CN1465419A - Supercritical carbon dioxide extraction apparatus - Google Patents
Supercritical carbon dioxide extraction apparatus Download PDFInfo
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- CN1465419A CN1465419A CNA021324840A CN02132484A CN1465419A CN 1465419 A CN1465419 A CN 1465419A CN A021324840 A CNA021324840 A CN A021324840A CN 02132484 A CN02132484 A CN 02132484A CN 1465419 A CN1465419 A CN 1465419A
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- carbon dioxide
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- extraction kettle
- separating still
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Abstract
The present invention relates to a supercritical CO2 extraction equipment, it includes CO2 cylinder and mixer, cold tank, storage tank, CO2 plunger pump, heat exchanger which is parallelly-connected with connected with inlet of bottom portion of every extractor, two sides of upper end of every extractor are respectively equipped with two outlets, one outlet is connected with inlet of separator so as to form separation pipeline, another outlet is connected with drying filter by means of non-return valve so as to form gas-supply pipeline, the outlet of upper end of separation is connected with drying filter by means of nonreturn valve, and the material outlet of the lower end of separator is connected with receiver, so that it can save CO2 and can continuously make production.
Description
The present invention relates to a kind of commercial scale supercritical carbon dioxide extraction equipment, particularly relate to a kind of efficient, energy-conservation supercritical carbon dioxide extraction apparatus.
Present supercritical carbon dioxide extraction apparatus, what adopted is single still or two still batch (-type), also has multi-still continuous.But their weak point is: must be carbon dioxide emptying more than the 5Mpa being deposited in pressure at least in the extraction kettle after the balance before discharging, available carbon dioxide is slatterned, energy consumption be big.
The object of the present invention is to provide a kind of high efficiency that has, the supercritical carbon dioxide device of low energy consumption.
In order to achieve the above object, the technical solution used in the present invention is: carbon dioxide steel cylinder and blender, ice chest, storage tank, the carbon dioxide plunger displacement pump is together in series, carbon dioxide plunger delivery side of pump and each extraction kettle bottom inlet are connected in parallel, heat exchangers in series all between carbon dioxide plunger displacement pump and the extraction kettle, the both sides, upper end of each extraction kettle have two outlets respectively, an outlet is connected with the separating still import, constitute and separate pipeline, separate on the pipeline and also be provided with Pressure gauge and safety valve, another outlet is passed through back only to be connected with device for drying and filtering, constitute supply air line, the supply air line of each extraction kettle all is connected with next extraction kettle bottom inlet, first separating still upper end exports in second separating still upper end import and connects, second separating still upper end outlet passed through back to end valve and is connected with device for drying and filtering, and separating still lower end material outlet links to each other with receiver.
Compare with prior art, the present invention has following advantage:
1, energy serialization production is raised the efficiency;
2, can save carbon dioxide, the big more saving carbon dioxide of extraction kettle volume is many more.
As shown in Figure 1, four extraction kettles are divided into two groups, promptly 11,12 is first group, and 13,14 is second group, but two still series and parallel switchover operations of every group.First group 11,12 parallel runnings; Open stop valve 1,7,8,24,26 and control valve 27, remaining valve closing, at this moment carbon dioxide enters in extraction kettle 11,12 and the separating still 28,31 immediately in the steel cylinder, get rid of the air in each still simultaneously, after treating pressure balance, close control valve 27, open carbon dioxide plunger displacement pump 5, condition such as extraction temperature, pressure is decided on different products, concrete operating path is: the carbon dioxide in the steel cylinder 33 enters in the extraction kettle 11,12 through blender 2, ice chest 3, storage tank 4, heat exchanger 5 under the effect of plunger displacement pump 5.When extraction kettle pressure reaches setting pressure, open control valve 27, the beginning dynamic operation enters in the separating still 28,31 supercritical carbon dioxide fluid and solute and separates, and the carbon dioxide after the separation enters device for drying and filtering 35 through valve 34 time only and anhydrates and recycle after part.After running to setting-up time, the big pump 5 of closing carbon dioxide plunger is emitted product from receiver 29,32, and extraction finishes.Second group 13,14 parallel runnings; Close stop valve 1, cut off the steel cylinder air supply source, close stop valve 7,8,24,26 and control valve 27, open stop valve 15,16,17, extraction