CN1453262A - Production process of pyrogallic acid - Google Patents
Production process of pyrogallic acid Download PDFInfo
- Publication number
- CN1453262A CN1453262A CN 03117943 CN03117943A CN1453262A CN 1453262 A CN1453262 A CN 1453262A CN 03117943 CN03117943 CN 03117943 CN 03117943 A CN03117943 A CN 03117943A CN 1453262 A CN1453262 A CN 1453262A
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- Prior art keywords
- decarboxylation
- narrow
- pyrogallol
- drainage
- earthen jar
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Claims (1)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN 03117943 CN1209338C (en) | 2003-05-23 | 2003-05-23 | Production process of pyrogallic acid |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
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CN 03117943 CN1209338C (en) | 2003-05-23 | 2003-05-23 | Production process of pyrogallic acid |
Publications (2)
Publication Number | Publication Date |
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CN1453262A true CN1453262A (en) | 2003-11-05 |
CN1209338C CN1209338C (en) | 2005-07-06 |
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Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
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CN 03117943 Expired - Fee Related CN1209338C (en) | 2003-05-23 | 2003-05-23 | Production process of pyrogallic acid |
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CN (1) | CN1209338C (en) |
Cited By (12)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN100336791C (en) * | 2005-07-29 | 2007-09-12 | 保廷荣 | Coupling type heating method for preparing pyrogallic acid |
CN101161628B (en) * | 2007-11-15 | 2010-06-16 | 浙江大学 | Method for preparing gallic acid and pyrogallic acid synchronously by non-catalyzed hydrolysis of tannin-containing biomass in high-temperature liquid water medium |
CN101928204A (en) * | 2009-06-18 | 2010-12-29 | 遵义林源医药化工有限责任公司 | Production method of high-purity pyrogallol |
CN102671413A (en) * | 2012-05-16 | 2012-09-19 | 六盘水神驰生物科技有限公司 | Multi-point multi-temperature control coking gallic acid sublimation device for sublimation method |
CN102671411A (en) * | 2012-05-16 | 2012-09-19 | 六盘水神驰生物科技有限公司 | Device for recovering pyrogallic acids through electrostatic adsorption by using sublimation method |
CN103449977A (en) * | 2013-08-19 | 2013-12-18 | 竹山县天新医药化工有限责任公司 | Pyrogallic acid production method |
CN106220476A (en) * | 2016-08-02 | 2016-12-14 | 遵义市倍缘化工有限责任公司 | A kind of low pressure catalytic prepares the method for pyrogallic acid |
CN106621441A (en) * | 2016-11-10 | 2017-05-10 | 遵义林源医药化工有限责任公司 | Sublimation kettle and method for preparing pyrogallic acid by utilizing same |
CN107445804A (en) * | 2017-08-25 | 2017-12-08 | 贵州自然生物科技有限公司 | A kind of high-purity pyrogallol production method |
CN109400447A (en) * | 2018-11-13 | 2019-03-01 | 科利生物科技(徐州)有限公司 | The preparation method of pyrogallol |
CN109534962A (en) * | 2018-12-18 | 2019-03-29 | 湘潭大学 | The method of pyrogallic acid is prepared using organic amine as gallate decarboxylation accelerant |
CN111517924A (en) * | 2020-04-24 | 2020-08-11 | 遵义市倍缘化工有限责任公司 | Method for producing pyrogallic acid by using tannic acid |
-
2003
- 2003-05-23 CN CN 03117943 patent/CN1209338C/en not_active Expired - Fee Related
Cited By (16)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN100336791C (en) * | 2005-07-29 | 2007-09-12 | 保廷荣 | Coupling type heating method for preparing pyrogallic acid |
CN101161628B (en) * | 2007-11-15 | 2010-06-16 | 浙江大学 | Method for preparing gallic acid and pyrogallic acid synchronously by non-catalyzed hydrolysis of tannin-containing biomass in high-temperature liquid water medium |
CN101928204A (en) * | 2009-06-18 | 2010-12-29 | 遵义林源医药化工有限责任公司 | Production method of high-purity pyrogallol |
CN102671413A (en) * | 2012-05-16 | 2012-09-19 | 六盘水神驰生物科技有限公司 | Multi-point multi-temperature control coking gallic acid sublimation device for sublimation method |
CN102671411A (en) * | 2012-05-16 | 2012-09-19 | 六盘水神驰生物科技有限公司 | Device for recovering pyrogallic acids through electrostatic adsorption by using sublimation method |
CN102671411B (en) * | 2012-05-16 | 2015-01-14 | 六盘水神驰生物科技有限公司 | Device for recovering pyrogallic acids through electrostatic adsorption by using sublimation method |
CN103449977A (en) * | 2013-08-19 | 2013-12-18 | 竹山县天新医药化工有限责任公司 | Pyrogallic acid production method |
CN103449977B (en) * | 2013-08-19 | 2015-09-30 | 竹山县天新医药化工有限责任公司 | A kind of production method of pyrogallol |
CN106220476A (en) * | 2016-08-02 | 2016-12-14 | 遵义市倍缘化工有限责任公司 | A kind of low pressure catalytic prepares the method for pyrogallic acid |
CN106220476B (en) * | 2016-08-02 | 2018-12-18 | 遵义市倍缘化工有限责任公司 | A kind of method that low pressure catalytic prepares pyrogallic acid |
CN106621441A (en) * | 2016-11-10 | 2017-05-10 | 遵义林源医药化工有限责任公司 | Sublimation kettle and method for preparing pyrogallic acid by utilizing same |
CN106621441B (en) * | 2016-11-10 | 2019-01-25 | 遵义林源医药化工有限责任公司 | A method of distillation and prepares pyrogallic acid using it at kettle |
CN107445804A (en) * | 2017-08-25 | 2017-12-08 | 贵州自然生物科技有限公司 | A kind of high-purity pyrogallol production method |
CN109400447A (en) * | 2018-11-13 | 2019-03-01 | 科利生物科技(徐州)有限公司 | The preparation method of pyrogallol |
CN109534962A (en) * | 2018-12-18 | 2019-03-29 | 湘潭大学 | The method of pyrogallic acid is prepared using organic amine as gallate decarboxylation accelerant |
CN111517924A (en) * | 2020-04-24 | 2020-08-11 | 遵义市倍缘化工有限责任公司 | Method for producing pyrogallic acid by using tannic acid |
Also Published As
Publication number | Publication date |
---|---|
CN1209338C (en) | 2005-07-06 |
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C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
ASS | Succession or assignment of patent right |
Owner name: LUPANSHUI SHENCHI BIOLOGY TECHNOLOGY LTD. Free format text: FORMER OWNER: HUAXIANG CHEMICAL INDUSTRY CO., LTD., LIUPANSHUI Effective date: 20060728 |
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C41 | Transfer of patent application or patent right or utility model | ||
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Effective date of registration: 20060728 Address after: 553004 Guizhou city of Liupanshui province Zhongshan dewu South Road Patentee after: Liupanshui Shenchi Biotechnology Co., Ltd. Address before: 553001 flower fishing cave, Zijin Mountain District, Guizhou City, Liupanshui province (Shuicheng Brewing Factory) Patentee before: Huaxiang Chemical Industry Co., Ltd., Liupanshui |
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CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20050706 Termination date: 20130523 |