 | 泰山医学院 | Composite fly poisoning rope with oleander water extractive |
| CN113367165A (en) * | 2018-03-02 | 2021-09-10 | 中国农业科学院棉花研究所 | Method for extracting castor-containing insecticidal active substance and combined application of castor-containing insecticidal active substance and pyrethroid insecticide |
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