kettle 11, carbon dioxide in 12 is put into extraction kettle 13,14 li, air in the still of emptying simultaneously, after treating 4 still pressure balances, close stop valve 15,16,17, open stop valve 9,10,23,25, open carbon dioxide plunger displacement pump 5, extraction kettle 11,12 carbon dioxide is as source of the gas, squeeze into extraction kettle 13,14 li, open stop valve 20,22, with control valve 27 control extraction kettles 13,14 pressure, when extraction kettle 11, when 12 pressure drop to 3Mpa, extraction kettle 11, carbon dioxide in 12 can not utilize again, closes stop valve 23,25, switch to steel cylinder 33 air feed.Bleed off the residual air in the extraction kettle 11,12 then, shed waste residue, the virgin material of packing into is stand-by.After running to setting-up time, closing carbon dioxide plunger displacement pump 5 is emitted product from receiver 29,32, and extraction finishes.Switch back to first sets in parallel operation; Close stop valve 1,9,10,22 and control valve 27, open stop valve 20,22,15,16, extraction kettle 13, carbon dioxide in 14 is put into extraction kettle 11,12 li, air in the still of emptying simultaneously, after treating 4 still pressure balances, close stop valve 20,22,15,16, open stop valve 7,8,19,21, open carbon dioxide plunger displacement pump 5, extraction kettle 13,14 carbon dioxide is as source of the gas, squeeze into extraction kettle 11,12 li, open stop valve 24,26, with control valve 27 control extraction kettles 11,12 pressure is when extraction kettle 13, when 14 pressure drop to 3Pma, extraction kettle 13, carbon dioxide in 14 can not utilize again, close stop valve 19,21, can change to steel cylinder 33 air feed, bleed off extraction kettle 13 then, residual air in 14, shed waste residue, the virgin material of packing into is stand-by.After running to setting-up time, the closing carbon dioxide plunger displacement pump is emitted product from receiver 29,32, and extraction finishes.Operation is later on all undertaken by above-mentioned method of operating.
Description of drawings
Fig. 1 is a structural representation of the present invention
Specific embodiment
Below in conjunction with accompanying drawing embodiments of the invention 1 being done to advance to go up the step comment describes
It is at carbon dioxide steel cylinder 33 and blender 2, ice chest 3, storage tank 4, carbon dioxide plunger displacement pump 5 is together in series, the outlet of carbon dioxide plunger displacement pump 5 and each extraction kettle 11,12,13,14 bottom inlet are connected in parallel, carbon dioxide plunger displacement pump 5 and extraction kettle 11,12,13, heat exchangers in series 6 all between 14, each extraction kettle 11,12,13,14 both sides, upper end have two outlets respectively, one outlet and separating still 28,29 imports connect, constitute and separate pipeline, separate on the pipeline and also be provided with Pressure gauge and safety valve, another outlet is only passed through back, and valve 33 is connected with device for drying and filtering 35, constitute supply air line, each extraction kettle 11,12,13,14 supply air line all with next extraction kettle 11,12,13,14 bottom inlet connect, first separating still 28 upper ends export in the 31 upper end imports of second separating still and connect, second separating still 31 upper ends outlet only passed through back, and valve 34 is connected separating still 28 with device for drying and filtering 35,31 lower end material outlets and receiver 29,32 link to each other.
Described supply air line with separate pipeline on stop valve 7,8,9,10,15,16,17,18,19,20,21,22,23,24,25,26,27 is installed respectively.
Extraction kettle of the present invention can adopt a plurality of extraction kettles to be divided into two groups of alternate runs.
Claims (2)
1, a kind of supercritical carbon dioxide extraction apparatus, it is characterized in that: carbon dioxide steel cylinder (33) and blender (2), ice chest (3), storage tank (4), carbon dioxide plunger displacement pump (5) is together in series, the outlet of carbon dioxide plunger displacement pump (5) and each extraction kettle (11), (12), (13), (14) bottom inlet is connected in parallel, carbon dioxide plunger displacement pump (5) and extraction kettle (11), (12), (13), (14) heat exchangers in series (6) all between, each extraction kettle (11), (12), (13), (14) both sides, upper end have two outlets respectively, one outlet and separating still (28), (29) import connects, constitute and separate pipeline, separate on the pipeline and also be provided with Pressure gauge and safety valve, another outlet is only passed through back, and valve (33) is connected with device for drying and filtering (35), constitute supply air line, each extraction kettle (11), (12), (13), (14) supply air line all with next extraction kettle (11), (12), (13), (14) bottom inlet connects, first separating still (28) upper end exports in second separating still (31) upper end import and connects, the outlet of second separating still (31) upper end is only passed through back, and valve (34) is connected separating still (28) with device for drying and filtering (35), (31) lower end material outlet and receiver (29), (32) link to each other.
