CN1405367A - Method for preparing extra high molecular polyethylene high-concentrated solution for spinning - Google Patents
Method for preparing extra high molecular polyethylene high-concentrated solution for spinning Download PDFInfo
- Publication number
- CN1405367A CN1405367A CN 01123600 CN01123600A CN1405367A CN 1405367 A CN1405367 A CN 1405367A CN 01123600 CN01123600 CN 01123600 CN 01123600 A CN01123600 A CN 01123600A CN 1405367 A CN1405367 A CN 1405367A
- Authority
- CN
- China
- Prior art keywords
- mother liquor
- temperature
- preparation
- solution
- concentration
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 229920000573 polyethylene Polymers 0.000 title claims abstract description 28
- 238000009987 spinning Methods 0.000 title claims description 41
- 239000004698 Polyethylene Substances 0.000 title claims description 25
- -1 polyethylene Polymers 0.000 title claims description 25
- 238000000034 method Methods 0.000 title description 10
- 238000003756 stirring Methods 0.000 claims abstract description 47
- 239000000843 powder Substances 0.000 claims abstract description 24
- 239000003292 glue Substances 0.000 claims abstract description 16
- 239000002002 slurry Substances 0.000 claims abstract description 12
- 239000002245 particle Substances 0.000 claims abstract description 8
- 239000002904 solvent Substances 0.000 claims abstract description 8
- 239000012452 mother liquor Substances 0.000 claims description 55
- 239000007788 liquid Substances 0.000 claims description 25
- 238000002360 preparation method Methods 0.000 claims description 25
- 238000004090 dissolution Methods 0.000 claims description 12
- 230000035699 permeability Effects 0.000 claims description 9
- 238000005191 phase separation Methods 0.000 claims description 9
- 230000008961 swelling Effects 0.000 claims description 9
- 230000010355 oscillation Effects 0.000 claims description 7
- 239000002994 raw material Substances 0.000 claims description 6
- 239000003507 refrigerant Substances 0.000 claims description 6
- 238000010438 heat treatment Methods 0.000 claims description 4
- 230000000630 rising effect Effects 0.000 claims description 4
- 238000009826 distribution Methods 0.000 claims description 3
- 238000010410 dusting Methods 0.000 claims description 3
- 239000000945 filler Substances 0.000 claims description 3
- 239000007921 spray Substances 0.000 claims description 3
- 238000010792 warming Methods 0.000 claims description 3
- 239000005662 Paraffin oil Substances 0.000 claims description 2
- 229910004116 SrO 2 Inorganic materials 0.000 claims description 2
- 239000003963 antioxidant agent Substances 0.000 claims description 2
- 230000003078 antioxidant effect Effects 0.000 claims description 2
- 239000000203 mixture Substances 0.000 claims description 2
- 239000002086 nanomaterial Substances 0.000 claims description 2
- 238000000926 separation method Methods 0.000 claims description 2
- 239000003381 stabilizer Substances 0.000 claims description 2
- 239000004699 Ultra-high molecular weight polyethylene Substances 0.000 claims 1
- 230000002045 lasting effect Effects 0.000 claims 1
- 229920000785 ultra high molecular weight polyethylene Polymers 0.000 claims 1
- 239000000243 solution Substances 0.000 abstract description 49
- 238000004519 manufacturing process Methods 0.000 abstract description 11
- 239000000835 fiber Substances 0.000 abstract description 9
- 229920000098 polyolefin Polymers 0.000 abstract description 6
- 230000008014 freezing Effects 0.000 abstract 2
- 238000007710 freezing Methods 0.000 abstract 2
- 150000001336 alkenes Chemical class 0.000 abstract 1
- 239000010413 mother solution Substances 0.000 abstract 1
- JRZJOMJEPLMPRA-UHFFFAOYSA-N olefin Natural products CCCCCCCC=C JRZJOMJEPLMPRA-UHFFFAOYSA-N 0.000 abstract 1
- 238000001816 cooling Methods 0.000 description 6
- 229920000642 polymer Polymers 0.000 description 5
- 238000005516 engineering process Methods 0.000 description 4
- 230000000052 comparative effect Effects 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- 230000015556 catabolic process Effects 0.000 description 2
- 230000008859 change Effects 0.000 description 2
- 230000006835 compression Effects 0.000 description 2
- 238000007906 compression Methods 0.000 description 2
- 238000006731 degradation reaction Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000002474 experimental method Methods 0.000 description 2
- 238000001125 extrusion Methods 0.000 description 2
- 230000009471 action Effects 0.000 description 1
- 238000007664 blowing Methods 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 238000009413 insulation Methods 0.000 description 1
- 239000011259 mixed solution Substances 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 238000004321 preservation Methods 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 238000005086 pumping Methods 0.000 description 1
- 238000004904 shortening Methods 0.000 description 1
- 230000007704 transition Effects 0.000 description 1
Landscapes
- Artificial Filaments (AREA)
Abstract
Description
Project unit | TENSILE STRENGTH g/d | Modulus g/d | Extension at break % | Continuous reeling time hour | Matched proportion density % | Production cycle process time hour | Remarks |
Embodiment 1 | ??30 | ??1100 | ????3 | ????60 | ????12 | ????6 | |
Embodiment 2 | ??32 | ??1300 | ????2 | ????80 | ????24 | ????4 | |
Comparative example 1 | ??22 | ??750 | ????4 | ????10 | ????6 | ????48 |
Claims (8)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN 01123600 CN1256471C (en) | 2001-08-13 | 2001-08-13 | Method for preparing extra high molecular polyethylene high-concentrated solution for spinning |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN 01123600 CN1256471C (en) | 2001-08-13 | 2001-08-13 | Method for preparing extra high molecular polyethylene high-concentrated solution for spinning |
Publications (2)
Publication Number | Publication Date |
---|---|
CN1405367A true CN1405367A (en) | 2003-03-26 |
CN1256471C CN1256471C (en) | 2006-05-17 |
Family
ID=4665180
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN 01123600 Expired - Lifetime CN1256471C (en) | 2001-08-13 | 2001-08-13 | Method for preparing extra high molecular polyethylene high-concentrated solution for spinning |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN1256471C (en) |
Cited By (11)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2005066397A1 (en) * | 2003-12-19 | 2005-07-21 | Sinotex Investment & Development Co., Ltd. | A process for preparing ultra high molecular weight polyethylene fibres |
CN100441753C (en) * | 2006-07-18 | 2008-12-10 | 东华大学 | Prepn of hollow high-strength light-modulus polyethylene fiber |
CN101153079B (en) * | 2006-09-29 | 2010-05-12 | 上海化工研究院天地科技发展有限公司 | Method of preprocessing ultrahigh molecular weight polyethylene for spinning |
CN101575743B (en) * | 2008-05-05 | 2011-04-13 | 宁波荣溢化纤科技有限公司 | Preparation method of spinning solution of ultra-high molecular weight polyethylene fiber |
CN101629323B (en) * | 2008-07-17 | 2011-07-27 | 宁波荣溢化纤科技有限公司 | Method for conveying spinning suspension of ultra-high molecular weight polyethylene fiber |
WO2012025034A1 (en) * | 2010-08-24 | 2012-03-01 | 北京同益中特种纤维技术开发有限公司 | Method for preparing spinning solution of ultra-high molecular weight polyethylene fiber |
CN101724921B (en) * | 2009-11-26 | 2012-11-21 | 宁波大成新材料股份有限公司 | Process for evenly preparing spinning by using ultrahigh molecular weight polyethylene high-shearing solution |
CN107988632A (en) * | 2017-11-24 | 2018-05-04 | 龙游龙纤新材料有限公司 | A kind of UHMWPE fibers production distribution for realizing continuous uniform feeding |
CN109468700A (en) * | 2018-10-31 | 2019-03-15 | 盐城优和博新材料有限公司 | A kind of manufacturing method of antibacterial high-strength polyethylene fibre |
CN110158160A (en) * | 2019-06-28 | 2019-08-23 | 上海化工研究院有限公司 | A kind of method of high concentration gel spinning preparation ultra high molecular weight polyethylene fiber |
CN111005079A (en) * | 2019-12-18 | 2020-04-14 | 黑龙江金源仑特种纤维有限公司 | Method for manufacturing ultra-high molecular weight polyethylene monofilament fiber |
Families Citing this family (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101967686B (en) * | 2010-09-21 | 2012-04-25 | 中国科学院宁波材料技术与工程研究所 | Method for preparing ultra-high molecular weight polyethylene fiber spinning solution |
-
2001
- 2001-08-13 CN CN 01123600 patent/CN1256471C/en not_active Expired - Lifetime
Cited By (15)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2005066397A1 (en) * | 2003-12-19 | 2005-07-21 | Sinotex Investment & Development Co., Ltd. | A process for preparing ultra high molecular weight polyethylene fibres |
CN100441753C (en) * | 2006-07-18 | 2008-12-10 | 东华大学 | Prepn of hollow high-strength light-modulus polyethylene fiber |
CN101153079B (en) * | 2006-09-29 | 2010-05-12 | 上海化工研究院天地科技发展有限公司 | Method of preprocessing ultrahigh molecular weight polyethylene for spinning |
CN101575743B (en) * | 2008-05-05 | 2011-04-13 | 宁波荣溢化纤科技有限公司 | Preparation method of spinning solution of ultra-high molecular weight polyethylene fiber |