2, according to the described supercritical carbon dioxide extraction apparatus of claim 1, it is characterized in that: supply air line with separate pipeline on install respectively stop valve (7), (8), (90, (10), (15), (16), (17), (18), (19), (20), (21), (22), (23), (24), (25), (26), (27).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNA021324840A CN1465419A (en) | 2002-06-24 | 2002-06-24 | Supercritical carbon dioxide extraction apparatus |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNA021324840A CN1465419A (en) | 2002-06-24 | 2002-06-24 | Supercritical carbon dioxide extraction apparatus |
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| Publication Number | Publication Date |
|---|---|
| CN1465419A true CN1465419A (en) | 2004-01-07 |
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| Application Number | Title | Priority Date | Filing Date |
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| CNA021324840A Pending CN1465419A (en) | 2002-06-24 | 2002-06-24 | Supercritical carbon dioxide extraction apparatus |
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Cited By (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100427172C (en) * | 2005-03-04 | 2008-10-22 | 山东大学 | Apparatus for continuous extracting and sterilizing solid materials under high and ultrahigh pressure |
| CN102120100A (en) * | 2011-02-12 | 2011-07-13 | 重庆市润东油脂有限公司 | Process and device for continuously extracting supercritical CO2 in flat turn manner |
| CN103724388A (en) * | 2013-11-26 | 2014-04-16 | 沃太能源南通有限公司 | Method for extracting phytosterol from beans |
| CN104645663A (en) * | 2015-03-12 | 2015-05-27 | 浙江天草生物科技股份有限公司 | Heat exchange type continuous plant extraction system |
| TWI492777B (en) * | 2013-05-07 | 2015-07-21 | Ta Chiang Internat Co | Parallel ultrasonic extraction device |
| CN104931647A (en) * | 2015-04-09 | 2015-09-23 | 青岛科技大学 | Dynamical quick measuring device for desolventizing residual solvent in thermosensitive solid medicine in high-pressure CO2 (carbon dioxide) manner |
| CN105597368A (en) * | 2016-03-14 | 2016-05-25 | 青岛利和萃取股份有限公司 | Supercritical extraction kettle and extraction system comprising supercritical extraction kettle |
| CN107057849A (en) * | 2017-05-12 | 2017-08-18 | 祖柏实 | A kind of continous way supercritical CO 2 refining edible fat production equipment |
| CN107126725A (en) * | 2017-05-19 | 2017-09-05 | 江苏宏博机械制造有限公司 | A kind of continuous flow upstream supercritical extraction unit |
| CN110899248A (en) * | 2019-06-21 | 2020-03-24 | 杭州杭氧股份有限公司 | System and method for cleaning ultrahigh-purity gas steel cylinders in batch by using supercritical fluid |
| CN112604320A (en) * | 2020-11-30 | 2021-04-06 | 青岛理工大学 | Pre-dispersion micro-nano bubble supported liquid film generator |
-
2002
- 2002-06-24 CN CNA021324840A patent/CN1465419A/en active Pending
Cited By (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100427172C (en) * | 2005-03-04 | 2008-10-22 | 山东大学 | Apparatus for continuous extracting and sterilizing solid materials under high and ultrahigh pressure |
| CN102120100A (en) * | 2011-02-12 | 2011-07-13 | 重庆市润东油脂有限公司 | Process and device for continuously extracting supercritical CO2 in flat turn manner |
| TWI492777B (en) * | 2013-05-07 | 2015-07-21 | Ta Chiang Internat Co | Parallel ultrasonic extraction device |
| CN103724388A (en) * | 2013-11-26 | 2014-04-16 | 沃太能源南通有限公司 | Method for extracting phytosterol from beans |
| CN104645663A (en) * | 2015-03-12 | 2015-05-27 | 浙江天草生物科技股份有限公司 | Heat exchange type continuous plant extraction system |
| CN104931647A (en) * | 2015-04-09 | 2015-09-23 | 青岛科技大学 | Dynamical quick measuring device for desolventizing residual solvent in thermosensitive solid medicine in high-pressure CO2 (carbon dioxide) manner |
| CN105597368A (en) * | 2016-03-14 | 2016-05-25 | 青岛利和萃取股份有限公司 | Supercritical extraction kettle and extraction system comprising supercritical extraction kettle |
| CN107057849A (en) * | 2017-05-12 | 2017-08-18 | 祖柏实 | A kind of continous way supercritical CO 2 refining edible fat production equipment |
| CN107126725A (en) * | 2017-05-19 | 2017-09-05 | 江苏宏博机械制造有限公司 | A kind of continuous flow upstream supercritical extraction unit |
| CN110899248A (en) * | 2019-06-21 | 2020-03-24 | 杭州杭氧股份有限公司 | System and method for cleaning ultrahigh-purity gas steel cylinders in batch by using supercritical fluid |
| CN112604320A (en) * | 2020-11-30 | 2021-04-06 | 青岛理工大学 | Pre-dispersion micro-nano bubble supported liquid film generator |
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