CN101629323B (en) * | 2008-07-17 | 2011-07-27 | 宁波荣溢化纤科技有限公司 | Method for conveying spinning suspension of ultra-high molecular weight polyethylene fiber |
CN101724921B (en) * | 2009-11-26 | 2012-11-21 | 宁波大成新材料股份有限公司 | Process for evenly preparing spinning by using ultrahigh molecular weight polyethylene high-shearing solution |
WO2012025034A1 (en) * | 2010-08-24 | 2012-03-01 | 北京同益中特种纤维技术开发有限公司 | Method for preparing spinning solution of ultra-high molecular weight polyethylene fiber |
RU2533130C1 (en) * | 2010-08-24 | 2014-11-20 | Бэйцзин Туничжун Спешиалти Файбер Текнолоджи Энд Дивелопмент Ко., Лтд | Method of obtaining spinning solution for ultra-high molecular weight polyethylene fibre |
US9296875B2 (en) | 2010-08-24 | 2016-03-29 | Beijing Tongyizhong Specialty Fibre Technology & Development Co., Ltd | Method for preparing spinning solution of ultra-high molecular weight polyethylene fiber |
CN107988632A (en) * | 2017-11-24 | 2018-05-04 | 龙游龙纤新材料有限公司 | A kind of UHMWPE fibers production distribution for realizing continuous uniform feeding |
CN107988632B (en) * | 2017-11-24 | 2020-04-24 | 龙游龙纤新材料有限公司 | UHMWPE fiber production and batching method capable of realizing continuous and uniform feeding |
CN109468700A (en) * | 2018-10-31 | 2019-03-15 | 盐城优和博新材料有限公司 | A kind of manufacturing method of antibacterial high-strength polyethylene fibre |
CN110158160A (en) * | 2019-06-28 | 2019-08-23 | 上海化工研究院有限公司 | A kind of method of high concentration gel spinning preparation ultra high molecular weight polyethylene fiber |
CN110158160B (en) * | 2019-06-28 | 2024-02-27 | 上海化工研究院有限公司 | Method for preparing ultra-high molecular weight polyethylene fiber by high-concentration gel spinning |
CN111005079A (en) * | 2019-12-18 | 2020-04-14 | 黑龙江金源仑特种纤维有限公司 | Method for manufacturing ultra-high molecular weight polyethylene monofilament fiber |
Also Published As
Publication number | Publication date |
---|---|
CN1256471C (en) | 2006-05-17 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
C06 | Publication | ||
PB01 | Publication | ||
C10 | Entry into substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
EE01 | Entry into force of recordation of patent licensing contract |
Assignee: BEIJING TONGYIZHONG SPECIALTY FIBRE TECHNOLOGY & DEVELOPMENT Co.,Ltd. Assignor: SINOTEX INVESTMENT&DEVELOPMENT Co.,Ltd. Contract fulfillment period: 2007.10.10 to 2017.10.10 Contract record no.: 2008110000119 Denomination of invention: Method for preparing extra high molecular polyethylene high-concentrated solution for spinning Granted publication date: 20060517 License type: Exclusive license Record date: 20081114 |
|
LIC | Patent licence contract for exploitation submitted for record |
Free format text: EXCLUSIVE LICENSE; TIME LIMIT OF IMPLEMENTING CONTACT: 2007.10.10 TO 2017.10.10; CHANGE OF CONTRACT Name of requester: BEIJING TONGYIZHONG SPECIAL FIBER TECHNOLOGY DEVEL Effective date: 20081114 |
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C41 | Transfer of patent application or patent right or utility model | ||
C56 | Change in the name or address of the patentee | ||
CP03 | Change of name, title or address |
Address after: 4202, room 200120, National Development Bank, 500 Pudong Road, Shanghai Patentee after: SDIC Limited by Share Ltd. Address before: 200120, room 1805, Liao Sheng Liao building, Shangcheng Road, Shanghai, Pudong New Area Patentee before: SINOTEX INVESTMENT&DEVELOPMENT Co.,Ltd. |
|
TR01 | Transfer of patent right |
Effective date of registration: 20151104 Address after: 100176 901 factory building, No. 16 Zhonghe street, Beijing economic and Technological Development Zone, Beijing, Daxing District Patentee after: BEIJING TONGYIZHONG SPECIALTY FIBRE TECHNOLOGY & DEVELOPMENT Co.,Ltd. Address before: 4202, room 200120, National Development Bank, 500 Pudong Road, Shanghai Patentee before: SDIC Limited by Share Ltd. |
|
CP03 | Change of name, title or address | ||
CP03 | Change of name, title or address |
Address after: 100076 901 Workshop, No. 16 Zhonghe Street, Beijing Economic and Technological Development Zone Patentee after: BEIJING TONGYIZHONG NEW MATERIAL TECHNOLOGY Corp. Address before: 100176 901 Workshop, No. 16 Zhonghe Street, Daxing District, Beijing Economic and Technological Development Zone Patentee before: BEIJING TONGYIZHONG SPECIALTY FIBRE TECHNOLOGY & DEVELOPMENT Co.,Ltd. |
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CX01 | Expiry of patent term | ||
CX01 | Expiry of patent term |
Granted publication date: 20060517 |